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Synthesis and characterization of four metal-organophosphonates with one-, two-, and three-dimensional structures.

Inorganic chemistry

Konar S, Zoń J, Prosvirin AV, Dunbar KR, Clearfield A.
PMID: 17539631
Inorg Chem. 2007 Jun 25;46(13):5229-36. doi: 10.1021/ic070132u. Epub 2007 Jun 01.

A series of metal-organic hybrid compounds were synthesized using two new phosphonic acids, pyridyl-4-phosphonic acid and p-xylylenediphosphonic acid (H(2)O(3)PCH(2)C(6)H(4)CH(2)PO(3)H(2)). The phosphonic acid ligands have been synthesized from their corresponding bromides following two different types of reactions. The reaction of...

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Konar S, Zoń J, Prosvirin AV, et al. Synthesis and characterization of four metal-organophosphonates with one-, two-, and three-dimensional structures. Inorg Chem. 2007;46(13):5229-36doi: 10.1021/ic070132u.
Konar, S., Zoń, J., Prosvirin, A. V., Dunbar, K. R., & Clearfield, A. (2007). Synthesis and characterization of four metal-organophosphonates with one-, two-, and three-dimensional structures. Inorganic chemistry, 46(13), 5229-36. https://doi.org/10.1021/ic070132u
Konar, Sanjit, et al. "Synthesis and characterization of four metal-organophosphonates with one-, two-, and three-dimensional structures." Inorganic chemistry vol. 46,13 (2007): 5229-36. doi: https://doi.org/10.1021/ic070132u
Konar S, Zoń J, Prosvirin AV, Dunbar KR, Clearfield A. Synthesis and characterization of four metal-organophosphonates with one-, two-, and three-dimensional structures. Inorg Chem. 2007 Jun 25;46(13):5229-36. doi: 10.1021/ic070132u. Epub 2007 Jun 01. PMID: 17539631.
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Detection methods for highly toxic organophosphonates A literature survey.

Talanta

Smith SJ.
PMID: 18963456
Talanta. 1983 Oct;30(10):725-39. doi: 10.1016/0039-9140(83)80169-6.

A review is given of the literature on the methods available for the detection of the organophosphonate compounds known as the "nerve gases".

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Smith SJ. Detection methods for highly toxic organophosphonates A literature survey. Talanta. 1983;30(10):725-39doi: 10.1016/0039-9140(83)80169-6.
Smith, S. J. (1983). Detection methods for highly toxic organophosphonates A literature survey. Talanta, 30(10), 725-39. https://doi.org/10.1016/0039-9140(83)80169-6
Smith, S J. "Detection methods for highly toxic organophosphonates A literature survey." Talanta vol. 30,10 (1983): 725-39. doi: https://doi.org/10.1016/0039-9140(83)80169-6
Smith SJ. Detection methods for highly toxic organophosphonates A literature survey. Talanta. 1983 Oct;30(10):725-39. doi: 10.1016/0039-9140(83)80169-6. PMID: 18963456.
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Further Understanding of the Reactivity Control of Bisphosphonates to a Metal Source for Fabricating Highly Ordered Mesoporous Films.

Chemistry (Weinheim an der Bergstrasse, Germany)

Wakabayashi R, Kimura T.
PMID: 30821398
Chemistry. 2019 Apr 23;25(23):5971-5977. doi: 10.1002/chem.201900250. Epub 2019 Mar 28.

Mesoporous metal organophosphonates having embedded organic functions are a promising platform to hybridize organics and non-siliceous inorganic frameworks in their molecular scale. However, the reactivity between a bisphosphonate and a metal source is dramatically different for their combination and...

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Wakabayashi R, Kimura T. Further Understanding of the Reactivity Control of Bisphosphonates to a Metal Source for Fabricating Highly Ordered Mesoporous Films. Chemistry. 2019;25(23):5971-5977doi: 10.1002/chem.201900250.
Wakabayashi, R., & Kimura, T. (2019). Further Understanding of the Reactivity Control of Bisphosphonates to a Metal Source for Fabricating Highly Ordered Mesoporous Films. Chemistry (Weinheim an der Bergstrasse, Germany), 25(23), 5971-5977. https://doi.org/10.1002/chem.201900250
Wakabayashi, Ryutaro, and Kimura, Tatsuo. "Further Understanding of the Reactivity Control of Bisphosphonates to a Metal Source for Fabricating Highly Ordered Mesoporous Films." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 25,23 (2019): 5971-5977. doi: https://doi.org/10.1002/chem.201900250
Wakabayashi R, Kimura T. Further Understanding of the Reactivity Control of Bisphosphonates to a Metal Source for Fabricating Highly Ordered Mesoporous Films. Chemistry. 2019 Apr 23;25(23):5971-5977. doi: 10.1002/chem.201900250. Epub 2019 Mar 28. PMID: 30821398.
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Dimethyl methylphosphonate adsorption and decomposition on MoO.

Journal of physics. Condensed matter : an Institute of Physics journal

Head AR, Tsyshevsky R, Trotochaud L, Yu Y, Karslıoǧlu O, Eichhorn B, Kuklja MM, Bluhm H.
PMID: 29469812
J Phys Condens Matter. 2018 Apr 04;30(13):134005. doi: 10.1088/1361-648X/aab192. Epub 2018 Feb 22.

Organophosphonates range in their toxicity and are used as pesticides, herbicides, and chemical warfare agents (CWAs). Few laboratories are equipped to handle the most toxic molecules, thus simulants such as dimethyl methylphosphonate (DMMP), are used as a first step...

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Head AR, Tsyshevsky R, Trotochaud L, et al. Dimethyl methylphosphonate adsorption and decomposition on MoO. J Phys Condens Matter. 2018;30(13):134005doi: 10.1088/1361-648X/aab192.
Head, A. R., Tsyshevsky, R., Trotochaud, L., Yu, Y., Karslıoǧlu, O., Eichhorn, B., Kuklja, M. M., & Bluhm, H. (2018). Dimethyl methylphosphonate adsorption and decomposition on MoO. Journal of physics. Condensed matter : an Institute of Physics journal, 30(13), 134005. https://doi.org/10.1088/1361-648X/aab192
Head, Ashley R, et al. "Dimethyl methylphosphonate adsorption and decomposition on MoO." Journal of physics. Condensed matter : an Institute of Physics journal vol. 30,13 (2018): 134005. doi: https://doi.org/10.1088/1361-648X/aab192
Head AR, Tsyshevsky R, Trotochaud L, Yu Y, Karslıoǧlu O, Eichhorn B, Kuklja MM, Bluhm H. Dimethyl methylphosphonate adsorption and decomposition on MoO. J Phys Condens Matter. 2018 Apr 04;30(13):134005. doi: 10.1088/1361-648X/aab192. Epub 2018 Feb 22. PMID: 29469812.
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Mechanofluorochromic Anthryl Phosphonate/Benzoic Acid Cocrystals with a Large Blue Shift: The Role of P=O⋅⋅⋅H Interactions.

ChemPlusChem

Prusti B, Chakravarty M.
PMID: 33305906
Chempluschem. 2020 Dec;85(12):2652-2656. doi: 10.1002/cplu.202000689.

Organophosphonates have a rich and diverse chemistry, but their mechanofluorochromic features have rarely been documented. Herein, we report on cocrystals of anthranylphosphonate with (E)-4-(2-(anthracen-9-yl)vinyl)benzoic acid that exhibit reversible mechanofluorochromic properties with large blue shifts. Anisotropic grinding (or pressure of...

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Prusti B, Chakravarty M. Mechanofluorochromic Anthryl Phosphonate/Benzoic Acid Cocrystals with a Large Blue Shift: The Role of P=O⋅⋅⋅H Interactions. Chempluschem. 2020;85(12):2652-2656doi: 10.1002/cplu.202000689.
Prusti, B., & Chakravarty, M. (2020). Mechanofluorochromic Anthryl Phosphonate/Benzoic Acid Cocrystals with a Large Blue Shift: The Role of P=O⋅⋅⋅H Interactions. ChemPlusChem, 85(12), 2652-2656. https://doi.org/10.1002/cplu.202000689
Prusti, Banchhanidhi, and Chakravarty, Manab. "Mechanofluorochromic Anthryl Phosphonate/Benzoic Acid Cocrystals with a Large Blue Shift: The Role of P=O⋅⋅⋅H Interactions." ChemPlusChem vol. 85,12 (2020): 2652-2656. doi: https://doi.org/10.1002/cplu.202000689
Prusti B, Chakravarty M. Mechanofluorochromic Anthryl Phosphonate/Benzoic Acid Cocrystals with a Large Blue Shift: The Role of P=O⋅⋅⋅H Interactions. Chempluschem. 2020 Dec;85(12):2652-2656. doi: 10.1002/cplu.202000689. PMID: 33305906.
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Role of aromatic .

Dalton transactions (Cambridge, England : 2003)

Rom T, Paul AK.
PMID: 32975259
Dalton Trans. 2020 Oct 12;49(39):13618-13634. doi: 10.1039/d0dt02796k.

Four inorganic-organic hybrid silver phosphonate compounds, [Ag(C10H8N2)(H4hedp)] (1), [Ag2(C10H8N2)(H3hedp)]·2H2O (2), [C4H12N2][Ag4(H2hedp)2] (3) and [C4H12N2][Ag10(H2hedp)4(H2O)2]·2H2O (4) (H5hedp = 1-hydroxyethane-1,1-diphosphonic acid), have been prepared by virtue of the variable amine-directed hydrothermal strategy. The subsequent roles of coordinated aromatic amine (4,4'-bipyridine) and...

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Rom T, Paul AK. Role of aromatic . Dalton Trans. 2020;49(39):13618-13634doi: 10.1039/d0dt02796k.
Rom, T., & Paul, A. K. (2020). Role of aromatic . Dalton transactions (Cambridge, England : 2003), 49(39), 13618-13634. https://doi.org/10.1039/d0dt02796k
Rom, Tanmay, and Paul, Avijit Kumar. "Role of aromatic ." Dalton transactions (Cambridge, England : 2003) vol. 49,39 (2020): 13618-13634. doi: https://doi.org/10.1039/d0dt02796k
Rom T, Paul AK. Role of aromatic . Dalton Trans. 2020 Oct 12;49(39):13618-13634. doi: 10.1039/d0dt02796k. PMID: 32975259.
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Complex Structural Landscape of Titanium Organophosphonates: Isolation of Structurally Related Ti.

Inorganic chemistry

Sharma K, Antony R, Kalita AC, Gupta SK, Davis P, Murugavel R.
PMID: 29052984
Inorg Chem. 2017 Nov 06;56(21):12848-12858. doi: 10.1021/acs.inorgchem.7b01651.

[Ti(acac)

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Sharma K, Antony R, Kalita AC, et al. Complex Structural Landscape of Titanium Organophosphonates: Isolation of Structurally Related Ti. Inorg Chem. 2017;56(21):12848-12858doi: 10.1021/acs.inorgchem.7b01651.
Sharma, K., Antony, R., Kalita, A. C., Gupta, S. K., Davis, P., & Murugavel, R. (2017). Complex Structural Landscape of Titanium Organophosphonates: Isolation of Structurally Related Ti. Inorganic chemistry, 56(21), 12848-12858. https://doi.org/10.1021/acs.inorgchem.7b01651
Sharma, Kamna, et al. "Complex Structural Landscape of Titanium Organophosphonates: Isolation of Structurally Related Ti." Inorganic chemistry vol. 56,21 (2017): 12848-12858. doi: https://doi.org/10.1021/acs.inorgchem.7b01651
Sharma K, Antony R, Kalita AC, Gupta SK, Davis P, Murugavel R. Complex Structural Landscape of Titanium Organophosphonates: Isolation of Structurally Related Ti. Inorg Chem. 2017 Nov 06;56(21):12848-12858. doi: 10.1021/acs.inorgchem.7b01651. PMID: 29052984.
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Hydrophosphorylation of alkenes with dialkyl phosphites catalyzed by Mn(III) under air.

The Journal of organic chemistry

Tayama O, Nakano A, Iwahama T, Sakaguchi S, Ishii Y.
PMID: 15287806
J Org Chem. 2004 Aug 06;69(16):5494-6. doi: 10.1021/jo049657j.

A facile method for the synthesis of organophosphonates from alkenes and dialkyl phosphites was developed by the use of Mn(II) under air. Thus, the reaction of 1-octene with diethyl phosphite in the presence of Mn(OAc)2 (5 mol %) under...

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Tayama O, Nakano A, Iwahama T, et al. Hydrophosphorylation of alkenes with dialkyl phosphites catalyzed by Mn(III) under air. J Org Chem. 2004;69(16):5494-6doi: 10.1021/jo049657j.
Tayama, O., Nakano, A., Iwahama, T., Sakaguchi, S., & Ishii, Y. (2004). Hydrophosphorylation of alkenes with dialkyl phosphites catalyzed by Mn(III) under air. The Journal of organic chemistry, 69(16), 5494-6. https://doi.org/10.1021/jo049657j
Tayama, Osamu, et al. "Hydrophosphorylation of alkenes with dialkyl phosphites catalyzed by Mn(III) under air." The Journal of organic chemistry vol. 69,16 (2004): 5494-6. doi: https://doi.org/10.1021/jo049657j
Tayama O, Nakano A, Iwahama T, Sakaguchi S, Ishii Y. Hydrophosphorylation of alkenes with dialkyl phosphites catalyzed by Mn(III) under air. J Org Chem. 2004 Aug 06;69(16):5494-6. doi: 10.1021/jo049657j. PMID: 15287806.
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Efficient conversion of arylene precursors into photoluminescent phosphonates for surface modification of metal oxides.

Dalton transactions (Cambridge, England : 2003)

Keceli E, Hemgesberg M, Bay S, Wilhelm C, Sun Y, Ernst S, Müller TJ, Thiel WR.
PMID: 23340827
Dalton Trans. 2013 May 14;42(18):6344-52. doi: 10.1039/c2dt32553e.

Three highly fluorescent phosphonates have been prepared in good yields from different arylene bridged 5-iodothiophenes by following an optimized four-step procedure. The compounds have been immobilised on mesoporous zirconia, alumina and titania particles in order to probe their luminescence...

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Keceli E, Hemgesberg M, Bay S, et al. Efficient conversion of arylene precursors into photoluminescent phosphonates for surface modification of metal oxides. Dalton Trans. 2013;42(18):6344-52doi: 10.1039/c2dt32553e.
Keceli, E., Hemgesberg, M., Bay, S., Wilhelm, C., Sun, Y., Ernst, S., Müller, T. J., & Thiel, W. R. (2013). Efficient conversion of arylene precursors into photoluminescent phosphonates for surface modification of metal oxides. Dalton transactions (Cambridge, England : 2003), 42(18), 6344-52. https://doi.org/10.1039/c2dt32553e
Keceli, Ezgi, et al. "Efficient conversion of arylene precursors into photoluminescent phosphonates for surface modification of metal oxides." Dalton transactions (Cambridge, England : 2003) vol. 42,18 (2013): 6344-52. doi: https://doi.org/10.1039/c2dt32553e
Keceli E, Hemgesberg M, Bay S, Wilhelm C, Sun Y, Ernst S, Müller TJ, Thiel WR. Efficient conversion of arylene precursors into photoluminescent phosphonates for surface modification of metal oxides. Dalton Trans. 2013 May 14;42(18):6344-52. doi: 10.1039/c2dt32553e. PMID: 23340827.
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Uptake of Glyphosate by an Arthrobacter sp.

Applied and environmental microbiology

Pipke R, Schulz A, Amrhein N.
PMID: 16347356
Appl Environ Microbiol. 1987 May;53(5):974-8. doi: 10.1128/aem.53.5.974-978.1987.

The uptake of glyphosate (N-[phosphonomethyl]glycine) by an Arthrobacter sp. which can utilize this herbicide as its sole source of phosphorus was investigated. Orthophosphate suppressed the expression of the uptake system for glyphosate and also competed with glyphosate for uptake....

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Pipke R, Schulz A, Amrhein N. Uptake of Glyphosate by an Arthrobacter sp. Appl Environ Microbiol. 1987;53(5):974-8doi: 10.1128/aem.53.5.974-978.1987.
Pipke, R., Schulz, A., & Amrhein, N. (1987). Uptake of Glyphosate by an Arthrobacter sp. Applied and environmental microbiology, 53(5), 974-8. https://doi.org/10.1128/aem.53.5.974-978.1987
Pipke, R, et al. "Uptake of Glyphosate by an Arthrobacter sp." Applied and environmental microbiology vol. 53,5 (1987): 974-8. doi: https://doi.org/10.1128/aem.53.5.974-978.1987
Pipke R, Schulz A, Amrhein N. Uptake of Glyphosate by an Arthrobacter sp. Appl Environ Microbiol. 1987 May;53(5):974-8. doi: 10.1128/aem.53.5.974-978.1987. PMID: 16347356; PMCID: PMC203797.
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Dispersive solid-phase extraction for in-sorbent Fourier-transform infrared detection and identification of nerve agent simulants in analysis for verification of chemical weapon convention.

Analytical and bioanalytical chemistry

Garg P, Pardasani D, Mazumder A, Purohit A, Dubey DK.
PMID: 21058018
Anal Bioanal Chem. 2011 Jan;399(2):955-63. doi: 10.1007/s00216-010-4337-9. Epub 2010 Nov 08.

The combination of dispersive solid-phase extraction (DSPE) and Fourier-transform infrared (FTIR) spectroscopy is presented for detection and quantification of markers and simulants of nerve agents. Hydrophilic-lipophilic balance (HLB) sorbent was used for extraction and enrichment of organophosphonates from water....

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Garg P, Pardasani D, Mazumder A, et al. Dispersive solid-phase extraction for in-sorbent Fourier-transform infrared detection and identification of nerve agent simulants in analysis for verification of chemical weapon convention. Anal Bioanal Chem. 2010;399(2):955-63doi: 10.1007/s00216-010-4337-9.
Garg, P., Pardasani, D., Mazumder, A., Purohit, A., & Dubey, D. K. (2011). Dispersive solid-phase extraction for in-sorbent Fourier-transform infrared detection and identification of nerve agent simulants in analysis for verification of chemical weapon convention. Analytical and bioanalytical chemistry, 399(2), 955-63. https://doi.org/10.1007/s00216-010-4337-9
Garg, Prabhat, et al. "Dispersive solid-phase extraction for in-sorbent Fourier-transform infrared detection and identification of nerve agent simulants in analysis for verification of chemical weapon convention." Analytical and bioanalytical chemistry vol. 399,2 (2011): 955-63. doi: https://doi.org/10.1007/s00216-010-4337-9
Garg P, Pardasani D, Mazumder A, Purohit A, Dubey DK. Dispersive solid-phase extraction for in-sorbent Fourier-transform infrared detection and identification of nerve agent simulants in analysis for verification of chemical weapon convention. Anal Bioanal Chem. 2011 Jan;399(2):955-63. doi: 10.1007/s00216-010-4337-9. Epub 2010 Nov 08. PMID: 21058018.
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Nanocylindrical confinement imparts highest structural order in molecular self-assembly of organophosphonates on aluminum oxide.

Nanoscale

Pathak A, Bora A, Braunschweig B, Meltzer C, Yan H, Lemmens P, Daum W, Schwartz J, Tornow M.
PMID: 28485443
Nanoscale. 2017 May 18;9(19):6291-6295. doi: 10.1039/c7nr02420g.

We report the impact of geometrical constraint on intramolecular interactions in self-assembled monolayers (SAMs) of alkylphosphonates grown on anodically oxidized aluminum (AAO). Molecular order in these films was determined by sum frequency generation (SFG) spectroscopy, a more sensitive measure...

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Pathak A, Bora A, Braunschweig B, et al. Nanocylindrical confinement imparts highest structural order in molecular self-assembly of organophosphonates on aluminum oxide. Nanoscale. 2017;9(19):6291-6295doi: 10.1039/c7nr02420g.
Pathak, A., Bora, A., Braunschweig, B., Meltzer, C., Yan, H., Lemmens, P., Daum, W., Schwartz, J., & Tornow, M. (2017). Nanocylindrical confinement imparts highest structural order in molecular self-assembly of organophosphonates on aluminum oxide. Nanoscale, 9(19), 6291-6295. https://doi.org/10.1039/c7nr02420g
Pathak, Anshuma, et al. "Nanocylindrical confinement imparts highest structural order in molecular self-assembly of organophosphonates on aluminum oxide." Nanoscale vol. 9,19 (2017): 6291-6295. doi: https://doi.org/10.1039/c7nr02420g
Pathak A, Bora A, Braunschweig B, Meltzer C, Yan H, Lemmens P, Daum W, Schwartz J, Tornow M. Nanocylindrical confinement imparts highest structural order in molecular self-assembly of organophosphonates on aluminum oxide. Nanoscale. 2017 May 18;9(19):6291-6295. doi: 10.1039/c7nr02420g. PMID: 28485443.
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