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Showing 1 to 12 of 118 entries
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Development and validation of a liquid chromatography-mass spectrometry method for the determination of zileuton in human plasma.

Scientia pharmaceutica

Prakash K, Adiki SK, Kalakuntla RR.
PMID: 25853069
Sci Pharm. 2014 Mar 26;82(3):571-83. doi: 10.3797/scipharm.1402-19. Print 2014.

A selective and sensitive liquid chromatography-tandem mass spectrometric method (LC-MS/MS) has been developed and validated for the quantification of zileuton in human plasma. Deuterated internal standard (zileuton D4) was used as the internal standard (ISTD). Zileuton was extracted by...

Use of Methyl Tert-Butyl Ether for the Treatment of Refractory Intrahepatic Biliary Strictures and Bile Casts: A Modern Perspective.

Case reports in surgery

Kim G, Malayaman SN, Green MS.
PMID: 26236535
Case Rep Surg. 2015;2015:408175. doi: 10.1155/2015/408175. Epub 2015 Jul 07.

Cholelithiasis is a prevalent problem in the United States with 14% or more adults affected. Definitive treatment of cholelithiasis is cholecystectomy. When cholecystectomy yields minimal resolution treatment options include expectant management of asymptomatic gallstones or endoscopic retrograde cholangiopancreatogram. We...

Cometabolic biodegradation of methyl tert-butyl ether by a soil consortium: Effect of components present in gasoline.

The Journal of general and applied microbiology

Garnier PM, Auria R.
PMID: 12483594
J Gen Appl Microbiol. 2000 Apr;46(2):79-84. doi: 10.2323/jgam.46.79.

A soil consortium was tested for its ability to degrade reformulated gasoline, containing methyl tert-butyl ether (MTBE). Reformulated gasoline was rapidly degraded to completion. However, MTBE tested alone was not degraded. A screening was carried out to identify compounds...

Hydrogen storage in sH clathrate hydrates: thermodynamic model.

The journal of physical chemistry. B

Martín A, Peters CJ.
PMID: 19456175
J Phys Chem B. 2009 May 28;113(21):7558-63. doi: 10.1021/jp8074578.

A thermodynamic model of equilibrium states of structure sH clathrate hydrates of hydrogen with methyl tert-butyl ether, methyl cylohexane, or 1,1-dimethyl cyclohexane is presented. The model uses the van der Waals-Platteeuw statistical-thermodynamical model to represent the hydrates and the...

Catalysis in a porous molecular capsule: activation by regulated access to sixty metal centers spanning a truncated icosahedron.

Journal of the American Chemical Society

Kopilevich S, Gil A, Garcia-Ratés M, Bonet-Ávalos J, Bo C, Müller A, Weinstock IA.
PMID: 22765884
J Am Chem Soc. 2012 Aug 08;134(31):13082-8. doi: 10.1021/ja304513t. Epub 2012 Jul 30.

The 30 cationic {Mo(V)2O4(acetate)}(+) units linking 12 negatively charged pentagonal "ligands," {(Mo(VI))Mo(VI)5O21(H2O)6}(6-) of the porous metal-oxide capsule, [{Mo(VI)6O21(H2O)6}12{Mo(V)2O4(acetate)}30](42-) provide active sites for catalytic transformations of organic "guests". This is demonstrated using a well-behaved model reaction, the fully reversible cleavage...

High-sensitivity simultaneous liquid chromatography-tandem mass spectrometry assay of ethinyl estradiol and levonorgestrel in human plasma.

Journal of pharmaceutical analysis

Gandhi A, Guttikar S, Trivedi P.
PMID: 29403945
J Pharm Anal. 2015 Oct;5(5):316-326. doi: 10.1016/j.jpha.2015.02.002. Epub 2015 Feb 20.

A sensitive and simultaneous liquid chromatography-tandem mass spectrometry method was developed and validated for quantification of ethinyl estradiol and levonorgestrel. The analytes were extracted with methyl-tert-butyl ether: n-hexane (50:50, v/v) solvent mixture, followed by dansyl derivatization. The chromatographic separation...

Multivariate optimization of a microextraction by packed sorbent-programmed temperature vaporization-gas chromatography-tandem mass spectrometry method for organophosphate flame retardant analysis in environmental aqueous matrices.

Analytical and bioanalytical chemistry

Naccarato A, Elliani R, Sindona G, Tagarelli A.
PMID: 29032454
Anal Bioanal Chem. 2017 Dec;409(30):7105-7120. doi: 10.1007/s00216-017-0669-z. Epub 2017 Oct 14.

In this work, organophosphate ester flame retardant (OPFRs) assay in environmental waters was addressed by using microextraction by packed sorbent (MEPS) and gas chromatography-tandem mass spectrometry (GC-MS/MS). Ten OPFRs with different physicochemical properties were taken into account as target...

Systematic evaluation of supported liquid extraction in reducing matrix effect and improving extraction efficiency in LC-MS/MS based bioanalysis for 10 model pharmaceutical compounds.

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences

Jiang H, Cao H, Zhang Y, Fast DM.
PMID: 22410088
J Chromatogr B Analyt Technol Biomed Life Sci. 2012 Apr 01;891:71-80. doi: 10.1016/j.jchromb.2012.02.031. Epub 2012 Feb 23.

In past a few years, there has been a large increase in the application of supported liquid extraction (SLE) for LC-MS/MS based bioanalysis due to its distinct practical advantage in reduced time cost, ease of operation and the feasibility...

Influence of the interfacial tension on the microstructural and mechanical properties of microgels at fluid interfaces.

Journal of colloid and interface science

Vialetto J, Nussbaum N, Bergfreund J, Fischer P, Isa L.
PMID: 34774321
J Colloid Interface Sci. 2022 Feb 15;608:2584-2592. doi: 10.1016/j.jcis.2021.10.186. Epub 2021 Nov 02.

Microgels are soft colloidal particles constituted by cross-linked polymer networks with a high potential for applications. In particular, after adsorption at a fluid interface, interfacial tension provides two-dimensional (2D) confinement for microgel monolayers and drives the reconfiguration of the...

Evaluation of different stool extraction methods for metabolomics measurements in human faecal samples.

BMJ nutrition, prevention & health

Erben V, Poschet G, Schrotz-King P, Brenner H.
PMID: 35028509
BMJ Nutr Prev Health. 2021 Jul 02;4(2):374-384. doi: 10.1136/bmjnph-2020-000202. eCollection 2021.

BACKGROUND: Metabolomics analysis of human stool samples is of great interest for a broad range of applications in biomedical research including early detection of colorectal neoplasms. However, due to the complexity of metabolites there is no consensus on how...

A Validated LC-MS/MS Method for Simultaneous Quantification of Simvastatin and Simvastatin Acid in Beagle Plasma: Application to an Absolute Bioavailability Study.

Biomedical chromatography : BMC

Zhang Y, He J, Tang X, Zhang Z, Tian Y.
PMID: 34854096
Biomed Chromatogr. 2021 Dec 01;e5290. doi: 10.1002/bmc.5290. Epub 2021 Dec 01.

A highly sensitive LC-MS/MS method for simultaneous detection of both simvastatin (SV) and simvastatin acid (SVA) in beagle plasma was developed and successfully applied to an absolute bioavailability study. Lovastatin (LV) was used as internal standard (IS). The analysis...

Fatty Acid Composition of the Lipids from Atlantic Salmon-Comparison of Two Extraction Methods without Halogenated Solvents.

Foods (Basel, Switzerland)

Nechev JT, Edvinsen GK, Eilertsen KE.
PMID: 33401472
Foods. 2021 Jan 01;10(1). doi: 10.3390/foods10010073.

The scope of this paper was to apply two recently developed methods for lipid extraction: the methyl tert-butyl ether (MTBE) method and the BUME method. These two methods do not include halogenated solvents, which makes them less hazardous to...

Showing 1 to 12 of 118 entries