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Acta Crystallogr C. 2000 Sep;56:1126-8. doi: 10.1107/s010827010000771x.

Threefold interweaving of (4,4) nets built from R(10)10(58) rings inthe hydrogen-bonded adduct 1,4-diazabicyclo.

Acta crystallographica. Section C, Crystal structure communications

Burchell, Ferguson, Lough, Glidewell

Affiliations

  1. School of Chemistry, University of St Andrews, St Andrews, Fife KY16 9ST, Scotland.

PMID: 10986506 DOI: 10.1107/s010827010000771x

Abstract

The 1:1 adduct of 1,4-diazabicyclo[2.2.2]octane and 5-hydroxyisophthalic acid is a salt, [H(C(6)H(12)N(2))](+). [HOC(6)H(3)(COOH)COO](-) or C(6)H(13)N(2)(+).C(8)H(5)O(5)(-). The ions are linked by three types of hydrogen bond, i.e. N-H.O, O-H.O and O-H.N, into continuous two-dimensional (4,4) nets built from a single type of R(10)(10)(58) ring. Six independent sheets of this type make up the structure and these are interwoven in sets of three.

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