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Braga D, Maini L, Polito M, et al. Mechanochemical assembly of hydrogen bonded organic-organometallic solid compounds. Chem Commun (Camb). 2002;(24):2960-1doi: 10.1039/b209861j.
Braga, D., Maini, L., Polito, M., Mirolo, L., & Grepioni, F. (2002). Mechanochemical assembly of hydrogen bonded organic-organometallic solid compounds. Chemical communications (Cambridge, England), (24), 2960-1. https://doi.org/10.1039/b209861j
Braga, Dario, et al. "Mechanochemical assembly of hydrogen bonded organic-organometallic solid compounds." Chemical communications (Cambridge, England) vol. ,24 (2002): 2960-1. doi: https://doi.org/10.1039/b209861j
Braga D, Maini L, Polito M, Mirolo L, Grepioni F. Mechanochemical assembly of hydrogen bonded organic-organometallic solid compounds. Chem Commun (Camb). 2002 Dec 21;(24):2960-1. doi: 10.1039/b209861j. PMID: 12536766.
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Chem Commun (Camb). 2002 Dec 21;(24):2960-1. doi: 10.1039/b209861j.

Mechanochemical assembly of hydrogen bonded organic-organometallic solid compounds.

Chemical communications (Cambridge, England)

Dario Braga, Lucia Maini, Marco Polito, Laurent Mirolo, Fabrizia Grepioni

Affiliations

  1. Dipartimento di Chimica G. Ciamician, Università di Bologna, Via Selmi 2, 40126 Bologna, Italy. [email protected]

PMID: 12536766 DOI: 10.1039/b209861j

Abstract

Solvent-free reactions with molecular systems have been exploited to prepare hybrid organic-organometallic solids: grinding of the complex [Fe(eta 5-C5H4COOH)2] with solid bases B generates quantitatively the corresponding hydrogen bonded salts [Fe(eta 5-C5H4COOH)(eta 5-C5H4COO)][HB] (B = 1,4-diazabicyclo[2.2.2]octane, 1,4-phenylenediamine); gas-solid reactions are also possible with volatile bases.

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