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Katime I, Arellano J, Schulz P. Poly(n-hexyl methacrylate) polymerization in three-component microemulsion stabilized by a cationic surfactant. J Colloid Interface Sci. 2005;296(2):490-5doi: 10.1016/j.jcis.2005.09.027.
Katime, I., Arellano, J., & Schulz, P. (2006). Poly(n-hexyl methacrylate) polymerization in three-component microemulsion stabilized by a cationic surfactant. Journal of colloid and interface science, 296(2), 490-5. https://doi.org/10.1016/j.jcis.2005.09.027
Katime, Issa, et al. "Poly(n-hexyl methacrylate) polymerization in three-component microemulsion stabilized by a cationic surfactant." Journal of colloid and interface science vol. 296,2 (2006): 490-5. doi: https://doi.org/10.1016/j.jcis.2005.09.027
Katime I, Arellano J, Schulz P. Poly(n-hexyl methacrylate) polymerization in three-component microemulsion stabilized by a cationic surfactant. J Colloid Interface Sci. 2006 Apr 15;296(2):490-5. doi: 10.1016/j.jcis.2005.09.027. Epub 2005 Oct 17. PMID: 16236300.
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J Colloid Interface Sci. 2006 Apr 15;296(2):490-5. doi: 10.1016/j.jcis.2005.09.027. Epub 2005 Oct 17.

Poly(n-hexyl methacrylate) polymerization in three-component microemulsion stabilized by a cationic surfactant.

Journal of colloid and interface science

Issa Katime, Jesús Arellano, Pablo Schulz

Affiliations

  1. Grupo de Nuevos Materiales, Departamento de Química Física, Facultad de Ciencias, Campus de Leioa, Universidad del País Vasco, Apartado 644, Bilbao, Spain.

PMID: 16236300 DOI: 10.1016/j.jcis.2005.09.027

Abstract

The polymerization of n-hexyl methacrylate (n-HMA) in three-component microemulsion stabilized with dodecyltrimethylammonium bromide (DTAB) is reported as a function of monomer and initiator concentrations and temperature. The obtained latices were bluish, transparent, and translucent. Particle sizes and molar masses were on the order of 20 nm and 3 x 10(6) g/mol, respectively. In all cases, high reaction rates and final conversions of 98% were obtained. Polymerization temperature has a strong effect on reaction rate and conversion.

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