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Glazar L, Radisek M, Segedin P, et al. Di-mu-formato-1kappa2O:2kappa2O'-di-mu-pyridin-2-olato-1kappaO:2kappaN;1kappaN:2kappaO-bis[(2-pyridone-kappaO)copper(II)] acetonitrile 1.02-solvate. Acta Crystallogr C. 2005;61:m526-8doi: 10.1107/S0108270105033871.
Glazar, L., Radisek, M., Segedin, P., & Golobic, A. (2005). Di-mu-formato-1kappa2O:2kappa2O'-di-mu-pyridin-2-olato-1kappaO:2kappaN;1kappaN:2kappaO-bis[(2-pyridone-kappaO)copper(II)] acetonitrile 1.02-solvate. Acta crystallographica. Section C, Crystal structure communications, 61m526-8. https://doi.org/10.1107/S0108270105033871
Glazar, Lea, et al. "Di-mu-formato-1kappa2O:2kappa2O'-di-mu-pyridin-2-olato-1kappaO:2kappaN;1kappaN:2kappaO-bis[(2-pyridone-kappaO)copper(II)] acetonitrile 1.02-solvate." Acta crystallographica. Section C, Crystal structure communications vol. 61 (2005): m526-8. doi: https://doi.org/10.1107/S0108270105033871
Glazar L, Radisek M, Segedin P, Golobic A. Di-mu-formato-1kappa2O:2kappa2O'-di-mu-pyridin-2-olato-1kappaO:2kappaN;1kappaN:2kappaO-bis[(2-pyridone-kappaO)copper(II)] acetonitrile 1.02-solvate. Acta Crystallogr C. 2005 Dec;61:m526-8. doi: 10.1107/S0108270105033871. Epub 2005 Nov 19. PMID: 16330838.
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Acta Crystallogr C. 2005 Dec;61:m526-8. doi: 10.1107/S0108270105033871. Epub 2005 Nov 19.

Di-mu-formato-1kappa2O:2kappa2O'-di-mu-pyridin-2-olato-1kappaO:2kappaN;1kappaN:2kappaO-bis[(2-pyridone-kappaO)copper(II)] acetonitrile 1.02-solvate.

Acta crystallographica. Section C, Crystal structure communications

Lea Glazar, Marjeta Radisek, Primoz Segedin, Amalija Golobic

Affiliations

  1. University of Ljubljana, Faculty of Chemistry and Chemical Technology, Askerceva 5, 1000 Ljubljana, Slovenia.

PMID: 16330838 DOI: 10.1107/S0108270105033871

Abstract

In the title compound, [Cu2(CHO2)2(C5H4NO)2(C5H5NO)2].1.02CH3CN, the dimeric unit is centrosymmetric, with two bidentate pyridin-2-olate and two bidentate formate syn-syn bridges, and two apical 2-pyridone ligands coordinated through the O atoms. The N atom from the apical 2-pyridone ligand is a donor of a hydrogen bond to the O atom of the bridging pyridinolate ligand of the same complex. The coordination polyhedron of the Cu atom is a distorted square pyramid.

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