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Tkachenko BA, Fokina NA, Chernish LV, et al. Functionalized nanodiamonds part 3: thiolation of tertiary/bridgehead alcohols. Org Lett. 2006;8(9):1767-70doi: 10.1021/ol053136g.
Tkachenko, B. A., Fokina, N. A., Chernish, L. V., Dahl, J. E., Liu, S., Carlson, R. M., Fokin, A. A., & Schreiner, P. R. (2006). Functionalized nanodiamonds part 3: thiolation of tertiary/bridgehead alcohols. Organic letters, 8(9), 1767-70. https://doi.org/10.1021/ol053136g
Tkachenko, Boryslav A, et al. "Functionalized nanodiamonds part 3: thiolation of tertiary/bridgehead alcohols." Organic letters vol. 8,9 (2006): 1767-70. doi: https://doi.org/10.1021/ol053136g
Tkachenko BA, Fokina NA, Chernish LV, Dahl JE, Liu S, Carlson RM, Fokin AA, Schreiner PR. Functionalized nanodiamonds part 3: thiolation of tertiary/bridgehead alcohols. Org Lett. 2006 Apr 27;8(9):1767-70. doi: 10.1021/ol053136g. PMID: 16623546.
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Org Lett. 2006 Apr 27;8(9):1767-70. doi: 10.1021/ol053136g.

Functionalized nanodiamonds part 3: thiolation of tertiary/bridgehead alcohols.

Organic letters

Boryslav A Tkachenko, Natalie A Fokina, Lesya V Chernish, Jeremy E P Dahl, Shenggao Liu, Robert M K Carlson, Andrey A Fokin, Peter R Schreiner

Affiliations

  1. Institut für Organische Chemie, Justus-Liebig University, Heinrich-Buff-Ring 58, D-35392 Giessen, Germany.

PMID: 16623546 DOI: 10.1021/ol053136g

Abstract

[reaction: see text] Treatment of acyclic as well as polycyclic tertiary mono- and dihydroxy hydrocarbon derivatives with thiourea in the presence of hydrobromic and acetic acid represents a convenient one-step route to the respective tertiary thiols and dithiols. This procedure was used for the preparation of diamondoid thiols of diamantane, triamantane, [121]tetramantane, and others that are prospective nanoelectronic materials.

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