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Marchione AA, Buck RC. Complete multinuclear magnetic resonance characterization of a set of polyfluorinated acids and alcohols. Magn Reson Chem. 2009;47(2):194-8doi: 10.1002/mrc.2376.
Marchione, A. A., & Buck, R. C. (2009). Complete multinuclear magnetic resonance characterization of a set of polyfluorinated acids and alcohols. Magnetic resonance in chemistry : MRC, 47(2), 194-8. https://doi.org/10.1002/mrc.2376
Marchione, Alexander A, and Buck, Robert C. "Complete multinuclear magnetic resonance characterization of a set of polyfluorinated acids and alcohols." Magnetic resonance in chemistry : MRC vol. 47,2 (2009): 194-8. doi: https://doi.org/10.1002/mrc.2376
Marchione AA, Buck RC. Complete multinuclear magnetic resonance characterization of a set of polyfluorinated acids and alcohols. Magn Reson Chem. 2009 Feb;47(2):194-8. doi: 10.1002/mrc.2376. PMID: 19025971.
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Magn Reson Chem. 2009 Feb;47(2):194-8. doi: 10.1002/mrc.2376.

Complete multinuclear magnetic resonance characterization of a set of polyfluorinated acids and alcohols.

Magnetic resonance in chemistry : MRC

Alexander A Marchione, Robert C Buck

Affiliations

  1. DuPont Central Research and Development, Experimental Station, Wilmington, DE 19880, USA. [email protected]

PMID: 19025971 DOI: 10.1002/mrc.2376

Abstract

A complete (1)H, (19)F, and (13)C NMR assignment of a homologous series of polyfluorinated acids and alcohols is reported. These assignments were obtained chiefly through single and multiple-bond (1)H-(13)C and (19)F-(13)C correlation experiments (HSQC, HMBC). (19)F NOESY experiments were required for assignment of two compounds with diastereotopic (19)F nuclei in the CF(2)chain of the molecule.

2008 John Wiley & Sons, Ltd.

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