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Grignard B, Calberg C, Jérôme C, et al. Supported ATRP of fluorinated methacrylates in supercritical carbon dioxide: preparation of scCO2 soluble polymers with low catalytic residues. Chem Commun (Camb). 2008;(44):5803-5doi: 10.1039/b812297k.
Grignard, B., Calberg, C., Jérôme, C., Wang, W., Howdle, S., & Detrembleur, C. (2008). Supported ATRP of fluorinated methacrylates in supercritical carbon dioxide: preparation of scCO2 soluble polymers with low catalytic residues. Chemical communications (Cambridge, England), (44), 5803-5. https://doi.org/10.1039/b812297k
Grignard, Bruno, et al. "Supported ATRP of fluorinated methacrylates in supercritical carbon dioxide: preparation of scCO2 soluble polymers with low catalytic residues." Chemical communications (Cambridge, England) vol. ,44 (2008): 5803-5. doi: https://doi.org/10.1039/b812297k
Grignard B, Calberg C, Jérôme C, Wang W, Howdle S, Detrembleur C. Supported ATRP of fluorinated methacrylates in supercritical carbon dioxide: preparation of scCO2 soluble polymers with low catalytic residues. Chem Commun (Camb). 2008 Nov 30;(44):5803-5. doi: 10.1039/b812297k. Epub 2008 Oct 01. PMID: 19009087.
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Chem Commun (Camb). 2008 Nov 30;(44):5803-5. doi: 10.1039/b812297k. Epub 2008 Oct 01.

Supported ATRP of fluorinated methacrylates in supercritical carbon dioxide: preparation of scCO2 soluble polymers with low catalytic residues.

Chemical communications (Cambridge, England)

Bruno Grignard, Cédric Calberg, Christine Jérôme, Wenxin Wang, Steven Howdle, Christophe Detrembleur

Affiliations

  1. Center for Education and Research on Macromolecules, University of Liège, Sart-Tilman, B6a, B-4000, Liège, Belgium.

PMID: 19009087 DOI: 10.1039/b812297k

Abstract

Synthesis of poly(2,2,2-trifluoroethyl methacrylate) by supported ATRP was investigated in supercritical carbon dioxide using a copper salt ligated to a polymeric ligand immobilised onto silica; after polymerisation, fluorinated polymers with well defined molecular weight and low polydispersity were obtained.

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