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Calderon Moreno JM, Pol VG, Suh SH, et al. Autogenic synthesis of green- and red-emitting single-phase Pr(2)O(2)CO(3) and PrO(1.833) luminescent nanopowders. Inorg Chem. 2010;49(21):10067-73doi: 10.1021/ic101414x.
Calderon Moreno, J. M., Pol, V. G., Suh, S. H., & Popa, M. (2010). Autogenic synthesis of green- and red-emitting single-phase Pr(2)O(2)CO(3) and PrO(1.833) luminescent nanopowders. Inorganic chemistry, 49(21), 10067-73. https://doi.org/10.1021/ic101414x
Calderon Moreno, Jose M, et al. "Autogenic synthesis of green- and red-emitting single-phase Pr(2)O(2)CO(3) and PrO(1.833) luminescent nanopowders." Inorganic chemistry vol. 49,21 (2010): 10067-73. doi: https://doi.org/10.1021/ic101414x
Calderon Moreno JM, Pol VG, Suh SH, Popa M. Autogenic synthesis of green- and red-emitting single-phase Pr(2)O(2)CO(3) and PrO(1.833) luminescent nanopowders. Inorg Chem. 2010 Nov 01;49(21):10067-73. doi: 10.1021/ic101414x. PMID: 20923161.
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Inorg Chem. 2010 Nov 01;49(21):10067-73. doi: 10.1021/ic101414x.

Autogenic synthesis of green- and red-emitting single-phase Pr(2)O(2)CO(3) and PrO(1.833) luminescent nanopowders.

Inorganic chemistry

Jose M Calderon Moreno, Vilas G Pol, Soong-Hyuck Suh, Monica Popa

Affiliations

  1. Institute of Physical Chemistry Ilie Murgulescu, Romanian Academy, Splaiul Independentei 202, Bucharest 060021, Romania. [email protected]

PMID: 20923161 DOI: 10.1021/ic101414x

Abstract

This Article reveals a rare synthesis of pure Pr(2)O(2)CO(3) (POC) nanopowder by thermolysis (700 °C) of a single chemical precursor in an autogenic reaction. The autogenic thermolysis of praseodymium acetate is a solvent-free, efficient, and straightforward approach yielding luminescent POC nanoparticles. The as-prepared POC nanopowder converted to PrO(1.833) (PO) powder via combustion. Methodical morphological, structural, and compositional characterizations of POC and PO powders are carried out, supported by mechanistic elucidation and the photoluminescent properties.

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