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Osyanin VA, Ivleva EA, Rybakov VB, et al. 2-(4-Meth-oxy-phen-yl)-4H-1,3,2-benzoxathia-phosphinine 2-sulfide. Acta Crystallogr Sect E Struct Rep Online. 2011;67:o388-9doi: 10.1107/S1600536810053146.
Osyanin, V. A., Ivleva, E. A., Rybakov, V. B., & Klimochkin, Y. N. (2011). 2-(4-Meth-oxy-phen-yl)-4H-1,3,2-benzoxathia-phosphinine 2-sulfide. Acta crystallographica. Section E, Structure reports online, 67o388-9. https://doi.org/10.1107/S1600536810053146
Osyanin, Vitaly A, et al. "2-(4-Meth-oxy-phen-yl)-4H-1,3,2-benzoxathia-phosphinine 2-sulfide." Acta crystallographica. Section E, Structure reports online vol. 67 (2011): o388-9. doi: https://doi.org/10.1107/S1600536810053146
Osyanin VA, Ivleva EA, Rybakov VB, Klimochkin YN. 2-(4-Meth-oxy-phen-yl)-4H-1,3,2-benzoxathia-phosphinine 2-sulfide. Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 15;67:o388-9. doi: 10.1107/S1600536810053146. PMID: 21523063; PMCID: PMC3051562.
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Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 15;67:o388-9. doi: 10.1107/S1600536810053146.

2-(4-Meth-oxy-phen-yl)-4H-1,3,2-benzoxathia-phosphinine 2-sulfide.

Acta crystallographica. Section E, Structure reports online

Vitaly A Osyanin, Elena A Ivleva, Victor B Rybakov, Yurij N Klimochkin

PMID: 21523063 PMCID: PMC3051562 DOI: 10.1107/S1600536810053146

Abstract

The asymmetric unit of the title compound, C(14)H(13)O(2)PS(2), contains two crystallographically independent mol-ecules, which differ in the conformation of the 1,3,2-benzoxathia-phosphinine moieties (screw boat in the first mol-ecule and envelope in the second mol-ecule). In the crystal, neither classical nor non-classical hydrogen bonds are found. Weak inter-actions (about 2.9-3.0 Å) between the lone pair of the terminal S atoms with H atoms occur. This compound was further characterized by (1)H NMR and IR spectroscopy.

References

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