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de Souza MV, Pinheiro AC, Tiekink ER, et al. Benzyl N-{(1S)-2-hy-droxy-1-[N'-(2-nitro-benzyl-idene)hydrazinylcarbon-yl]eth-yl}carbamate. Acta Crystallogr Sect E Struct Rep Online. 2010;66:o2023-4doi: 10.1107/S1600536810027273.
de Souza, M. V., Pinheiro, A. C., Tiekink, E. R., Wardell, S. M., & Wardell, J. L. (2010). Benzyl N-{(1S)-2-hy-droxy-1-[N'-(2-nitro-benzyl-idene)hydrazinylcarbon-yl]eth-yl}carbamate. Acta crystallographica. Section E, Structure reports online, 66o2023-4. https://doi.org/10.1107/S1600536810027273
de Souza, Marcus V N, et al. "Benzyl N-{(1S)-2-hy-droxy-1-[N'-(2-nitro-benzyl-idene)hydrazinylcarbon-yl]eth-yl}carbamate." Acta crystallographica. Section E, Structure reports online vol. 66 (2010): o2023-4. doi: https://doi.org/10.1107/S1600536810027273
de Souza MV, Pinheiro AC, Tiekink ER, Wardell SM, Wardell JL. Benzyl N-{(1S)-2-hy-droxy-1-[N'-(2-nitro-benzyl-idene)hydrazinylcarbon-yl]eth-yl}carbamate. Acta Crystallogr Sect E Struct Rep Online. 2010 Jul 14;66:o2023-4. doi: 10.1107/S1600536810027273. PMID: 21588334; PMCID: PMC3007287.
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Acta Crystallogr Sect E Struct Rep Online. 2010 Jul 14;66:o2023-4. doi: 10.1107/S1600536810027273.

Benzyl N-{(1S)-2-hy-droxy-1-[N'-(2-nitro-benzyl-idene)hydrazinylcarbon-yl]eth-yl}carbamate.

Acta crystallographica. Section E, Structure reports online

Marcus V N de Souza, Alessandra C Pinheiro, Edward R T Tiekink, Solange M S V Wardell, James L Wardell

PMID: 21588334 PMCID: PMC3007287 DOI: 10.1107/S1600536810027273

Abstract

The carbamate and hydrazone groups in the title compound, C(18)H(18)N(4)O(6), are approximately orthogonal [dihedral angle = 83.3 (4)°], and the carbonyl groups are effectively anti [O=C⋯C=O torsion angle = -116.2 (7)°]. The conformation about the imine bond [1.295 (11) Å] is E. The crystal packing is dominated by O-H⋯O and N-H⋯O hydrogen bonding, which leads to two-dimensional arrays in the ab plane.

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