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Dai J, Yang J. (2,2'-Bipyridine-κN,N')bis-(4-hydroxy-benzoato-κO,O')lead(II) monohydrate. Acta Crystallogr Sect E Struct Rep Online. 2010;66:m237doi: 10.1107/S1600536810002941.
Dai, J., & Yang, J. (2010). (2,2'-Bipyridine-κN,N')bis-(4-hydroxy-benzoato-κO,O')lead(II) monohydrate. Acta crystallographica. Section E, Structure reports online, 66m237. https://doi.org/10.1107/S1600536810002941
Dai, Jun, and Yang, Juan. "(2,2'-Bipyridine-κN,N')bis-(4-hydroxy-benzoato-κO,O')lead(II) monohydrate." Acta crystallographica. Section E, Structure reports online vol. 66 (2010): m237. doi: https://doi.org/10.1107/S1600536810002941
Dai J, Yang J. (2,2'-Bipyridine-κN,N')bis-(4-hydroxy-benzoato-κO,O')lead(II) monohydrate. Acta Crystallogr Sect E Struct Rep Online. 2010 Jan 30;66:m237. doi: 10.1107/S1600536810002941. PMID: 21579690; PMCID: PMC2979701.
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Acta Crystallogr Sect E Struct Rep Online. 2010 Jan 30;66:m237. doi: 10.1107/S1600536810002941.

(2,2'-Bipyridine-κN,N')bis-(4-hydroxy-benzoato-κO,O')lead(II) monohydrate.

Acta crystallographica. Section E, Structure reports online

Jun Dai, Juan Yang

PMID: 21579690 PMCID: PMC2979701 DOI: 10.1107/S1600536810002941

Abstract

The reaction of lead acetate, 4-hydroxy-benzoic acid and 2,2'-bipyridine in aqueous solution gave the title complex, [Pb(C(7)H(5)O(3))(2)(C(10)H(8)N(2))]·H(2)O. The asymmetric unit contains one Pb(II) atom, two 4-hydroxy-benzoate ligands, one 2,2'-bipyridine ligand and one uncoordinated water mol-ecule. The Pb(II) atom is hexa-coordinated in a distorted tetra-gonal-bipyramidal geometry and is chelated by four carboxyl-ate O atoms and two N atoms. O-H⋯O hydrogen-bonding inter-actions, involving the uncoordinated water, the carboxyl-ate O atoms and hydr-oxy O atoms, produce a three-dimensional supra-molecular structure.

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