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Shahani T, Fun HK, Ragavan RV, et al. Tert-butyl 3-oxo-2,3,4,5,6,7-hexa-hydro-1H-pyrazolo[4,3-c]pyridine-5-carboxyl-ate. Acta Crystallogr Sect E Struct Rep Online. 2009;66:o142-3doi: 10.1107/S1600536809053021.
Shahani, T., Fun, H. K., Ragavan, R. V., Vijayakumar, V., & Sarveswari, S. (2009). Tert-butyl 3-oxo-2,3,4,5,6,7-hexa-hydro-1H-pyrazolo[4,3-c]pyridine-5-carboxyl-ate. Acta crystallographica. Section E, Structure reports online, 66o142-3. https://doi.org/10.1107/S1600536809053021
Shahani, Tara, et al. "Tert-butyl 3-oxo-2,3,4,5,6,7-hexa-hydro-1H-pyrazolo[4,3-c]pyridine-5-carboxyl-ate." Acta crystallographica. Section E, Structure reports online vol. 66 (2009): o142-3. doi: https://doi.org/10.1107/S1600536809053021
Shahani T, Fun HK, Ragavan RV, Vijayakumar V, Sarveswari S. Tert-butyl 3-oxo-2,3,4,5,6,7-hexa-hydro-1H-pyrazolo[4,3-c]pyridine-5-carboxyl-ate. Acta Crystallogr Sect E Struct Rep Online. 2009 Dec 16;66:o142-3. doi: 10.1107/S1600536809053021. PMID: 21580034; PMCID: PMC2980051.
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Acta Crystallogr Sect E Struct Rep Online. 2009 Dec 16;66:o142-3. doi: 10.1107/S1600536809053021.

Tert-butyl 3-oxo-2,3,4,5,6,7-hexa-hydro-1H-pyrazolo[4,3-c]pyridine-5-carboxyl-ate.

Acta crystallographica. Section E, Structure reports online

Tara Shahani, Hoong-Kun Fun, R Venkat Ragavan, V Vijayakumar, S Sarveswari

PMID: 21580034 PMCID: PMC2980051 DOI: 10.1107/S1600536809053021

Abstract

In the title compound, C(11)H(17)N(3)O(3), the pyrazole ring is approximately planar, with a maximum deviation of 0.005 (2) Å, and forms a dihedral angle of 5.69 (13)° with the plane through the six atoms of the piperidine ring. In the crystal, pairs of inter-molecular N-H⋯O hydrogen bonds form dimers with neighbouring mol-ecules, generating R(2) (2)(8) ring motifs. These dimers are further linked into two-dimensional arrays parallel to the bc plane by inter-molecular N-H⋯O and C-H⋯O hydrogen bonds.

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