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El Ashry el SH, Amer MR, Shah MR, et al. 2-Hydroxy-ethyl 2-(2,4-dichloro-anilino)-4,4-dimethyl-6-oxocyclo-hex-1-ene-carbo-dithio-ate. Acta Crystallogr Sect E Struct Rep Online. 2009;65:o602doi: 10.1107/S1600536809006199.
El Ashry, e. l. . S. H., Amer, M. R., Shah, M. R., & Ng, S. W. (2009). 2-Hydroxy-ethyl 2-(2,4-dichloro-anilino)-4,4-dimethyl-6-oxocyclo-hex-1-ene-carbo-dithio-ate. Acta crystallographica. Section E, Structure reports online, 65o602. https://doi.org/10.1107/S1600536809006199
El Ashry, El Sayed H, et al. "2-Hydroxy-ethyl 2-(2,4-dichloro-anilino)-4,4-dimethyl-6-oxocyclo-hex-1-ene-carbo-dithio-ate." Acta crystallographica. Section E, Structure reports online vol. 65 (2009): o602. doi: https://doi.org/10.1107/S1600536809006199
El Ashry el SH, Amer MR, Shah MR, Ng SW. 2-Hydroxy-ethyl 2-(2,4-dichloro-anilino)-4,4-dimethyl-6-oxocyclo-hex-1-ene-carbo-dithio-ate. Acta Crystallogr Sect E Struct Rep Online. 2009 Feb 25;65:o602. doi: 10.1107/S1600536809006199. PMID: 21582256; PMCID: PMC2968539.
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Acta Crystallogr Sect E Struct Rep Online. 2009 Feb 25;65:o602. doi: 10.1107/S1600536809006199.

2-Hydroxy-ethyl 2-(2,4-dichloro-anilino)-4,4-dimethyl-6-oxocyclo-hex-1-ene-carbo-dithio-ate.

Acta crystallographica. Section E, Structure reports online

El Sayed H El Ashry, Mohammed R Amer, M Raza Shah, Seik Weng Ng

PMID: 21582256 PMCID: PMC2968539 DOI: 10.1107/S1600536809006199

Abstract

The six-membered cyclo-hexene ring in the title compound, C(17)H(19)Cl(2)NOS(2), adopts an envelope conformation, with the C atom bearing the two methyl groups representing the flap. This atom deviates by 0.716 (3) Å from the plane passing through the other five atoms of the ring (r.m.s. deviation = 0.072 Å). The mol-ecular conformation is stabilized by an intra-molecular N-H⋯S hydrogen bond. The hydr-oxy group engages in inter-molecular O-H⋯O hydrogen bonding with adjacent acceptor atoms to generate a zigzag chain running along the c axis.

References

  1. Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22 - PubMed
  2. Acta Crystallogr Sect E Struct Rep Online. 2009 Feb 25;65(Pt 3):o597 - PubMed

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