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Kianpour G, Salavati-Niasari M, Emadi H. Sonochemical synthesis and characterization of NiMoO4 nanorods. Ultrason Sonochem. 2012;20(1):418-24doi: 10.1016/j.ultsonch.2012.08.012.
Kianpour, G., Salavati-Niasari, M., & Emadi, H. (2013). Sonochemical synthesis and characterization of NiMoO4 nanorods. Ultrasonics sonochemistry, 20(1), 418-24. https://doi.org/10.1016/j.ultsonch.2012.08.012
Kianpour, Ghazal, et al. "Sonochemical synthesis and characterization of NiMoO4 nanorods." Ultrasonics sonochemistry vol. 20,1 (2013): 418-24. doi: https://doi.org/10.1016/j.ultsonch.2012.08.012
Kianpour G, Salavati-Niasari M, Emadi H. Sonochemical synthesis and characterization of NiMoO4 nanorods. Ultrason Sonochem. 2013 Jan;20(1):418-24. doi: 10.1016/j.ultsonch.2012.08.012. Epub 2012 Aug 29. PMID: 22998810.
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Ultrason Sonochem. 2013 Jan;20(1):418-24. doi: 10.1016/j.ultsonch.2012.08.012. Epub 2012 Aug 29.

Sonochemical synthesis and characterization of NiMoO4 nanorods.

Ultrasonics sonochemistry

Ghazal Kianpour, Masoud Salavati-Niasari, Hamid Emadi

Affiliations

  1. Institute of Nano Science and Nano Technology, University of Kashan, Kashan, PO Box 87317-51167, Islamic Republic of Iran.

PMID: 22998810 DOI: 10.1016/j.ultsonch.2012.08.012

Abstract

NiMoO(4) nanorods have been successfully synthesized by sonochemical method process by using Ni(CH(3)COO)(2) · 4H(2)O and (NH(4))(6)Mo(7)O(24) · 4H(2)O as starting materials. Some parameters including ultrasonic power, ultrasonic irradiation time, stirring effect, solvent effect, and surfactant effect were investigated to reach optimum condition. The as synthesized nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmittance electron microscopy (TEM), photoluminescence (PL) spectroscopy, Fourier transform infrared (FT-IR) spectra and energy dispersive X-ray microanalysis (EDX). Facile preparation and separation are important features of this route. This work has provided a general, simple, and effective method to control the composition and morphology of NiMoO(4) in aqueous solution, which will be important for inorganic synthesis methodology.

Copyright © 2012 Elsevier B.V. All rights reserved.

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