Display options
Cite
Akkurt M, Mague JT, Mohamed SK, et al. Bis(2-amino-5-benzyl-3-eth-oxy-carbonyl-4,5,6,7-tetra-hydro-thieno[3,2-c]pyridin-5-ium) bis-(4-meth-oxy-phen-yl)di-phos-phon-ate. Acta Crystallogr Sect E Struct Rep Online. 2014;70:o348-9doi: 10.1107/S1600536814003766.
Akkurt, M., Mague, J. T., Mohamed, S. K., Younes, S. H., & Albayati, M. R. (2014). Bis(2-amino-5-benzyl-3-eth-oxy-carbonyl-4,5,6,7-tetra-hydro-thieno[3,2-c]pyridin-5-ium) bis-(4-meth-oxy-phen-yl)di-phos-phon-ate. Acta crystallographica. Section E, Structure reports online, 70o348-9. https://doi.org/10.1107/S1600536814003766
Akkurt, Mehmet, et al. "Bis(2-amino-5-benzyl-3-eth-oxy-carbonyl-4,5,6,7-tetra-hydro-thieno[3,2-c]pyridin-5-ium) bis-(4-meth-oxy-phen-yl)di-phos-phon-ate." Acta crystallographica. Section E, Structure reports online vol. 70 (2014): o348-9. doi: https://doi.org/10.1107/S1600536814003766
Akkurt M, Mague JT, Mohamed SK, Younes SH, Albayati MR. Bis(2-amino-5-benzyl-3-eth-oxy-carbonyl-4,5,6,7-tetra-hydro-thieno[3,2-c]pyridin-5-ium) bis-(4-meth-oxy-phen-yl)di-phos-phon-ate. Acta Crystallogr Sect E Struct Rep Online. 2014 Feb 22;70:o348-9. doi: 10.1107/S1600536814003766. eCollection 2014 Mar 01. PMID: 24765038; PMCID: PMC3998403.
Copy Download .nbib Format: NLM
Share it on

Acta Crystallogr Sect E Struct Rep Online. 2014 Feb 22;70:o348-9. doi: 10.1107/S1600536814003766. eCollection 2014 Mar 01.

Bis(2-amino-5-benzyl-3-eth-oxy-carbonyl-4,5,6,7-tetra-hydro-thieno[3,2-c]pyridin-5-ium) bis-(4-meth-oxy-phen-yl)di-phos-phon-ate.

Acta crystallographica. Section E, Structure reports online

Mehmet Akkurt, Joel T Mague, Shaaban K Mohamed, Sabry H H Younes, Mustafa R Albayati

Affiliations

  1. Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, Turkey.
  2. Department of Chemistry, Tulane University, New Orleans, LA 70118, USA.
  3. Chemistry and Environmental Division, Manchester Metropolitan University, Manchester M1 5GD, England ; Chemistry Department, Faculty of Science, Mini University, 61519 El-Minia, Egypt.
  4. Department of Chemistry, Faculty of Science, Sohag University, 82524 Sohag, Egypt.
  5. Kirkuk University, College of Science, Department of Chemistry, Kirkuk, Iraq.

PMID: 24765038 PMCID: PMC3998403 DOI: 10.1107/S1600536814003766

Abstract

The asymmetric unit of the title salt, 2C17H21N2O2S(+)·C14H14O7P2 (2-), contains half of a centrosymmetric bis-(4-meth-oxy-phen-yl)di-phospho-nate anion and one 2-amino-5-benzyl-3-eth-oxy-carbonyl-4,5,6,7-tetra-hydro-thieno[3,2-c]pyri-din-5-ium cation. In the anion, the O atoms of the di-phospho-nate group are disordered over two positions with equal occupancies. In the cation, the ethyl group is disordered over two orientations with a refined occupancy ratio of 0.753 (5):0.247 (5), and the tetra-hydro-pyridinium ring adopts a distorted half-chair conformation. In the crystal, the ions are linked by C-H⋯O, N-H⋯O and C-H⋯S hydrogen bonds into a three-dimensional network.

References

  1. Nat Rev Drug Discov. 2009 Jun;8(6):449-50 - PubMed
  2. Bioorg Med Chem Lett. 2008 Aug 1;18(15):4420-3 - PubMed
  3. Acta Crystallogr Sect E Struct Rep Online. 2010 Dec 24;67(Pt 1):o226 - PubMed
  4. Am J Cardiovasc Drugs. 2009;9(4):213-29 - PubMed
  5. Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22 - PubMed
  6. Bioorg Med Chem Lett. 2005 Dec 15;15(24):5567-73 - PubMed
  7. Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55 - PubMed
  8. J Med Chem. 2002 Sep 26;45(20):4443-59 - PubMed
  9. Bioorg Med Chem Lett. 2005 Nov 1;15(21):4681-4 - PubMed

Publication Types