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Foroozandeh M, Adams RW, Kiraly P, et al. Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis. Chem Commun (Camb). 2015;51(84):15410-3doi: 10.1039/c5cc06293d.
Foroozandeh, M., Adams, R. W., Kiraly, P., Nilsson, M., & Morris, G. A. (2015). Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis. Chemical communications (Cambridge, England), 51(84), 15410-3. https://doi.org/10.1039/c5cc06293d
Foroozandeh, M, et al. "Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis." Chemical communications (Cambridge, England) vol. 51,84 (2015): 15410-3. doi: https://doi.org/10.1039/c5cc06293d
Foroozandeh M, Adams RW, Kiraly P, Nilsson M, Morris GA. Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis. Chem Commun (Camb). 2015 Oct 28;51(84):15410-3. doi: 10.1039/c5cc06293d. PMID: 26343867.
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Chem Commun (Camb). 2015 Oct 28;51(84):15410-3. doi: 10.1039/c5cc06293d.

Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis.

Chemical communications (Cambridge, England)

M Foroozandeh, R W Adams, P Kiraly, M Nilsson, G A Morris

Affiliations

  1. School of Chemistry, University of Manchester, Oxford Road, Manchester M13 9PL, UK. [email protected].

PMID: 26343867 DOI: 10.1039/c5cc06293d

Abstract

The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin-spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.

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