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Tang J, Xu B, Mao X, et al. One-Pot Synthesis of Pyrrolo[3,2,1-kl]phenothiazines through Copper-Catalyzed Tandem Coupling/Double Cyclization Reaction. J Org Chem. 2015;80(21):11108-14doi: 10.1021/acs.joc.5b01745.
Tang, J., Xu, B., Mao, X., Yang, H., Wang, X., & Lv, X. (2015). One-Pot Synthesis of Pyrrolo[3,2,1-kl]phenothiazines through Copper-Catalyzed Tandem Coupling/Double Cyclization Reaction. The Journal of organic chemistry, 80(21), 11108-14. https://doi.org/10.1021/acs.joc.5b01745
Tang, Jiaming, et al. "One-Pot Synthesis of Pyrrolo[3,2,1-kl]phenothiazines through Copper-Catalyzed Tandem Coupling/Double Cyclization Reaction." The Journal of organic chemistry vol. 80,21 (2015): 11108-14. doi: https://doi.org/10.1021/acs.joc.5b01745
Tang J, Xu B, Mao X, Yang H, Wang X, Lv X. One-Pot Synthesis of Pyrrolo[3,2,1-kl]phenothiazines through Copper-Catalyzed Tandem Coupling/Double Cyclization Reaction. J Org Chem. 2015 Nov 06;80(21):11108-14. doi: 10.1021/acs.joc.5b01745. Epub 2015 Oct 09. PMID: 26430717.
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J Org Chem. 2015 Nov 06;80(21):11108-14. doi: 10.1021/acs.joc.5b01745. Epub 2015 Oct 09.

One-Pot Synthesis of Pyrrolo[3,2,1-kl]phenothiazines through Copper-Catalyzed Tandem Coupling/Double Cyclization Reaction.

The Journal of organic chemistry

Jiaming Tang, Bingqing Xu, Xi Mao, Hongyan Yang, Xiaoxia Wang, Xin Lv

Affiliations

  1. Department of Chemistry, College of Chemistry and Life Sciences, Zhejiang Normal University , Jinhua 321004, People's Republic of China.

PMID: 26430717 DOI: 10.1021/acs.joc.5b01745

Abstract

A novel and efficient synthesis of pyrrolo[3,2,1-kl]phenothiazines has been developed through a Cu(I)-catalyzed tandem C-S coupling/double cyclization process. Using 2-alkynyl-6-iodoanilines and o-bromobenzenethiols as the starting materials, a wide range of pyrrolo[3,2,1-kl]phenothiazine derivatives were facilely and efficiently generated in one pot under Cu(I) catalysis.

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