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Vaccaro FA, Koplitz LV, Mague JT. Crystal structure of 2-cyano-1-methyl-pyridinium tetra-fluoro-borate. Acta Crystallogr E Crystallogr Commun. 2015;71:o697-8doi: 10.1107/S2056989015016011.
Vaccaro, F. A., Koplitz, L. V., & Mague, J. T. (2015). Crystal structure of 2-cyano-1-methyl-pyridinium tetra-fluoro-borate. Acta crystallographica. Section E, Crystallographic communications, 71o697-8. https://doi.org/10.1107/S2056989015016011
Vaccaro, Francesca A, et al. "Crystal structure of 2-cyano-1-methyl-pyridinium tetra-fluoro-borate." Acta crystallographica. Section E, Crystallographic communications vol. 71 (2015): o697-8. doi: https://doi.org/10.1107/S2056989015016011
Vaccaro FA, Koplitz LV, Mague JT. Crystal structure of 2-cyano-1-methyl-pyridinium tetra-fluoro-borate. Acta Crystallogr E Crystallogr Commun. 2015 Sep 12;71:o697-8. doi: 10.1107/S2056989015016011. eCollection 2015 Oct 01. PMID: 26594429; PMCID: PMC4647419.
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Acta Crystallogr E Crystallogr Commun. 2015 Sep 12;71:o697-8. doi: 10.1107/S2056989015016011. eCollection 2015 Oct 01.

Crystal structure of 2-cyano-1-methyl-pyridinium tetra-fluoro-borate.

Acta crystallographica. Section E, Crystallographic communications

Francesca A Vaccaro, Lynn V Koplitz, Joel T Mague

Affiliations

  1. Department of Chemistry, Loyola University, New Orleans, LA 70118, USA.
  2. Department of Chemistry, Tulane University, New Orleans, LA 70118, USA.

PMID: 26594429 PMCID: PMC4647419 DOI: 10.1107/S2056989015016011

Abstract

The asymmetric unit of the title salt, C7H7N2 (+)·BF4 (-), comprises two independent but nearly identical formula units. The solid-state structure comprises corrugated layers of cations and anions, formed by C-H⋯F hydrogen bonding, that are approximately parallel to (010). Further C-H⋯F hydrogen bonding consolidates the three-dimensional architecture. The sample was refined as a two-component non-merohedral twin.

Keywords: C—H⋯F inter­actions; crystal structure; salt

References

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