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Priya K, Saravanan K, Kabilan S, et al. Crystal structure of 2-(2,4-diphenyl-3-aza-bicyclo-[3.3.1]nonan-9-yl-idene)aceto-nitrile. Acta Crystallogr E Crystallogr Commun. 2015;71:o792-3doi: 10.1107/S2056989015017740.
Priya, K., Saravanan, K., Kabilan, S., & Selvanayagam, S. (2015). Crystal structure of 2-(2,4-diphenyl-3-aza-bicyclo-[3.3.1]nonan-9-yl-idene)aceto-nitrile. Acta crystallographica. Section E, Crystallographic communications, 71o792-3. https://doi.org/10.1107/S2056989015017740
Priya, K, et al. "Crystal structure of 2-(2,4-diphenyl-3-aza-bicyclo-[3.3.1]nonan-9-yl-idene)aceto-nitrile." Acta crystallographica. Section E, Crystallographic communications vol. 71 (2015): o792-3. doi: https://doi.org/10.1107/S2056989015017740
Priya K, Saravanan K, Kabilan S, Selvanayagam S. Crystal structure of 2-(2,4-diphenyl-3-aza-bicyclo-[3.3.1]nonan-9-yl-idene)aceto-nitrile. Acta Crystallogr E Crystallogr Commun. 2015 Sep 26;71:o792-3. doi: 10.1107/S2056989015017740. eCollection 2015 Oct 01. PMID: 26594482; PMCID: PMC4647352.
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Acta Crystallogr E Crystallogr Commun. 2015 Sep 26;71:o792-3. doi: 10.1107/S2056989015017740. eCollection 2015 Oct 01.

Crystal structure of 2-(2,4-diphenyl-3-aza-bicyclo-[3.3.1]nonan-9-yl-idene)aceto-nitrile.

Acta crystallographica. Section E, Crystallographic communications

K Priya, K Saravanan, S Kabilan, S Selvanayagam

Affiliations

  1. Department of Chemistry, Annamalai University, Annamalainagar 608 002, India.
  2. PG & Research Department of Physics, Government Arts College, Melur 625 106, India.

PMID: 26594482 PMCID: PMC4647352 DOI: 10.1107/S2056989015017740

Abstract

In the title 3-aza-bicyclo-nonane derivative, C22H22N2, both the fused piperidine and cyclo-hexane rings adopt a chair conformation. The phenyl rings attached to the central aza-bicylononane fragment in an equatorial orientation are inclined to each other at 23.7 (1)°. The amino group is not involved in any hydrogen bonding, so the crystal packing is stabilized only by van der Waals forces.

Keywords: 3-aza­bicyclo­nonane derivatives; chair conformation; crystal structure

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