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Reilly SW, Webster CE, Hollis TK, et al. Transmetallation from CCC-NHC pincer Zr complexes in the synthesis of air-stable CCC-NHC pincer Co(iii) complexes and initial hydroboration trials. Dalton Trans. 2016;45(7):2823-8doi: 10.1039/c5dt04752h.
Reilly, S. W., Webster, C. E., Hollis, T. K., & Valle, H. U. (2016). Transmetallation from CCC-NHC pincer Zr complexes in the synthesis of air-stable CCC-NHC pincer Co(iii) complexes and initial hydroboration trials. Dalton transactions (Cambridge, England : 2003), 45(7), 2823-8. https://doi.org/10.1039/c5dt04752h
Reilly, Sean W, et al. "Transmetallation from CCC-NHC pincer Zr complexes in the synthesis of air-stable CCC-NHC pincer Co(iii) complexes and initial hydroboration trials." Dalton transactions (Cambridge, England : 2003) vol. 45,7 (2016): 2823-8. doi: https://doi.org/10.1039/c5dt04752h
Reilly SW, Webster CE, Hollis TK, Valle HU. Transmetallation from CCC-NHC pincer Zr complexes in the synthesis of air-stable CCC-NHC pincer Co(iii) complexes and initial hydroboration trials. Dalton Trans. 2016 Feb 21;45(7):2823-8. doi: 10.1039/c5dt04752h. Epub 2016 Jan 27. PMID: 26814468.
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Dalton Trans. 2016 Feb 21;45(7):2823-8. doi: 10.1039/c5dt04752h. Epub 2016 Jan 27.

Transmetallation from CCC-NHC pincer Zr complexes in the synthesis of air-stable CCC-NHC pincer Co(iii) complexes and initial hydroboration trials.

Dalton transactions (Cambridge, England : 2003)

Sean W Reilly, Charles Edwin Webster, T Keith Hollis, Henry U Valle

Affiliations

  1. Department of Chemistry, Mississippi State University, Mississippi State, MS 39762-9573, USA. [email protected].

PMID: 26814468 DOI: 10.1039/c5dt04752h

Abstract

Development of CCC-NHC pincer Co complexes via transmetalation from Zr is reported. Formation of these air-stable Co(iii) complexes was achieved through use of a CoCl2 or Co(acac)3in situ or with a discrete CCC-NHC pincer Zr transmetallating agent. Preliminary activity in the hydroboration of styrene is reported. This facile methodology will further the development of CCC-NHC pincer first-row transition metal complexes.

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