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Woźniak-Braszak A, Jurga K, Baranowski M. The Lipari-Szabo Model-Free Analysis as a Method for Study of Molecular Motion in Solid State Heteronuclear Systems Using NMR Off-Resonance. Appl Magn Reson. 2016;47:567-574doi: 10.1007/s00723-016-0785-5.
Woźniak-Braszak, A., Jurga, K., & Baranowski, M. (2016). The Lipari-Szabo Model-Free Analysis as a Method for Study of Molecular Motion in Solid State Heteronuclear Systems Using NMR Off-Resonance. Applied magnetic resonance, 47567-574. https://doi.org/10.1007/s00723-016-0785-5
Woźniak-Braszak, A, et al. "The Lipari-Szabo Model-Free Analysis as a Method for Study of Molecular Motion in Solid State Heteronuclear Systems Using NMR Off-Resonance." Applied magnetic resonance vol. 47 (2016): 567-574. doi: https://doi.org/10.1007/s00723-016-0785-5
Woźniak-Braszak A, Jurga K, Baranowski M. The Lipari-Szabo Model-Free Analysis as a Method for Study of Molecular Motion in Solid State Heteronuclear Systems Using NMR Off-Resonance. Appl Magn Reson. 2016;47:567-574. doi: 10.1007/s00723-016-0785-5. Epub 2016 Apr 28. PMID: 27340336; PMCID: PMC4875056.
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Appl Magn Reson. 2016;47:567-574. doi: 10.1007/s00723-016-0785-5. Epub 2016 Apr 28.

The Lipari-Szabo Model-Free Analysis as a Method for Study of Molecular Motion in Solid State Heteronuclear Systems Using NMR Off-Resonance.

Applied magnetic resonance

A Woźniak-Braszak, K Jurga, M Baranowski

Affiliations

  1. High Pressure Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan, Poland.

PMID: 27340336 PMCID: PMC4875056 DOI: 10.1007/s00723-016-0785-5

Abstract

In the present work, a new method for measuring motional parameters using the off-resonance technique was described. The Lipari-Szabo model-free formalism was used to analyze molecular dynamics in a heteronuclear system [1, 2]. Cross-relaxation solid state nuclear magnetic resonance off-resonance experiments were performed on a homebuilt pulse spectrometer operating at the frequency of 30.2 MHz for protons at temperature 173 K. The proton spins were spin-locked in the effective field [Formula: see text] while

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