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Kokhan SO, Tymtsunik AV, Grage SL, et al. Design, Synthesis, and Application of an Optimized Monofluorinated Aliphatic Label for Peptide Studies by Solid-State . Angew Chem Int Ed Engl. 2016;55(47):14788-14792doi: 10.1002/anie.201608116.
Kokhan, S. O., Tymtsunik, A. V., Grage, S. L., Afonin, S., Babii, O., Berditsch, M., Strizhak, A. V., Bandak, D., Platonov, M. O., Komarov, I. V., Ulrich, A. S., & Mykhailiuk, P. K. (2016). Design, Synthesis, and Application of an Optimized Monofluorinated Aliphatic Label for Peptide Studies by Solid-State . Angewandte Chemie (International ed. in English), 55(47), 14788-14792. https://doi.org/10.1002/anie.201608116
Kokhan, Serhii O, et al. "Design, Synthesis, and Application of an Optimized Monofluorinated Aliphatic Label for Peptide Studies by Solid-State ." Angewandte Chemie (International ed. in English) vol. 55,47 (2016): 14788-14792. doi: https://doi.org/10.1002/anie.201608116
Kokhan SO, Tymtsunik AV, Grage SL, Afonin S, Babii O, Berditsch M, Strizhak AV, Bandak D, Platonov MO, Komarov IV, Ulrich AS, Mykhailiuk PK. Design, Synthesis, and Application of an Optimized Monofluorinated Aliphatic Label for Peptide Studies by Solid-State . Angew Chem Int Ed Engl. 2016 Nov 14;55(47):14788-14792. doi: 10.1002/anie.201608116. Epub 2016 Oct 05. PMID: 27706889.
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Angew Chem Int Ed Engl. 2016 Nov 14;55(47):14788-14792. doi: 10.1002/anie.201608116. Epub 2016 Oct 05.

Design, Synthesis, and Application of an Optimized Monofluorinated Aliphatic Label for Peptide Studies by Solid-State .

Angewandte Chemie (International ed. in English)

Serhii O Kokhan, Andriy V Tymtsunik, Stephan L Grage, Sergii Afonin, Oleg Babii, Marina Berditsch, Alexander V Strizhak, Dmytro Bandak, Maxim O Platonov, Igor V Komarov, Anne S Ulrich, Pavel K Mykhailiuk

Affiliations

  1. Enamine Ltd, Chervonotkatska 78, 02094, Kyiv, Ukraine.
  2. Institute of High Technologies, Taras Shevchenko National University of Kyiv, Volodymyrska 60, 01601, Kyiv, Ukraine.
  3. Institute of Biological Interfaces (IBG-2), Karlsruhe Institute of Technology (KIT), POB 3640, 76021, Karlsruhe, Germany.
  4. Institute of Organic Chemistry (IOC), KIT, Fritz-Haber-Weg 6, 76131, Karlsruhe, Germany.
  5. Chemistry Department, Taras Shevchenko National University of Kyiv, Volodymyrska 64, 01601, Kyiv, Ukraine.

PMID: 27706889 DOI: 10.1002/anie.201608116

Abstract

A conformationally restricted monofluorinated α-amino acid, (3-fluorobicyclo[1.1.1]pentyl)glycine (F-Bpg), was designed as a label for the structural analysis of membrane-bound peptides by solid-state

© 2016 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Keywords: amino acids; fluorine; peptides; propellanes; solid-state NMR spectroscopy

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