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Ndukwe IE, Shchukina A, Kazimierczuk K, et al. Rapid and safe ASAP acquisition with EXACT NMR. Chem Commun (Camb). 2016;52(86):12769-12772doi: 10.1039/c6cc07140f.
Ndukwe, I. E., Shchukina, A., Kazimierczuk, K., & Butts, C. P. (2016). Rapid and safe ASAP acquisition with EXACT NMR. Chemical communications (Cambridge, England), 52(86), 12769-12772. https://doi.org/10.1039/c6cc07140f
Ndukwe, I E, et al. "Rapid and safe ASAP acquisition with EXACT NMR." Chemical communications (Cambridge, England) vol. 52,86 (2016): 12769-12772. doi: https://doi.org/10.1039/c6cc07140f
Ndukwe IE, Shchukina A, Kazimierczuk K, Butts CP. Rapid and safe ASAP acquisition with EXACT NMR. Chem Commun (Camb). 2016 Oct 20;52(86):12769-12772. doi: 10.1039/c6cc07140f. PMID: 27727337.
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Chem Commun (Camb). 2016 Oct 20;52(86):12769-12772. doi: 10.1039/c6cc07140f.

Rapid and safe ASAP acquisition with EXACT NMR.

Chemical communications (Cambridge, England)

I E Ndukwe, A Shchukina, K Kazimierczuk, C P Butts

Affiliations

  1. School of Chemistry, University of Bristol, Cantocks Close, Bristol, BS8 1TS, UK. [email protected].
  2. Centre of New Technologies, University of Warsaw, Banacha 2C, 02089, Warszawa, Poland and Institute for Spectroscopy, Russian Academy of Sciences, Fizicheskaya 5, 142190, Moscow, Troitsk, Russia.
  3. Centre of New Technologies, University of Warsaw, Banacha 2C, 02089, Warszawa, Poland.

PMID: 27727337 DOI: 10.1039/c6cc07140f

Abstract

The dangerously high power levels required for fast ASAP-HSQC and ASAP-HMQC experiments are mitigated by employing EXACT NMR. The utility of this technique is demonstrated by application of the EXACT ASAP-HSQC to chemical reaction monitoring, accelerating data acquisition by up to 2 orders of magnitude - providing evidence of it's value in fast quantitative NMR processes.

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