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Lu J, Hua X, Long YT. Recent advances in real-time and in situ analysis of an electrode-electrolyte interface by mass spectrometry. Analyst. 2017;142(5):691-699doi: 10.1039/c6an02757a.
Lu, J., Hua, X., & Long, Y. T. (2017). Recent advances in real-time and in situ analysis of an electrode-electrolyte interface by mass spectrometry. The Analyst, 142(5), 691-699. https://doi.org/10.1039/c6an02757a
Lu, Jusheng, et al. "Recent advances in real-time and in situ analysis of an electrode-electrolyte interface by mass spectrometry." The Analyst vol. 142,5 (2017): 691-699. doi: https://doi.org/10.1039/c6an02757a
Lu J, Hua X, Long YT. Recent advances in real-time and in situ analysis of an electrode-electrolyte interface by mass spectrometry. Analyst. 2017 Feb 27;142(5):691-699. doi: 10.1039/c6an02757a. PMID: 28180217.
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Analyst. 2017 Feb 27;142(5):691-699. doi: 10.1039/c6an02757a.

Recent advances in real-time and in situ analysis of an electrode-electrolyte interface by mass spectrometry.

The Analyst

Jusheng Lu, Xin Hua, Yi-Tao Long

Affiliations

  1. School of Chemistry and Chemical Engineering, Jiangsu Normal University, Xuzhou, 221116, P. R. China.
  2. Key Laboratory for Advanced Materials and Department of Chemistry, East China University of Science and Technology, Shanghai, 200237, P. R. China. [email protected].

PMID: 28180217 DOI: 10.1039/c6an02757a

Abstract

Electrode-electrolyte interface (EEI) analysis is of great significance in the investigation of electrochemical (EC) processes. Current ex situ surface techniques provided rich information of the structural/chemical composition of the EEI. However, real-time and in situ monitoring of the EEI is in great demand for a better understanding of the dynamic changes of the redox systems. Mass spectrometry (MS) is a useful technique for mass-resolved analysis of various analytes with the capability of on-line measurement. In this review, we give a brief overview of the development of online EC-MS techniques. Recent advances of well-established EC-MS techniques, such as differential electrochemical mass spectrometry and EC-electrospray ionization mass spectrometry, and their applications are summarized. Specifically, some newly designed EC reactors coupled with state-of-the-art mass spectrometry for the detection of short-lived intermediate species are highlighted.

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