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Rev Sci Instrum. 2018 Dec;89(12):123115. doi: 10.1063/1.5052374.

Capillary-tube package devices for the quantitative performance evaluation of nuclear magnetic resonance spectrometers and pulse sequences.

The Review of scientific instruments

Lingyu Chi, Ming Huang, Annalise R Pfaff, Jie Huang, Rex E Gerald, Klaus Woelk

Affiliations

  1. Department of Chemistry, Missouri University of Science and Technology, 400 West 11th St., Rolla, Missouri 65409-0010, USA.
  2. Department of Electrical and Computer Engineering, Missouri University of Science and Technology, 301 West 16th St., Rolla, Missouri 65409-0040, USA.
  3. American Inventor Institute, 141 B Willows Edge Court, Willow Springs, Illinois 60480, USA.

PMID: 30599605 DOI: 10.1063/1.5052374

Abstract

With the increased sensitivity of modern nuclear magnetic resonance (NMR) spectrometers, the minimum amount needed for chemical-shift referencing of NMR spectra has decreased to a point where a few microliters can be sufficient to observe a reference signal. The reduction in the amount of required reference material is the basis for the NMR Capillary-tube Package (CapPack) platform that utilizes capillary tubes with inner diameters smaller than 150

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