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J Clin Exp Dent. 2020 Feb 01;12(2):e103-e107. doi: 10.4317/jced.56412. eCollection 2020 Feb.

Bond strength of lithium disilicate after cleaning methods of the remaining hydrofluoric acid.

Journal of clinical and experimental dentistry

Daniela-Micheline Dos Santos, Sandro-Basso Bitencourt, Emily-Vivianne-Freitas da Silva, Adaias-Oliveira Matos, Georgia-de Castro Benez, Elidiane-Cipriano Rangel, Aldiéris-Alves Pesqueira, Valentim-Adelino-Ricardo Barão, Marcelo-Coelho Goiato

Affiliations

  1. DDS, PhD, Professor, Department of Dental Materials and Prosthodontics, Sao Paulo State University (UNESP), Araçatuba, Sao Paulo, Brazil.
  2. DDS, MSc, PhD student, Department of Dental Materials and Prosthodontics, Sao Paulo State University (UNESP), Araçatuba, Sao Paulo, Brazil.
  3. DDS, MSc, PhD Student, Department of Prosthodontics and Periodontology, University of Campinas (UNICAMP), Piracicaba, Sao Paulo, Brazil.
  4. DDS, Department of Dental Materials and Prosthodontics, Sao Paulo State University (UNESP), Araçatuba, Sao Paulo, Brazil.
  5. PhD, Professor, Laboratory of Technological Plasmas, São Paulo State University (UNESP), Sorocaba, Sao Paulo, Brazil.
  6. DDS, PhD, Professor, Department of Prosthodontics and Periodontology, University of Campinas (UNICAMP), Piracicaba, Sao Paulo, Brazil.

PMID: 32071690 PMCID: PMC7018474 DOI: 10.4317/jced.56412

Abstract

BACKGROUND: Different ceramic surface cleaning methods have been suggested after the acid conditioning. The aim was to evaluate the effect of different protocols used to remove the remaining hydrofluoric acid on the shear bond strength (SBS) between lithium disilicate and resin cement.

MATERIAL AND METHODS: Forty-four specimens of lithium disilicate (IPS e.max Press) were divided in 4 groups (n=11): group C (control, no treatment); group HF+S (5% hydrofluoric acid + silane); group HF+US+S (5% hydrofluoric acid + ultrasound cleaning + silane); group HF+PH+S (5% hydrofluoric acid + 37% phosphoric acid + silane). Scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) were performed to characterize the surface morphology. The SBS test was performed on the resin/ceramic interface, and the failure mode was characterized. SBS values were submitted to 1-way ANOVA and the Tukey test (α=.05). The relation between surface treatment and failure modes was analyzed using the chi-squared test (α=.05).

RESULTS: The surface treatment type interfered in the shear strength (

CONCLUSIONS: The utilization of ultrasound cleaning was an effective procedure to remove remaining fluorsilicate salts, promoting the highest SBS values.

Copyright: © 2020 Medicina Oral S.L.

Conflict of interest statement

Conflicts of interest The authors have declared that no conflict of interest exist.

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