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Chubarov VM, Pashkova GV, Panteeva SV, et al. Multielement analysis of continental and lacustrine ferromanganese nodules by WDXRF, TXRF, and ICP-MS methods. Intercomparison study and accuracy assessment. Appl Radiat Isot. 2021;178:109981doi: 10.1016/j.apradiso.2021.109981.
Chubarov, V. M., Pashkova, G. V., Panteeva, S. V., & Amosova, A. A. (2021). Multielement analysis of continental and lacustrine ferromanganese nodules by WDXRF, TXRF, and ICP-MS methods. Intercomparison study and accuracy assessment. Applied radiation and isotopes : including data, instrumentation and methods for use in agriculture, industry and medicine, 178109981. https://doi.org/10.1016/j.apradiso.2021.109981
Chubarov, Victor M, et al. "Multielement analysis of continental and lacustrine ferromanganese nodules by WDXRF, TXRF, and ICP-MS methods. Intercomparison study and accuracy assessment." Applied radiation and isotopes : including data, instrumentation and methods for use in agriculture, industry and medicine vol. 178 (2021): 109981. doi: https://doi.org/10.1016/j.apradiso.2021.109981
Chubarov VM, Pashkova GV, Panteeva SV, Amosova AA. Multielement analysis of continental and lacustrine ferromanganese nodules by WDXRF, TXRF, and ICP-MS methods. Intercomparison study and accuracy assessment. Appl Radiat Isot. 2021 Dec;178:109981. doi: 10.1016/j.apradiso.2021.109981. Epub 2021 Oct 14. PMID: 34678638.
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Appl Radiat Isot. 2021 Dec;178:109981. doi: 10.1016/j.apradiso.2021.109981. Epub 2021 Oct 14.

Multielement analysis of continental and lacustrine ferromanganese nodules by WDXRF, TXRF, and ICP-MS methods. Intercomparison study and accuracy assessment.

Applied radiation and isotopes : including data, instrumentation and methods for use in agriculture, industry and medicine

Victor M Chubarov, Galina V Pashkova, Svetlana V Panteeva, Alena A Amosova

Affiliations

  1. Laboratory of X-ray Analysis, Vinogradov Institute of Geochemistry, Siberian Branch of the Russian Academy of Sciences, 1A Favorsky St., 664033, Irkutsk, Russia. Electronic address: [email protected].
  2. Center for Geodynamics and Geochronology, Institute of Earth Crust, Siberian Branch of the Russian Academy of Sciences, 128 Lermontov St., 664033, Irkutsk, Russia.
  3. Laboratory of X-ray Analysis, Vinogradov Institute of Geochemistry, Siberian Branch of the Russian Academy of Sciences, 1A Favorsky St., 664033, Irkutsk, Russia.

PMID: 34678638 DOI: 10.1016/j.apradiso.2021.109981

Abstract

Specific elemental and mineral composition of lacustrine and continental nodules differ substantially from silicate sedimentary rock, oceanic nodules, and crusts. The examination of this rock type requires study of the applicability of analytical methods to get accurate data on the elemental composition due to the lack of matrix-matched certified reference materials. In this study, multielement analysis of continental and lacustrine ferromanganese nodules was performed using various analytical methods. Samples were prepared as fused glasses and pressed pellets for wavelength-dispersive X-ray fluorescence, suspensions for total reflection X-ray fluorescence, and solutions after fusion for inductively coupled plasma mass spectrometry measurements. An intercomparison test was carried out to study the results using several analytical methods.

Copyright © 2021 Elsevier Ltd. All rights reserved.

Keywords: Continental ferromanganese nodules; Inductively coupled plasma mass spectrometry; Lacustrine ferromanganese nodules; Total reflection X-ray fluorescence; Wavelength-dispersive X-ray fluorescence

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