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Lopukhov LV, Balandina AV, Nigmatullina LS, et al. Evaluation of multiple reaction monitoring cubed performed by a quadrupole-linear ion trap mass spectrometer for quantitative determination of 6-sulfatoxymelatonin in urine. J Chromatogr B Analyt Technol Biomed Life Sci. 2022;1190:123094doi: 10.1016/j.jchromb.2021.123094.
Lopukhov, L. V., Balandina, A. V., Nigmatullina, L. S., Mullakhmetova, A. F., Synbulatova, G. E., Laikov, A. V., Lopukhov, V. L., & Grigoryeva, T. V. (2022). Evaluation of multiple reaction monitoring cubed performed by a quadrupole-linear ion trap mass spectrometer for quantitative determination of 6-sulfatoxymelatonin in urine. Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 1190123094. https://doi.org/10.1016/j.jchromb.2021.123094
Lopukhov, Leonid V, et al. "Evaluation of multiple reaction monitoring cubed performed by a quadrupole-linear ion trap mass spectrometer for quantitative determination of 6-sulfatoxymelatonin in urine." Journal of chromatography. B, Analytical technologies in the biomedical and life sciences vol. 1190 (2022): 123094. doi: https://doi.org/10.1016/j.jchromb.2021.123094
Lopukhov LV, Balandina AV, Nigmatullina LS, Mullakhmetova AF, Synbulatova GE, Laikov AV, Lopukhov VL, Grigoryeva TV. Evaluation of multiple reaction monitoring cubed performed by a quadrupole-linear ion trap mass spectrometer for quantitative determination of 6-sulfatoxymelatonin in urine. J Chromatogr B Analyt Technol Biomed Life Sci. 2022 Jan 10;1190:123094. doi: 10.1016/j.jchromb.2021.123094. Epub 2022 Jan 10. PMID: 35030474.
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J Chromatogr B Analyt Technol Biomed Life Sci. 2022 Jan 10;1190:123094. doi: 10.1016/j.jchromb.2021.123094. Epub 2022 Jan 10.

Evaluation of multiple reaction monitoring cubed performed by a quadrupole-linear ion trap mass spectrometer for quantitative determination of 6-sulfatoxymelatonin in urine.

Journal of chromatography. B, Analytical technologies in the biomedical and life sciences

Leonid V Lopukhov, Anna V Balandina, Lilia S Nigmatullina, Adelya F Mullakhmetova, Gulnaz E Synbulatova, Alexander V Laikov, Victor L Lopukhov, Tatiana V Grigoryeva

Affiliations

  1. Kazan Federal University, Institute of Fundamental Medicine and Biology, Karl Marx 76, Kazan 420012, Russian Federation. Electronic address: [email protected].
  2. Kazan Federal University, Institute of Fundamental Medicine and Biology, Karl Marx 76, Kazan 420012, Russian Federation.

PMID: 35030474 DOI: 10.1016/j.jchromb.2021.123094

Abstract

Liquid chromatography (LC) - mass spectrometry quantitative analysis of substances in biological samples is usually performed in the multiple reaction monitoring (MRM) variant. In complex biological matrices, strong interferences can be observed when using the LC-MRM method. Interference levels can be significantly reduced by using LC - multiple reaction monitoring cubed (MRM

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Keywords: 6-sulfatoxymelatonin; Linear ion trap; MRM(3); Multiple reaction monitoring cubed

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