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Carbon Nanotubes and Related Nanomaterials: Critical Advances and Challenges for Synthesis toward Mainstream Commercial Applications.

ACS nano

Rao R, Pint CL, Islam AE, Weatherup RS, Hofmann S, Meshot ER, Wu F, Zhou C, Dee N, Amama PB, Carpena-Nuñez J, Shi W, Plata DL, Penev ES, Yakobson BI, Balbuena PB, Bichara C, Futaba DN, Noda S, Shin H, Kim KS, Simard B, Mirri F, Pasquali M, Fornasiero F, Kauppinen EI, Arnold M, Cola BA, Nikolaev P, Arepalli S, Cheng HM, Zakharov DN, Stach EA, Zhang J, Wei F, Terrones M, Geohegan DB, Maruyama B, Maruyama S, Li Y, Adams WW, Hart AJ.
PMID: 30516055
ACS Nano. 2018 Dec 26;12(12):11756-11784. doi: 10.1021/acsnano.8b06511. Epub 2018 Dec 05.

Advances in the synthesis and scalable manufacturing of single-walled carbon nanotubes (SWCNTs) remain critical to realizing many important commercial applications. Here we review recent breakthroughs in the synthesis of SWCNTs and highlight key ongoing research areas and challenges. A...

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Rao R, Pint CL, Islam AE, et al. Carbon Nanotubes and Related Nanomaterials: Critical Advances and Challenges for Synthesis toward Mainstream Commercial Applications. ACS Nano. 2018;12(12):11756-11784doi: 10.1021/acsnano.8b06511.
Rao, R., Pint, C. L., Islam, A. E., Weatherup, R. S., Hofmann, S., Meshot, E. R., Wu, F., Zhou, C., Dee, N., Amama, P. B., Carpena-Nuñez, J., Shi, W., Plata, D. L., Penev, E. S., Yakobson, B. I., Balbuena, P. B., Bichara, C., Futaba, D. N., Noda, S., Shin, H., Kim, K. S., Simard, B., Mirri, F., Pasquali, M., Fornasiero, F., Kauppinen, E. I., Arnold, M., Cola, B. A., Nikolaev, P., Arepalli, S., Cheng, H. M., Zakharov, D. N., Stach, E. A., Zhang, J., Wei, F., Terrones, M., Geohegan, D. B., Maruyama, B., Maruyama, S., Li, Y., Adams, W. W., & Hart, A. J. (2018). Carbon Nanotubes and Related Nanomaterials: Critical Advances and Challenges for Synthesis toward Mainstream Commercial Applications. ACS nano, 12(12), 11756-11784. https://doi.org/10.1021/acsnano.8b06511
Rao, Rahul, et al. "Carbon Nanotubes and Related Nanomaterials: Critical Advances and Challenges for Synthesis toward Mainstream Commercial Applications." ACS nano vol. 12,12 (2018): 11756-11784. doi: https://doi.org/10.1021/acsnano.8b06511
Rao R, Pint CL, Islam AE, Weatherup RS, Hofmann S, Meshot ER, Wu F, Zhou C, Dee N, Amama PB, Carpena-Nuñez J, Shi W, Plata DL, Penev ES, Yakobson BI, Balbuena PB, Bichara C, Futaba DN, Noda S, Shin H, Kim KS, Simard B, Mirri F, Pasquali M, Fornasiero F, Kauppinen EI, Arnold M, Cola BA, Nikolaev P, Arepalli S, Cheng HM, Zakharov DN, Stach EA, Zhang J, Wei F, Terrones M, Geohegan DB, Maruyama B, Maruyama S, Li Y, Adams WW, Hart AJ. Carbon Nanotubes and Related Nanomaterials: Critical Advances and Challenges for Synthesis toward Mainstream Commercial Applications. ACS Nano. 2018 Dec 26;12(12):11756-11784. doi: 10.1021/acsnano.8b06511. Epub 2018 Dec 05. PMID: 30516055.
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Isolating the Roles of Hydrogen Exposure and Trace Carbon Contamination on the Formation of Active Catalyst Populations for Carbon Nanotube Growth.

ACS nano

Carpena-Núñez J, Boscoboinik JA, Saber S, Rao R, Zhong JQ, Maschmann MR, Kidambi PR, Dee NT, Zakharov DN, Hart AJ, Stach EA, Maruyama B.
PMID: 31329425
ACS Nano. 2019 Aug 27;13(8):8736-8748. doi: 10.1021/acsnano.9b01382. Epub 2019 Jul 22.

Limited understanding of the factors influencing the yield of carbon nanotubes (CNTs) relative to the number of catalyst particles remains an important barrier to their large-scale production with high quality, and to tailoring CNT properties for applications. This lack...

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Carpena-Núñez J, Boscoboinik JA, Saber S, et al. Isolating the Roles of Hydrogen Exposure and Trace Carbon Contamination on the Formation of Active Catalyst Populations for Carbon Nanotube Growth. ACS Nano. 2019;13(8):8736-8748doi: 10.1021/acsnano.9b01382.
Carpena-Núñez, J., Boscoboinik, J. A., Saber, S., Rao, R., Zhong, J. Q., Maschmann, M. R., Kidambi, P. R., Dee, N. T., Zakharov, D. N., Hart, A. J., Stach, E. A., & Maruyama, B. (2019). Isolating the Roles of Hydrogen Exposure and Trace Carbon Contamination on the Formation of Active Catalyst Populations for Carbon Nanotube Growth. ACS nano, 13(8), 8736-8748. https://doi.org/10.1021/acsnano.9b01382
Carpena-Núñez, Jennifer, et al. "Isolating the Roles of Hydrogen Exposure and Trace Carbon Contamination on the Formation of Active Catalyst Populations for Carbon Nanotube Growth." ACS nano vol. 13,8 (2019): 8736-8748. doi: https://doi.org/10.1021/acsnano.9b01382
Carpena-Núñez J, Boscoboinik JA, Saber S, Rao R, Zhong JQ, Maschmann MR, Kidambi PR, Dee NT, Zakharov DN, Hart AJ, Stach EA, Maruyama B. Isolating the Roles of Hydrogen Exposure and Trace Carbon Contamination on the Formation of Active Catalyst Populations for Carbon Nanotube Growth. ACS Nano. 2019 Aug 27;13(8):8736-8748. doi: 10.1021/acsnano.9b01382. Epub 2019 Jul 22. PMID: 31329425.
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Polyaniline/carbon nanotube sheet nanocomposites: fabrication and characterization.

ACS applied materials & interfaces

Kim JW, Siochi EJ, Carpena-Núñez J, Wise KE, Connell JW, Lin Y, Wincheski RA.
PMID: 23981043
ACS Appl Mater Interfaces. 2013 Sep 11;5(17):8597-606. doi: 10.1021/am402077d. Epub 2013 Aug 28.

Practical approaches are needed to take advantage of the nanometer-scale mechanical properties of carbon nanotubes (CNTs) at the macroscopic scale. This study was conducted to elucidate the salient factors that can maximize the mechanical properties of nanocomposites fabricated from...

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Kim JW, Siochi EJ, Carpena-Núñez J, et al. Polyaniline/carbon nanotube sheet nanocomposites: fabrication and characterization. ACS Appl Mater Interfaces. 2013;5(17):8597-606doi: 10.1021/am402077d.
Kim, J. W., Siochi, E. J., Carpena-Núñez, J., Wise, K. E., Connell, J. W., Lin, Y., & Wincheski, R. A. (2013). Polyaniline/carbon nanotube sheet nanocomposites: fabrication and characterization. ACS applied materials & interfaces, 5(17), 8597-606. https://doi.org/10.1021/am402077d
Kim, Jae-Woo, et al. "Polyaniline/carbon nanotube sheet nanocomposites: fabrication and characterization." ACS applied materials & interfaces vol. 5,17 (2013): 8597-606. doi: https://doi.org/10.1021/am402077d
Kim JW, Siochi EJ, Carpena-Núñez J, Wise KE, Connell JW, Lin Y, Wincheski RA. Polyaniline/carbon nanotube sheet nanocomposites: fabrication and characterization. ACS Appl Mater Interfaces. 2013 Sep 11;5(17):8597-606. doi: 10.1021/am402077d. Epub 2013 Aug 28. PMID: 23981043.
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Single-crystal γ-MnS nanowires conformally coated with carbon.

ACS applied materials & interfaces

Beltran-Huarac J, Resto O, Carpena-Nuñez J, Jadwisienczak WM, Fonseca LF, Weiner BR, Morell G.
PMID: 24392737
ACS Appl Mater Interfaces. 2014 Jan 22;6(2):1180-6. doi: 10.1021/am404746k. Epub 2014 Jan 10.

We report for the first time the fabrication of single-crystal metastable manganese sulfide nanowires (γ-MnS NWs) conformally coated with graphitic carbon via chemical vapor deposition technique using a single-step route. Advanced spectroscopy and electron microscopy techniques were applied to...

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Beltran-Huarac J, Resto O, Carpena-Nuñez J, et al. Single-crystal γ-MnS nanowires conformally coated with carbon. ACS Appl Mater Interfaces. 2014;6(2):1180-6doi: 10.1021/am404746k.
Beltran-Huarac, J., Resto, O., Carpena-Nuñez, J., Jadwisienczak, W. M., Fonseca, L. F., Weiner, B. R., & Morell, G. (2014). Single-crystal γ-MnS nanowires conformally coated with carbon. ACS applied materials & interfaces, 6(2), 1180-6. https://doi.org/10.1021/am404746k
Beltran-Huarac, Juan, et al. "Single-crystal γ-MnS nanowires conformally coated with carbon." ACS applied materials & interfaces vol. 6,2 (2014): 1180-6. doi: https://doi.org/10.1021/am404746k
Beltran-Huarac J, Resto O, Carpena-Nuñez J, Jadwisienczak WM, Fonseca LF, Weiner BR, Morell G. Single-crystal γ-MnS nanowires conformally coated with carbon. ACS Appl Mater Interfaces. 2014 Jan 22;6(2):1180-6. doi: 10.1021/am404746k. Epub 2014 Jan 10. PMID: 24392737.
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Creasable Batteries: Understanding Failure Modes through Dynamic Electrochemical Mechanical Testing.

ACS applied materials & interfaces

Blake AJ, Kohlmeyer RR, Drummy LF, Gutiérrez-Kolar JS, Carpena-Núñez J, Maruyama B, Shahbazian-Yassar R, Huang H, Durstock MF.
PMID: 26741734
ACS Appl Mater Interfaces. 2016 Mar 02;8(8):5196-204. doi: 10.1021/acsami.5b11175. Epub 2016 Jan 19.

Thin-film batteries that can be folded, bent, and even repeatedly creased with minimal or no loss in electrochemical performance have been demonstrated and systematically evaluated using two dynamic mechanical testing approaches for either controlled bending or creasing of flexible...

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Blake AJ, Kohlmeyer RR, Drummy LF, et al. Creasable Batteries: Understanding Failure Modes through Dynamic Electrochemical Mechanical Testing. ACS Appl Mater Interfaces. 2016;8(8):5196-204doi: 10.1021/acsami.5b11175.
Blake, A. J., Kohlmeyer, R. R., Drummy, L. F., Gutiérrez-Kolar, J. S., Carpena-Núñez, J., Maruyama, B., Shahbazian-Yassar, R., Huang, H., & Durstock, M. F. (2016). Creasable Batteries: Understanding Failure Modes through Dynamic Electrochemical Mechanical Testing. ACS applied materials & interfaces, 8(8), 5196-204. https://doi.org/10.1021/acsami.5b11175
Blake, Aaron J, et al. "Creasable Batteries: Understanding Failure Modes through Dynamic Electrochemical Mechanical Testing." ACS applied materials & interfaces vol. 8,8 (2016): 5196-204. doi: https://doi.org/10.1021/acsami.5b11175
Blake AJ, Kohlmeyer RR, Drummy LF, Gutiérrez-Kolar JS, Carpena-Núñez J, Maruyama B, Shahbazian-Yassar R, Huang H, Durstock MF. Creasable Batteries: Understanding Failure Modes through Dynamic Electrochemical Mechanical Testing. ACS Appl Mater Interfaces. 2016 Mar 02;8(8):5196-204. doi: 10.1021/acsami.5b11175. Epub 2016 Jan 19. PMID: 26741734.
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Zeolite Nanosheets Stabilize Catalyst Particles to Promote the Growth of Thermodynamically Unfavorable, Small-Diameter Carbon Nanotubes.

Small (Weinheim an der Bergstrasse, Germany)

Carpena-Núñez J, Rao R, Kim D, Bets KV, Zakharov DN, Boscoboinik JA, Stach EA, Yakobson BI, Tsapatsis M, Stacchiola D, Maruyama B.
PMID: 32812375
Small. 2020 Sep;16(38):e2002120. doi: 10.1002/smll.202002120. Epub 2020 Aug 18.

A challenge in the synthesis of single-wall carbon nanotubes (SWCNTs) is the lack of control over the formation and evolution of catalyst nanoparticles and the lack of control over their size or chirality. Here, zeolite MFI nanosheets (MFI-Ns) are...

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Carpena-Núñez J, Rao R, Kim D, et al. Zeolite Nanosheets Stabilize Catalyst Particles to Promote the Growth of Thermodynamically Unfavorable, Small-Diameter Carbon Nanotubes. Small. 2020;16(38):e2002120doi: 10.1002/smll.202002120.
Carpena-Núñez, J., Rao, R., Kim, D., Bets, K. V., Zakharov, D. N., Boscoboinik, J. A., Stach, E. A., Yakobson, B. I., Tsapatsis, M., Stacchiola, D., & Maruyama, B. (2020). Zeolite Nanosheets Stabilize Catalyst Particles to Promote the Growth of Thermodynamically Unfavorable, Small-Diameter Carbon Nanotubes. Small (Weinheim an der Bergstrasse, Germany), 16(38), e2002120. https://doi.org/10.1002/smll.202002120
Carpena-Núñez, Jennifer, et al. "Zeolite Nanosheets Stabilize Catalyst Particles to Promote the Growth of Thermodynamically Unfavorable, Small-Diameter Carbon Nanotubes." Small (Weinheim an der Bergstrasse, Germany) vol. 16,38 (2020): e2002120. doi: https://doi.org/10.1002/smll.202002120
Carpena-Núñez J, Rao R, Kim D, Bets KV, Zakharov DN, Boscoboinik JA, Stach EA, Yakobson BI, Tsapatsis M, Stacchiola D, Maruyama B. Zeolite Nanosheets Stabilize Catalyst Particles to Promote the Growth of Thermodynamically Unfavorable, Small-Diameter Carbon Nanotubes. Small. 2020 Sep;16(38):e2002120. doi: 10.1002/smll.202002120. Epub 2020 Aug 18. PMID: 32812375.
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Gaseous product mixture from Fischer-Tropsch synthesis as an efficient carbon feedstock for low temperature CVD growth of carbon nanotube carpets.

Nanoscale

Almkhelfe H, Carpena-Núñez J, Back TC, Amama PB.
PMID: 27353432
Nanoscale. 2016 Jul 21;8(27):13476-87. doi: 10.1039/c6nr03679a. Epub 2016 Jun 29.

Low-temperature chemical vapor deposition (CVD) growth of carbon nanotube (CNT) carpets from Fe and Fe-Cu catalysts using a gaseous product mixture from Fischer-Tropsch synthesis (FTS-GP) as a superior carbon feedstock is demonstrated. This growth approach addresses a persistent issue...

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Almkhelfe H, Carpena-Núñez J, Back TC, et al. Gaseous product mixture from Fischer-Tropsch synthesis as an efficient carbon feedstock for low temperature CVD growth of carbon nanotube carpets. Nanoscale. 2016;8(27):13476-87doi: 10.1039/c6nr03679a.
Almkhelfe, H., Carpena-Núñez, J., Back, T. C., & Amama, P. B. (2016). Gaseous product mixture from Fischer-Tropsch synthesis as an efficient carbon feedstock for low temperature CVD growth of carbon nanotube carpets. Nanoscale, 8(27), 13476-87. https://doi.org/10.1039/c6nr03679a
Almkhelfe, Haider, et al. "Gaseous product mixture from Fischer-Tropsch synthesis as an efficient carbon feedstock for low temperature CVD growth of carbon nanotube carpets." Nanoscale vol. 8,27 (2016): 13476-87. doi: https://doi.org/10.1039/c6nr03679a
Almkhelfe H, Carpena-Núñez J, Back TC, Amama PB. Gaseous product mixture from Fischer-Tropsch synthesis as an efficient carbon feedstock for low temperature CVD growth of carbon nanotube carpets. Nanoscale. 2016 Jul 21;8(27):13476-87. doi: 10.1039/c6nr03679a. Epub 2016 Jun 29. PMID: 27353432.
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Thermoelectric properties and thermal tolerance of indium tin oxide nanowires.

Nanotechnology

Hernandez JA, Carpena-Nunez J, Fonseca LF, Pettes MT, Yacaman MJ, Benitez A.
PMID: 29901451
Nanotechnology. 2018 Sep 07;29(36):364001. doi: 10.1088/1361-6528/aaccd3. Epub 2018 Jun 14.

Highly crystalline indium tin oxide (ITO) nanowires were grown via a vapor-liquid-solid method, with thermal tolerance up to ∼1300 °C. We report the electric and thermoelectric properties of the ITO nanowires before and after heat treatments and draw conclusions...

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Hernandez JA, Carpena-Nunez J, Fonseca LF, et al. Thermoelectric properties and thermal tolerance of indium tin oxide nanowires. Nanotechnology. 2018;29(36):364001doi: 10.1088/1361-6528/aaccd3.
Hernandez, J. A., Carpena-Nunez, J., Fonseca, L. F., Pettes, M. T., Yacaman, M. J., & Benitez, A. (2018). Thermoelectric properties and thermal tolerance of indium tin oxide nanowires. Nanotechnology, 29(36), 364001. https://doi.org/10.1088/1361-6528/aaccd3
Hernandez, Jose A, et al. "Thermoelectric properties and thermal tolerance of indium tin oxide nanowires." Nanotechnology vol. 29,36 (2018): 364001. doi: https://doi.org/10.1088/1361-6528/aaccd3
Hernandez JA, Carpena-Nunez J, Fonseca LF, Pettes MT, Yacaman MJ, Benitez A. Thermoelectric properties and thermal tolerance of indium tin oxide nanowires. Nanotechnology. 2018 Sep 07;29(36):364001. doi: 10.1088/1361-6528/aaccd3. Epub 2018 Jun 14. PMID: 29901451.
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Mechanical characterization of pristine and hydrogen-exposed palladium nanowires by in situ TEM.

Nanotechnology

Carpena-Núñez J, Yang D, Kim JW, Park C, Fonseca LF.
PMID: 23262467
Nanotechnology. 2013 Jan 25;24(3):035701. doi: 10.1088/0957-4484/24/3/035701. Epub 2012 Dec 21.

Changes in the crystal lattice of palladium nanowires (Pd NWs) upon hydrogen exposure by absorption and interstitial introduction of hydrogen atoms within the matrix can induce swelling of the nanostructure and generate dislocations through the solid that may alter...

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Carpena-Núñez J, Yang D, Kim JW, et al. Mechanical characterization of pristine and hydrogen-exposed palladium nanowires by in situ TEM. Nanotechnology. 2012;24(3):035701doi: 10.1088/0957-4484/24/3/035701.
Carpena-Núñez, J., Yang, D., Kim, J. W., Park, C., & Fonseca, L. F. (2013). Mechanical characterization of pristine and hydrogen-exposed palladium nanowires by in situ TEM. Nanotechnology, 24(3), 035701. https://doi.org/10.1088/0957-4484/24/3/035701
Carpena-Núñez, Jennifer, et al. "Mechanical characterization of pristine and hydrogen-exposed palladium nanowires by in situ TEM." Nanotechnology vol. 24,3 (2013): 035701. doi: https://doi.org/10.1088/0957-4484/24/3/035701
Carpena-Núñez J, Yang D, Kim JW, Park C, Fonseca LF. Mechanical characterization of pristine and hydrogen-exposed palladium nanowires by in situ TEM. Nanotechnology. 2013 Jan 25;24(3):035701. doi: 10.1088/0957-4484/24/3/035701. Epub 2012 Dec 21. PMID: 23262467.
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Efficient Closed-loop Maximization of Carbon Nanotube Growth Rate using Bayesian Optimization.

Scientific reports

Chang J, Nikolaev P, Carpena-Núñez J, Rao R, Decker K, Islam AE, Kim J, Pitt MA, Myung JI, Maruyama B.
PMID: 32493911
Sci Rep. 2020 Jun 03;10(1):9040. doi: 10.1038/s41598-020-64397-3.

A major technological challenge in materials research is the large and complex parameter space, which hinders experimental throughput and ultimately slows down development and implementation. In single-walled carbon nanotube (CNT) synthesis, for instance, the poor yield obtained from conventional...

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Chang J, Nikolaev P, Carpena-Núñez J, et al. Efficient Closed-loop Maximization of Carbon Nanotube Growth Rate using Bayesian Optimization. Sci Rep. 2020;10(1):9040doi: 10.1038/s41598-020-64397-3.
Chang, J., Nikolaev, P., Carpena-Núñez, J., Rao, R., Decker, K., Islam, A. E., Kim, J., Pitt, M. A., Myung, J. I., & Maruyama, B. (2020). Efficient Closed-loop Maximization of Carbon Nanotube Growth Rate using Bayesian Optimization. Scientific reports, 10(1), 9040. https://doi.org/10.1038/s41598-020-64397-3
Chang, Jorge, et al. "Efficient Closed-loop Maximization of Carbon Nanotube Growth Rate using Bayesian Optimization." Scientific reports vol. 10,1 (2020): 9040. doi: https://doi.org/10.1038/s41598-020-64397-3
Chang J, Nikolaev P, Carpena-Núñez J, Rao R, Decker K, Islam AE, Kim J, Pitt MA, Myung JI, Maruyama B. Efficient Closed-loop Maximization of Carbon Nanotube Growth Rate using Bayesian Optimization. Sci Rep. 2020 Jun 03;10(1):9040. doi: 10.1038/s41598-020-64397-3. PMID: 32493911; PMCID: PMC7271124.
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Showing 1 to 10 of 10 entries