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Serial millisecond crystallography for routine room-temperature structure determination at synchrotrons.

Nature communications

Weinert T, Olieric N, Cheng R, Brünle S, James D, Ozerov D, Gashi D, Vera L, Marsh M, Jaeger K, Dworkowski F, Panepucci E, Basu S, Skopintsev P, Doré AS, Geng T, Cooke RM, Liang M, Prota AE, Panneels V, Nogly P, Ermler U, Schertler G, Hennig M, Steinmetz MO, Wang M, Standfuss J.
PMID: 28912485
Nat Commun. 2017 Sep 14;8(1):542. doi: 10.1038/s41467-017-00630-4.

Historically, room-temperature structure determination was succeeded by cryo-crystallography to mitigate radiation damage. Here, we demonstrate that serial millisecond crystallography at a synchrotron beamline equipped with high-viscosity injector and high frame-rate detector allows typical crystallographic experiments to be performed at...

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Weinert T, Olieric N, Cheng R, et al. Serial millisecond crystallography for routine room-temperature structure determination at synchrotrons. Nat Commun. 2017;8(1):542doi: 10.1038/s41467-017-00630-4.
Weinert, T., Olieric, N., Cheng, R., Brünle, S., James, D., Ozerov, D., Gashi, D., Vera, L., Marsh, M., Jaeger, K., Dworkowski, F., Panepucci, E., Basu, S., Skopintsev, P., Doré, A. S., Geng, T., Cooke, R. M., Liang, M., Prota, A. E., Panneels, V., Nogly, P., Ermler, U., Schertler, G., Hennig, M., Steinmetz, M. O., Wang, M., & Standfuss, J. (2017). Serial millisecond crystallography for routine room-temperature structure determination at synchrotrons. Nature communications, 8(1), 542. https://doi.org/10.1038/s41467-017-00630-4
Weinert, Tobias, et al. "Serial millisecond crystallography for routine room-temperature structure determination at synchrotrons." Nature communications vol. 8,1 (2017): 542. doi: https://doi.org/10.1038/s41467-017-00630-4
Weinert T, Olieric N, Cheng R, Brünle S, James D, Ozerov D, Gashi D, Vera L, Marsh M, Jaeger K, Dworkowski F, Panepucci E, Basu S, Skopintsev P, Doré AS, Geng T, Cooke RM, Liang M, Prota AE, Panneels V, Nogly P, Ermler U, Schertler G, Hennig M, Steinmetz MO, Wang M, Standfuss J. Serial millisecond crystallography for routine room-temperature structure determination at synchrotrons. Nat Commun. 2017 Sep 14;8(1):542. doi: 10.1038/s41467-017-00630-4. PMID: 28912485; PMCID: PMC5599499.
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Nickel-catalyzed reductive arylation of activated alkynes with aryl iodides.

Tetrahedron letters

Dorn SC, Olsen AK, Kelemen RE, Shrestha R, Weix DJ.
PMID: 26028781
Tetrahedron Lett. 2015 Jun 03;56(23):3365-3367. doi: 10.1016/j.tetlet.2015.02.120.

The direct, regioselective, and stereoselective arylation of activated alkynes with aryl iodides using a nickel catalyst and manganese reductant is described. The reaction conditions are mild (40 °C in MeOH, no acid or base) and an intermediate organomanganese reagent...

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Dorn SC, Olsen AK, Kelemen RE, et al. Nickel-catalyzed reductive arylation of activated alkynes with aryl iodides. Tetrahedron Lett. 2015;56(23):3365-3367doi: 10.1016/j.tetlet.2015.02.120.
Dorn, S. C., Olsen, A. K., Kelemen, R. E., Shrestha, R., & Weix, D. J. (2015). Nickel-catalyzed reductive arylation of activated alkynes with aryl iodides. Tetrahedron letters, 56(23), 3365-3367. https://doi.org/10.1016/j.tetlet.2015.02.120
Dorn, Stephanie C M, et al. "Nickel-catalyzed reductive arylation of activated alkynes with aryl iodides." Tetrahedron letters vol. 56,23 (2015): 3365-3367. doi: https://doi.org/10.1016/j.tetlet.2015.02.120
Dorn SC, Olsen AK, Kelemen RE, Shrestha R, Weix DJ. Nickel-catalyzed reductive arylation of activated alkynes with aryl iodides. Tetrahedron Lett. 2015 Jun 03;56(23):3365-3367. doi: 10.1016/j.tetlet.2015.02.120. PMID: 26028781; PMCID: PMC4446700.
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Correction to "A New Interleukin-13 Amino-Coated Gadolinium Metallofullerene Nanoparticle for Targeted MRI Detection of Glioblastoma Tumor Cells".

Journal of the American Chemical Society

Li T, Murphy S, Kiselev B, Bakshi KS, Zhang J, Eltahir A, Zhang Y, Chen Y, Zhu J, Davis RM, Madsen LA, Morris JR, Karolyi DR, LaConte SM, Sheng Z, Dorn HC.
PMID: 26820231
J Am Chem Soc. 2016 Feb 10;138(5):1723. doi: 10.1021/jacs.6b00117. Epub 2016 Jan 28.

No abstract available.

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Li T, Murphy S, Kiselev B, et al. Correction to "A New Interleukin-13 Amino-Coated Gadolinium Metallofullerene Nanoparticle for Targeted MRI Detection of Glioblastoma Tumor Cells". J Am Chem Soc. 2016;138(5):1723doi: 10.1021/jacs.6b00117.
Li, T., Murphy, S., Kiselev, B., Bakshi, K. S., Zhang, J., Eltahir, A., Zhang, Y., Chen, Y., Zhu, J., Davis, R. M., Madsen, L. A., Morris, J. R., Karolyi, D. R., LaConte, S. M., Sheng, Z., & Dorn, H. C. (2016). Correction to "A New Interleukin-13 Amino-Coated Gadolinium Metallofullerene Nanoparticle for Targeted MRI Detection of Glioblastoma Tumor Cells". Journal of the American Chemical Society, 138(5), 1723. https://doi.org/10.1021/jacs.6b00117
Li, Tinghui, et al. "Correction to "A New Interleukin-13 Amino-Coated Gadolinium Metallofullerene Nanoparticle for Targeted MRI Detection of Glioblastoma Tumor Cells"." Journal of the American Chemical Society vol. 138,5 (2016): 1723. doi: https://doi.org/10.1021/jacs.6b00117
Li T, Murphy S, Kiselev B, Bakshi KS, Zhang J, Eltahir A, Zhang Y, Chen Y, Zhu J, Davis RM, Madsen LA, Morris JR, Karolyi DR, LaConte SM, Sheng Z, Dorn HC. Correction to "A New Interleukin-13 Amino-Coated Gadolinium Metallofullerene Nanoparticle for Targeted MRI Detection of Glioblastoma Tumor Cells". J Am Chem Soc. 2016 Feb 10;138(5):1723. doi: 10.1021/jacs.6b00117. Epub 2016 Jan 28. PMID: 26820231.
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Crystallographic characterization of isomer 2 of Er2@C82 and comparison with isomer 1 of Er2@C82.

Chemical communications (Cambridge, England)

Olmstead MM, Lee HM, Stevenson S, Dorn HC, Balch AL.
PMID: 12510300
Chem Commun (Camb). 2002 Nov 21;(22):2688-9. doi: 10.1039/b209270k.

The X-ray crystal structure of (Isomer 2 of Er2@C82). NiII(OEP).2(benzene) shows that the fullerene cage in Isomer 2 of Er2@C82 is the C3v isomer (82:8) and that the erbium ions are distributed over 23 interior sites with occupancies ranging...

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Olmstead MM, Lee HM, Stevenson S, et al. Crystallographic characterization of isomer 2 of Er2@C82 and comparison with isomer 1 of Er2@C82. Chem Commun (Camb). 2002;(22):2688-9doi: 10.1039/b209270k.
Olmstead, M. M., Lee, H. M., Stevenson, S., Dorn, H. C., & Balch, A. L. (2002). Crystallographic characterization of isomer 2 of Er2@C82 and comparison with isomer 1 of Er2@C82. Chemical communications (Cambridge, England), (22), 2688-9. https://doi.org/10.1039/b209270k
Olmstead, Marilyn M, et al. "Crystallographic characterization of isomer 2 of Er2@C82 and comparison with isomer 1 of Er2@C82." Chemical communications (Cambridge, England) vol. ,22 (2002): 2688-9. doi: https://doi.org/10.1039/b209270k
Olmstead MM, Lee HM, Stevenson S, Dorn HC, Balch AL. Crystallographic characterization of isomer 2 of Er2@C82 and comparison with isomer 1 of Er2@C82. Chem Commun (Camb). 2002 Nov 21;(22):2688-9. doi: 10.1039/b209270k. PMID: 12510300.
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Sc3N@C68: folded pentalene coordination in an endohedral fullerene that does not obey the isolated pentagon rule.

Angewandte Chemie (International ed. in English)

Olmstead MM, Lee HM, Duchamp JC, Stevenson S, Marciu D, Dorn HC, Balch AL.
PMID: 12596171
Angew Chem Int Ed Engl. 2003 Feb 24;42(8):900-3. doi: 10.1002/anie.200390237.

No abstract available.

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Olmstead MM, Lee HM, Duchamp JC, et al. Sc3N@C68: folded pentalene coordination in an endohedral fullerene that does not obey the isolated pentagon rule. Angew Chem Int Ed Engl. 2003;42(8):900-3doi: 10.1002/anie.200390237.
Olmstead, M. M., Lee, H. M., Duchamp, J. C., Stevenson, S., Marciu, D., Dorn, H. C., & Balch, A. L. (2003). Sc3N@C68: folded pentalene coordination in an endohedral fullerene that does not obey the isolated pentagon rule. Angewandte Chemie (International ed. in English), 42(8), 900-3. https://doi.org/10.1002/anie.200390237
Olmstead, Marilyn M, et al. "Sc3N@C68: folded pentalene coordination in an endohedral fullerene that does not obey the isolated pentagon rule." Angewandte Chemie (International ed. in English) vol. 42,8 (2003): 900-3. doi: https://doi.org/10.1002/anie.200390237
Olmstead MM, Lee HM, Duchamp JC, Stevenson S, Marciu D, Dorn HC, Balch AL. Sc3N@C68: folded pentalene coordination in an endohedral fullerene that does not obey the isolated pentagon rule. Angew Chem Int Ed Engl. 2003 Feb 24;42(8):900-3. doi: 10.1002/anie.200390237. PMID: 12596171.
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Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons.

Journal of the American Chemical Society

Olmstead MM, de Bettencourt-Dias A, Stevenson S, Dorn HC, Balch AL.
PMID: 11960421
J Am Chem Soc. 2002 Apr 24;124(16):4172-3. doi: 10.1021/ja0116019.

The structure of one of the three previously separated isomers of {Er2@C82} has been determined through a single-crystal X-ray structure determination of the noncovalent adduct, {Er2@C82 Isomer I}.{CoII(OEP)}.1.4(C6H6).0.3(CHCl3). The C82 cage is identified specificlly as the Cs(82:6) isomer (one...

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Olmstead MM, de Bettencourt-Dias A, Stevenson S, et al. Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons. J Am Chem Soc. 2002;124(16):4172-3doi: 10.1021/ja0116019.
Olmstead, M. M., de Bettencourt-Dias, A., Stevenson, S., Dorn, H. C., & Balch, A. L. (2002). Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons. Journal of the American Chemical Society, 124(16), 4172-3. https://doi.org/10.1021/ja0116019
Olmstead, Marilyn M, et al. "Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons." Journal of the American Chemical Society vol. 124,16 (2002): 4172-3. doi: https://doi.org/10.1021/ja0116019
Olmstead MM, de Bettencourt-Dias A, Stevenson S, Dorn HC, Balch AL. Crystallographic characterization of the structure of the endohedral fullerene [Er2@C82 isomer I] with C(s) cage symmetry and multiple sites for erbium along a band of ten contiguous hexagons. J Am Chem Soc. 2002 Apr 24;124(16):4172-3. doi: 10.1021/ja0116019. PMID: 11960421.
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C60 rotation in the solid state: dynamics of a faceted spherical top.

Science (New York, N.Y.)

Johnson RD, Yannoni CS, Dorn HC, Salem JR, Bethune DS.
PMID: 17816831
Science. 1992 Mar 06;255(5049):1235-8. doi: 10.1126/science.255.5049.1235.

The rotational dynamics of C(60) in the solid state have been investigated with carbon-13 nuclear magnetic resonance ((13)C NMR). The relaxation rate due to chemical shift anisotropy (1/9T1(CSA)(1)) was precisely measured from the magnetic field dependence of T(1), allowing...

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Johnson RD, Yannoni CS, Dorn HC, et al. C60 rotation in the solid state: dynamics of a faceted spherical top. Science. 1992;255(5049):1235-8doi: 10.1126/science.255.5049.1235.
Johnson, R. D., Yannoni, C. S., Dorn, H. C., Salem, J. R., & Bethune, D. S. (1992). C60 rotation in the solid state: dynamics of a faceted spherical top. Science (New York, N.Y.), 255(5049), 1235-8. https://doi.org/10.1126/science.255.5049.1235
Johnson, R D, et al. "C60 rotation in the solid state: dynamics of a faceted spherical top." Science (New York, N.Y.) vol. 255,5049 (1992): 1235-8. doi: https://doi.org/10.1126/science.255.5049.1235
Johnson RD, Yannoni CS, Dorn HC, Salem JR, Bethune DS. C60 rotation in the solid state: dynamics of a faceted spherical top. Science. 1992 Mar 06;255(5049):1235-8. doi: 10.1126/science.255.5049.1235. PMID: 17816831.
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Trimethylamine as a Normal Constituent of Human Blood, Urine and Cerebrospinal Fluid.

The Biochemical journal

Dorée C, Golla F.
PMID: 16742173
Biochem J. 1911;5(6):306-24. doi: 10.1042/bj0050306.

No abstract available.

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Dorée C, Golla F. Trimethylamine as a Normal Constituent of Human Blood, Urine and Cerebrospinal Fluid. Biochem J. 1911;5(6):306-24doi: 10.1042/bj0050306.
Dorée, C., & Golla, F. (1911). Trimethylamine as a Normal Constituent of Human Blood, Urine and Cerebrospinal Fluid. The Biochemical journal, 5(6), 306-24. https://doi.org/10.1042/bj0050306
Dorée, C, and Golla, F. "Trimethylamine as a Normal Constituent of Human Blood, Urine and Cerebrospinal Fluid." The Biochemical journal vol. 5,6 (1911): 306-24. doi: https://doi.org/10.1042/bj0050306
Dorée C, Golla F. Trimethylamine as a Normal Constituent of Human Blood, Urine and Cerebrospinal Fluid. Biochem J. 1911;5(6):306-24. doi: 10.1042/bj0050306. PMID: 16742173; PMCID: PMC1276373.
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The Action of Sea Water on Cotton and other Textile Fibres.

The Biochemical journal

Dorée C.
PMID: 16742929
Biochem J. 1920 Dec;14(6):709-14. doi: 10.1042/bj0140709.

No abstract available.

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Dorée C. The Action of Sea Water on Cotton and other Textile Fibres. Biochem J. 1920;14(6):709-14doi: 10.1042/bj0140709.
Dorée, C. (1920). The Action of Sea Water on Cotton and other Textile Fibres. The Biochemical journal, 14(6), 709-14. https://doi.org/10.1042/bj0140709
Dorée, C. "The Action of Sea Water on Cotton and other Textile Fibres." The Biochemical journal vol. 14,6 (1920): 709-14. doi: https://doi.org/10.1042/bj0140709
Dorée C. The Action of Sea Water on Cotton and other Textile Fibres. Biochem J. 1920 Dec;14(6):709-14. doi: 10.1042/bj0140709. PMID: 16742929; PMCID: PMC1258937.
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The Stone Cells of the Pear.

The Biochemical journal

Dorée C, Barton-Wright EC.
PMID: 16743684
Biochem J. 1926;20(3):502-6. doi: 10.1042/bj0200502.

No abstract available.

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Dorée C, Barton-Wright EC. The Stone Cells of the Pear. Biochem J. 1926;20(3):502-6doi: 10.1042/bj0200502.
Dorée, C., & Barton-Wright, E. C. (1926). The Stone Cells of the Pear. The Biochemical journal, 20(3), 502-6. https://doi.org/10.1042/bj0200502
Dorée, C, and Barton-Wright, E C. "The Stone Cells of the Pear." The Biochemical journal vol. 20,3 (1926): 502-6. doi: https://doi.org/10.1042/bj0200502
Dorée C, Barton-Wright EC. The Stone Cells of the Pear. Biochem J. 1926;20(3):502-6. doi: 10.1042/bj0200502. PMID: 16743684; PMCID: PMC1251742.
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Contributions to the Study of Lignin: Part I. Metalignin, a New Type of Alkali Lignin.

The Biochemical journal

Dorée C, Barton-Wright EC.
PMID: 16743834
Biochem J. 1927;21(2):290-300. doi: 10.1042/bj0210290.

No abstract available.

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Dorée C, Barton-Wright EC. Contributions to the Study of Lignin: Part I. Metalignin, a New Type of Alkali Lignin. Biochem J. 1927;21(2):290-300doi: 10.1042/bj0210290.
Dorée, C., & Barton-Wright, E. C. (1927). Contributions to the Study of Lignin: Part I. Metalignin, a New Type of Alkali Lignin. The Biochemical journal, 21(2), 290-300. https://doi.org/10.1042/bj0210290
Dorée, C, and Barton-Wright, E C. "Contributions to the Study of Lignin: Part I. Metalignin, a New Type of Alkali Lignin." The Biochemical journal vol. 21,2 (1927): 290-300. doi: https://doi.org/10.1042/bj0210290
Dorée C, Barton-Wright EC. Contributions to the Study of Lignin: Part I. Metalignin, a New Type of Alkali Lignin. Biochem J. 1927;21(2):290-300. doi: 10.1042/bj0210290. PMID: 16743834; PMCID: PMC1251911.
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Nitroxide/substrate weak hydrogen bonding: attitude and dynamics of collisions in solution.

Journal of the American Chemical Society

Russ JL, Gu J, Tsai KH, Glass T, Duchamp JC, Dorn HC.
PMID: 17497854
J Am Chem Soc. 2007 Jun 06;129(22):7018-27. doi: 10.1021/ja064632i. Epub 2007 May 12.

The study of intermolecular collisions and bonding interactions in solutions is of critical importance in understanding and predicting solute/solvent properties. Previous work has established that stable paramagnetic nitroxide molecules are excellent probes of intermolecular interactions for hydrogen bonding in...

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Russ JL, Gu J, Tsai KH, et al. Nitroxide/substrate weak hydrogen bonding: attitude and dynamics of collisions in solution. J Am Chem Soc. 2007;129(22):7018-27doi: 10.1021/ja064632i.
Russ, J. L., Gu, J., Tsai, K. H., Glass, T., Duchamp, J. C., & Dorn, H. C. (2007). Nitroxide/substrate weak hydrogen bonding: attitude and dynamics of collisions in solution. Journal of the American Chemical Society, 129(22), 7018-27. https://doi.org/10.1021/ja064632i
Russ, Jennifer L, et al. "Nitroxide/substrate weak hydrogen bonding: attitude and dynamics of collisions in solution." Journal of the American Chemical Society vol. 129,22 (2007): 7018-27. doi: https://doi.org/10.1021/ja064632i
Russ JL, Gu J, Tsai KH, Glass T, Duchamp JC, Dorn HC. Nitroxide/substrate weak hydrogen bonding: attitude and dynamics of collisions in solution. J Am Chem Soc. 2007 Jun 06;129(22):7018-27. doi: 10.1021/ja064632i. Epub 2007 May 12. PMID: 17497854.
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Showing 1 to 12 of 120 entries