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Novel Syntheses of 2-Butyl-5-chloro-3H-imidazole-4-carbaldehyde: A Key Intermediate for the Synthesis of the Angiotensin II Antagonist Losartan.

The Journal of organic chemistry

Griffiths GJ, Hauck MB, Imwinkelried R, Kohr J, Roten CA, Stucky GC, Gosteli J.
PMID: 11674720
J Org Chem. 1999 Oct 29;64(22):8084-8089. doi: 10.1021/jo9824910.

Reaction of glycine methyl ester (19) with imidate 18 under carefully optimized conditions allowed preparation of the rather unstable imidazolinone 11 in ca. 90% yield. Reaction of 11 with POCl(3)/DMF followed by aqueous workup gave aldehyde 2, a key...

Cite
Griffiths GJ, Hauck MB, Imwinkelried R, et al. Novel Syntheses of 2-Butyl-5-chloro-3H-imidazole-4-carbaldehyde: A Key Intermediate for the Synthesis of the Angiotensin II Antagonist Losartan. J Org Chem. 1999;64(22):8084-8089doi: 10.1021/jo9824910.
Griffiths, G. J., Hauck, M. B., Imwinkelried, R., Kohr, J., Roten, C. A., Stucky, G. C., & Gosteli, J. (1999). Novel Syntheses of 2-Butyl-5-chloro-3H-imidazole-4-carbaldehyde: A Key Intermediate for the Synthesis of the Angiotensin II Antagonist Losartan. The Journal of organic chemistry, 64(22), 8084-8089. https://doi.org/10.1021/jo9824910
Griffiths, Gareth J., et al. "Novel Syntheses of 2-Butyl-5-chloro-3H-imidazole-4-carbaldehyde: A Key Intermediate for the Synthesis of the Angiotensin II Antagonist Losartan." The Journal of organic chemistry vol. 64,22 (1999): 8084-8089. doi: https://doi.org/10.1021/jo9824910
Griffiths GJ, Hauck MB, Imwinkelried R, Kohr J, Roten CA, Stucky GC, Gosteli J. Novel Syntheses of 2-Butyl-5-chloro-3H-imidazole-4-carbaldehyde: A Key Intermediate for the Synthesis of the Angiotensin II Antagonist Losartan. J Org Chem. 1999 Oct 29;64(22):8084-8089. doi: 10.1021/jo9824910. PMID: 11674720.
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Forensic bitemark identification: weak foundations, exaggerated claims.

Journal of law and the biosciences

Saks MJ, Albright T, Bohan TL, Bierer BE, Bowers CM, Bush MA, Bush PJ, Casadevall A, Cole SA, Denton MB, Diamond SS, Dioso-Villa R, Epstein J, Faigman D, Faigman L, Fienberg SE, Garrett BL, Giannelli PC, Greely HT, Imwinkelried E, Jamieson A, Kafadar K, Kassirer JP, Koehler J', Korn D, Mnookin J, Morrison AB, Murphy E, Peerwani N, Peterson JL, Risinger DM, Sensabaugh GF, Spiegelman C, Stern H, Thompson WC, Wayman JL, Zabell S, Zumwalt RE.
PMID: 28852538
J Law Biosci. 2016 Nov 23;3(3):538-575. doi: 10.1093/jlb/lsw045. eCollection 2016 Dec.

Several forensic sciences, especially of the pattern-matching kind, are increasingly seen to lack the scientific foundation needed to justify continuing admission as trial evidence. Indeed, several have been abolished in the recent past. A likely next candidate for elimination...

Cite
Saks MJ, Albright T, Bohan TL, et al. Forensic bitemark identification: weak foundations, exaggerated claims. J Law Biosci. 2016;3(3):538-575doi: 10.1093/jlb/lsw045.
Saks, M. J., Albright, T., Bohan, T. L., Bierer, B. E., Bowers, C. M., Bush, M. A., Bush, P. J., Casadevall, A., Cole, S. A., Denton, M. B., Diamond, S. S., Dioso-Villa, R., Epstein, J., Faigman, D., Faigman, L., Fienberg, S. E., Garrett, B. L., Giannelli, P. C., Greely, H. T., Imwinkelried, E., Jamieson, A., Kafadar, K., Kassirer, J. P., Koehler, J. '., Korn, D., Mnookin, J., Morrison, A. B., Murphy, E., Peerwani, N., Peterson, J. L., Risinger, D. M., Sensabaugh, G. F., Spiegelman, C., Stern, H., Thompson, W. C., Wayman, J. L., Zabell, S., & Zumwalt, R. E. (2016). Forensic bitemark identification: weak foundations, exaggerated claims. Journal of law and the biosciences, 3(3), 538-575. https://doi.org/10.1093/jlb/lsw045
Saks, Michael J, et al. "Forensic bitemark identification: weak foundations, exaggerated claims." Journal of law and the biosciences vol. 3,3 (2016): 538-575. doi: https://doi.org/10.1093/jlb/lsw045
Saks MJ, Albright T, Bohan TL, Bierer BE, Bowers CM, Bush MA, Bush PJ, Casadevall A, Cole SA, Denton MB, Diamond SS, Dioso-Villa R, Epstein J, Faigman D, Faigman L, Fienberg SE, Garrett BL, Giannelli PC, Greely HT, Imwinkelried E, Jamieson A, Kafadar K, Kassirer JP, Koehler J', Korn D, Mnookin J, Morrison AB, Murphy E, Peerwani N, Peterson JL, Risinger DM, Sensabaugh GF, Spiegelman C, Stern H, Thompson WC, Wayman JL, Zabell S, Zumwalt RE. Forensic bitemark identification: weak foundations, exaggerated claims. J Law Biosci. 2016 Nov 23;3(3):538-575. doi: 10.1093/jlb/lsw045. eCollection 2016 Dec. PMID: 28852538; PMCID: PMC5570687.
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Showing 1 to 2 of 2 entries