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Synthesis of Functionalized 1,4-Azaborinines by the Cyclization of Di-tert-butyliminoborane and Alkynes.

Journal of the American Chemical Society

Schäfer M, Beattie NA, Geetharani K, Schäfer J, Ewing WC, Krahfuß M, Hörl C, Dewhurst RD, Macgregor SA, Lambert C, Braunschweig H.
PMID: 27286231
J Am Chem Soc. 2016 Jul 06;138(26):8212-20. doi: 10.1021/jacs.6b04128. Epub 2016 Jun 27.

Di-tert-butyliminoborane is found to be a very useful synthon for the synthesis of a variety of functionalized 1,4-azaborinines by the Rh-mediated cyclization of iminoboranes with alkynes. The reactions proceed via [2 + 2] cycloaddition of iminoboranes and alkynes in...

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Schäfer M, Beattie NA, Geetharani K, et al. Synthesis of Functionalized 1,4-Azaborinines by the Cyclization of Di-tert-butyliminoborane and Alkynes. J Am Chem Soc. 2016;138(26):8212-20doi: 10.1021/jacs.6b04128.
Schäfer, M., Beattie, N. A., Geetharani, K., Schäfer, J., Ewing, W. C., Krahfuß, M., Hörl, C., Dewhurst, R. D., Macgregor, S. A., Lambert, C., & Braunschweig, H. (2016). Synthesis of Functionalized 1,4-Azaborinines by the Cyclization of Di-tert-butyliminoborane and Alkynes. Journal of the American Chemical Society, 138(26), 8212-20. https://doi.org/10.1021/jacs.6b04128
Schäfer, Marius, et al. "Synthesis of Functionalized 1,4-Azaborinines by the Cyclization of Di-tert-butyliminoborane and Alkynes." Journal of the American Chemical Society vol. 138,26 (2016): 8212-20. doi: https://doi.org/10.1021/jacs.6b04128
Schäfer M, Beattie NA, Geetharani K, Schäfer J, Ewing WC, Krahfuß M, Hörl C, Dewhurst RD, Macgregor SA, Lambert C, Braunschweig H. Synthesis of Functionalized 1,4-Azaborinines by the Cyclization of Di-tert-butyliminoborane and Alkynes. J Am Chem Soc. 2016 Jul 06;138(26):8212-20. doi: 10.1021/jacs.6b04128. Epub 2016 Jun 27. PMID: 27286231.
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Mild sp.

Organometallics

Lau S, Ward B, Zhou X, White AJP, Casely IJ, Macgregor SA, Crimmin MR.
PMID: 29151664
Organometallics. 2017 Sep 25;36(18):3654-3663. doi: 10.1021/acs.organomet.7b00632. Epub 2017 Sep 14.

The isolable ruthenium(II) bis(dinitrogen) complex [Ru(H)

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Lau S, Ward B, Zhou X, et al. Mild sp. Organometallics. 2017;36(18):3654-3663doi: 10.1021/acs.organomet.7b00632.
Lau, S., Ward, B., Zhou, X., White, A. J. P., Casely, I. J., Macgregor, S. A., & Crimmin, M. R. (2017). Mild sp. Organometallics, 36(18), 3654-3663. https://doi.org/10.1021/acs.organomet.7b00632
Lau, Samantha, et al. "Mild sp." Organometallics vol. 36,18 (2017): 3654-3663. doi: https://doi.org/10.1021/acs.organomet.7b00632
Lau S, Ward B, Zhou X, White AJP, Casely IJ, Macgregor SA, Crimmin MR. Mild sp. Organometallics. 2017 Sep 25;36(18):3654-3663. doi: 10.1021/acs.organomet.7b00632. Epub 2017 Sep 14. PMID: 29151664; PMCID: PMC5684690.
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Computational Studies of Carboxylate-Assisted C-H Activation and Functionalization at Group 8-10 Transition Metal Centers.

Chemical reviews

Davies DL, Macgregor SA, McMullin CL.
PMID: 28530807
Chem Rev. 2017 Jul 12;117(13):8649-8709. doi: 10.1021/acs.chemrev.6b00839. Epub 2017 May 22.

Computational studies on carboxylate-assisted C-H activation and functionalization at group 8-10 transition metal centers are reviewed. This Review is organized by metal and will cover work published from late 2009 until mid-2016. A brief overview of computational work prior...

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Davies DL, Macgregor SA, McMullin CL. Computational Studies of Carboxylate-Assisted C-H Activation and Functionalization at Group 8-10 Transition Metal Centers. Chem Rev. 2017;117(13):8649-8709doi: 10.1021/acs.chemrev.6b00839.
Davies, D. L., Macgregor, S. A., & McMullin, C. L. (2017). Computational Studies of Carboxylate-Assisted C-H Activation and Functionalization at Group 8-10 Transition Metal Centers. Chemical reviews, 117(13), 8649-8709. https://doi.org/10.1021/acs.chemrev.6b00839
Davies, David L, et al. "Computational Studies of Carboxylate-Assisted C-H Activation and Functionalization at Group 8-10 Transition Metal Centers." Chemical reviews vol. 117,13 (2017): 8649-8709. doi: https://doi.org/10.1021/acs.chemrev.6b00839
Davies DL, Macgregor SA, McMullin CL. Computational Studies of Carboxylate-Assisted C-H Activation and Functionalization at Group 8-10 Transition Metal Centers. Chem Rev. 2017 Jul 12;117(13):8649-8709. doi: 10.1021/acs.chemrev.6b00839. Epub 2017 May 22. PMID: 28530807.
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A Patient-Derived Xenograft Model of Parameningeal Embryonal Rhabdomyosarcoma for Preclinical Studies.

Sarcoma

Hooper JE, Cantor EL, Ehlen MS, Banerjee A, Malempati S, Stenzel P, Woltjer RL, Gandour-Edwards R, Goodwin NC, Yang Y, Kaur P, Bult CJ, Airhart SD, Keller C.
PMID: 26696773
Sarcoma. 2015;2015:826124. doi: 10.1155/2015/826124. Epub 2015 Nov 30.

Embryonal rhabdomyosarcoma (eRMS) is one of the most common soft tissue sarcomas in children and adolescents. Parameningeal eRMS is a variant that is often more difficult to treat than eRMS occurring at other sites. A 14-year-old female with persistent...

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Hooper JE, Cantor EL, Ehlen MS, et al. A Patient-Derived Xenograft Model of Parameningeal Embryonal Rhabdomyosarcoma for Preclinical Studies. Sarcoma. 2015;2015:826124doi: 10.1155/2015/826124.
Hooper, J. E., Cantor, E. L., Ehlen, M. S., Banerjee, A., Malempati, S., Stenzel, P., Woltjer, R. L., Gandour-Edwards, R., Goodwin, N. C., Yang, Y., Kaur, P., Bult, C. J., Airhart, S. D., & Keller, C. (2015). A Patient-Derived Xenograft Model of Parameningeal Embryonal Rhabdomyosarcoma for Preclinical Studies. Sarcoma, 2015826124. https://doi.org/10.1155/2015/826124
Hooper, Jody E, et al. "A Patient-Derived Xenograft Model of Parameningeal Embryonal Rhabdomyosarcoma for Preclinical Studies." Sarcoma vol. 2015 (2015): 826124. doi: https://doi.org/10.1155/2015/826124
Hooper JE, Cantor EL, Ehlen MS, Banerjee A, Malempati S, Stenzel P, Woltjer RL, Gandour-Edwards R, Goodwin NC, Yang Y, Kaur P, Bult CJ, Airhart SD, Keller C. A Patient-Derived Xenograft Model of Parameningeal Embryonal Rhabdomyosarcoma for Preclinical Studies. Sarcoma. 2015;2015:826124. doi: 10.1155/2015/826124. Epub 2015 Nov 30. PMID: 26696773; PMCID: PMC4677247.
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Revision of Staple Line Failure Following Roux-en-Y Gastric Bypass for Obesity: a follow-up of weight loss.

Obesity surgery

Macgregor AM, Rand CS.
PMID: 10775908
Obes Surg. 1991 Jun;1(2):151-154. doi: 10.1381/096089291765561169.

Eighty-one patients with primary Roux-en-Y gastric bypass for obesity underwent revisional surgery for staple-line failure. All patients (100%) were included in the follow-up. Two years later, patients had an excess weight loss of 77%; 91% of the patients had...

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Macgregor AM, Rand CS. Revision of Staple Line Failure Following Roux-en-Y Gastric Bypass for Obesity: a follow-up of weight loss. Obes Surg. 1991;1(2):151-154doi: 10.1381/096089291765561169.
Macgregor, A. M., & Rand, C. S. (1991). Revision of Staple Line Failure Following Roux-en-Y Gastric Bypass for Obesity: a follow-up of weight loss. Obesity surgery, 1(2), 151-154. https://doi.org/10.1381/096089291765561169
Macgregor, and Rand. "Revision of Staple Line Failure Following Roux-en-Y Gastric Bypass for Obesity: a follow-up of weight loss." Obesity surgery vol. 1,2 (1991): 151-154. doi: https://doi.org/10.1381/096089291765561169
Macgregor AM, Rand CS. Revision of Staple Line Failure Following Roux-en-Y Gastric Bypass for Obesity: a follow-up of weight loss. Obes Surg. 1991 Jun;1(2):151-154. doi: 10.1381/096089291765561169. PMID: 10775908.
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Metabolic Implications of Obesity, Weight Loss and Energy Expenditure following Gastric Restrictive Surgery.

Obesity surgery

Macgregor AM.
PMID: 10742770
Obes Surg. 1994 May;4(2):129-143. doi: 10.1381/096089294765558700.

This review examines the energetics and metabolic parameters which influence the effectiveness of gastric restrictive surgery in achieving weight loss in the clinically severely obese patient. Among the subjects discussed are the metabolic determinants and consequences of obesity, energy...

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Macgregor AM. Metabolic Implications of Obesity, Weight Loss and Energy Expenditure following Gastric Restrictive Surgery. Obes Surg. 1994;4(2):129-143doi: 10.1381/096089294765558700.
Macgregor, A. M. (1994). Metabolic Implications of Obesity, Weight Loss and Energy Expenditure following Gastric Restrictive Surgery. Obesity surgery, 4(2), 129-143. https://doi.org/10.1381/096089294765558700
Macgregor. "Metabolic Implications of Obesity, Weight Loss and Energy Expenditure following Gastric Restrictive Surgery." Obesity surgery vol. 4,2 (1994): 129-143. doi: https://doi.org/10.1381/096089294765558700
Macgregor AM. Metabolic Implications of Obesity, Weight Loss and Energy Expenditure following Gastric Restrictive Surgery. Obes Surg. 1994 May;4(2):129-143. doi: 10.1381/096089294765558700. PMID: 10742770.
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Headache and hormone replacement therapy in the postmenopausal woman.

Current treatment options in neurology

MacGregor EA.
PMID: 19094831
Curr Treat Options Neurol. 2009 Jan;11(1):10-7. doi: 10.1007/s11940-009-0002-z.

Headache and migraine are common symptoms of the menopause, often associated with irregular periods, hot flashes, and night sweats. Perimenopausal women should routinely be asked about headache and migraine, so that they can be offered appropriate advice. If attacks...

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MacGregor EA. Headache and hormone replacement therapy in the postmenopausal woman. Curr Treat Options Neurol. 2009;11(1):10-7doi: 10.1007/s11940-009-0002-z.
MacGregor, E. A. (2009). Headache and hormone replacement therapy in the postmenopausal woman. Current treatment options in neurology, 11(1), 10-7. https://doi.org/10.1007/s11940-009-0002-z
MacGregor, E Anne. "Headache and hormone replacement therapy in the postmenopausal woman." Current treatment options in neurology vol. 11,1 (2009): 10-7. doi: https://doi.org/10.1007/s11940-009-0002-z
MacGregor EA. Headache and hormone replacement therapy in the postmenopausal woman. Curr Treat Options Neurol. 2009 Jan;11(1):10-7. doi: 10.1007/s11940-009-0002-z. PMID: 19094831.
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Structure, reactivity, and computational studies of a novel ruthenium hydrogen sulfide dihydride complex.

Inorganic chemistry

Chatwin SL, Diggle RA, Jazzar RF, Macgregor SA, Mahon MF, Whittlesey MK.
PMID: 14632475
Inorg Chem. 2003 Dec 01;42(24):7695-7. doi: 10.1021/ic030241i.

Addition of 1 atm of H(2)S to [Ru(IMes)(2)(CO)(EtOH)H(2)] (IMes = 1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene) affords the air-stable hydrogen sulfide dihydride complex, [Ru(IMes)(2)(CO)(H(2)S)H(2)] 2. Treatment of 2 with excess H(2)S leads to formation of the 16-electron bis-hydrosulfido complex, [Ru(IMes)(2)(CO)(SH)(2)] 3. Preliminary studies show...

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Chatwin SL, Diggle RA, Jazzar RF, et al. Structure, reactivity, and computational studies of a novel ruthenium hydrogen sulfide dihydride complex. Inorg Chem. 2003;42(24):7695-7doi: 10.1021/ic030241i.
Chatwin, S. L., Diggle, R. A., Jazzar, R. F., Macgregor, S. A., Mahon, M. F., & Whittlesey, M. K. (2003). Structure, reactivity, and computational studies of a novel ruthenium hydrogen sulfide dihydride complex. Inorganic chemistry, 42(24), 7695-7. https://doi.org/10.1021/ic030241i
Chatwin, Sarah L, et al. "Structure, reactivity, and computational studies of a novel ruthenium hydrogen sulfide dihydride complex." Inorganic chemistry vol. 42,24 (2003): 7695-7. doi: https://doi.org/10.1021/ic030241i
Chatwin SL, Diggle RA, Jazzar RF, Macgregor SA, Mahon MF, Whittlesey MK. Structure, reactivity, and computational studies of a novel ruthenium hydrogen sulfide dihydride complex. Inorg Chem. 2003 Dec 01;42(24):7695-7. doi: 10.1021/ic030241i. PMID: 14632475.
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The F/Ph rearrangement reaction of [(Ph3P)3RhF], the fluoride congener of Wilkinson's catalyst.

Journal of the American Chemical Society

Macgregor SA, Roe DC, Marshall WJ, Bloch KM, Bakhmutov VI, Grushin VV.
PMID: 16248673
J Am Chem Soc. 2005 Nov 02;127(43):15304-21. doi: 10.1021/ja054506z.

The fluoride congener of Wilkinson's catalyst, [(Ph(3)P)(3)RhF] (1), has been synthesized and fully characterized. Unlike Wilkinson's catalyst, 1 easily activates the inert C-Cl bond of ArCl (Ar = Ph, p-tolyl) under mild conditions (3 h at 80 degrees C)...

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Macgregor SA, Roe DC, Marshall WJ, et al. The F/Ph rearrangement reaction of [(Ph3P)3RhF], the fluoride congener of Wilkinson's catalyst. J Am Chem Soc. 2005;127(43):15304-21doi: 10.1021/ja054506z.
Macgregor, S. A., Roe, D. C., Marshall, W. J., Bloch, K. M., Bakhmutov, V. I., & Grushin, V. V. (2005). The F/Ph rearrangement reaction of [(Ph3P)3RhF], the fluoride congener of Wilkinson's catalyst. Journal of the American Chemical Society, 127(43), 15304-21. https://doi.org/10.1021/ja054506z
Macgregor, Stuart A, et al. "The F/Ph rearrangement reaction of [(Ph3P)3RhF], the fluoride congener of Wilkinson's catalyst." Journal of the American Chemical Society vol. 127,43 (2005): 15304-21. doi: https://doi.org/10.1021/ja054506z
Macgregor SA, Roe DC, Marshall WJ, Bloch KM, Bakhmutov VI, Grushin VV. The F/Ph rearrangement reaction of [(Ph3P)3RhF], the fluoride congener of Wilkinson's catalyst. J Am Chem Soc. 2005 Nov 02;127(43):15304-21. doi: 10.1021/ja054506z. PMID: 16248673.
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Formation of [Ru(NHC)4(eta(2)-O2)H]+: an unusual, high frequency hydride chemical shift and facile, reversible coordination of O2.

Journal of the American Chemical Society

Häller LJ, Mas-Marzá E, Moreno A, Lowe JP, Macgregor SA, Mahon MF, Pregosin PS, Whittlesey MK.
PMID: 19601678
J Am Chem Soc. 2009 Jul 22;131(28):9618-9. doi: 10.1021/ja9039345.

Reaction of the purple tetrakiscarbene ruthenium cation [Ru(I(i)Pr(2)Me(2))(4)H](+) (1, I(i)Pr(2)Me(2) = 1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene) with oxygen affords the pink eta(2)-O(2) hydride species [Ru(I(i)Pr(2)Me(2))(4)(eta(2)-O(2))H](+) (2). 2 displays (i) a very facile, reversible O(2) coordination and (ii) an unexpectedly positive hydride chemical shift,...

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Häller LJ, Mas-Marzá E, Moreno A, et al. Formation of [Ru(NHC)4(eta(2)-O2)H]+: an unusual, high frequency hydride chemical shift and facile, reversible coordination of O2. J Am Chem Soc. 2009;131(28):9618-9doi: 10.1021/ja9039345.
Häller, L. J., Mas-Marzá, E., Moreno, A., Lowe, J. P., Macgregor, S. A., Mahon, M. F., Pregosin, P. S., & Whittlesey, M. K. (2009). Formation of [Ru(NHC)4(eta(2)-O2)H]+: an unusual, high frequency hydride chemical shift and facile, reversible coordination of O2. Journal of the American Chemical Society, 131(28), 9618-9. https://doi.org/10.1021/ja9039345
Häller, L Jonas L, et al. "Formation of [Ru(NHC)4(eta(2)-O2)H]+: an unusual, high frequency hydride chemical shift and facile, reversible coordination of O2." Journal of the American Chemical Society vol. 131,28 (2009): 9618-9. doi: https://doi.org/10.1021/ja9039345
Häller LJ, Mas-Marzá E, Moreno A, Lowe JP, Macgregor SA, Mahon MF, Pregosin PS, Whittlesey MK. Formation of [Ru(NHC)4(eta(2)-O2)H]+: an unusual, high frequency hydride chemical shift and facile, reversible coordination of O2. J Am Chem Soc. 2009 Jul 22;131(28):9618-9. doi: 10.1021/ja9039345. PMID: 19601678.
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Composting process control based on interaction between microbial heat output and temperature.

Applied and environmental microbiology

Macgregor ST, Miller FC, Psarianos KM, Finstein MS.
PMID: 16345786
Appl Environ Microbiol. 1981 Jun;41(6):1321-30. doi: 10.1128/aem.41.6.1321-1330.1981.

Rational composting process control involves the interrelated factors of heat output, temperature, ventilation, and water removal. The heat is released microbially at the expense of organic material; temperature is an effect and, because it is a determinant of microbial...

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Macgregor ST, Miller FC, Psarianos KM, et al. Composting process control based on interaction between microbial heat output and temperature. Appl Environ Microbiol. 1981;41(6):1321-30doi: 10.1128/aem.41.6.1321-1330.1981.
Macgregor, S. T., Miller, F. C., Psarianos, K. M., & Finstein, M. S. (1981). Composting process control based on interaction between microbial heat output and temperature. Applied and environmental microbiology, 41(6), 1321-30. https://doi.org/10.1128/aem.41.6.1321-1330.1981
Macgregor, S T, et al. "Composting process control based on interaction between microbial heat output and temperature." Applied and environmental microbiology vol. 41,6 (1981): 1321-30. doi: https://doi.org/10.1128/aem.41.6.1321-1330.1981
Macgregor ST, Miller FC, Psarianos KM, Finstein MS. Composting process control based on interaction between microbial heat output and temperature. Appl Environ Microbiol. 1981 Jun;41(6):1321-30. doi: 10.1128/aem.41.6.1321-1330.1981. PMID: 16345786; PMCID: PMC243918.
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Can choices between alternative hip prostheses be evidence based? a review of the economic evaluation literature.

Cost effectiveness and resource allocation : C/E

Davies C, Lorgelly P, Shemilt I, Mugford M, Tucker K, Macgregor A.
PMID: 21034434
Cost Eff Resour Alloc. 2010 Oct 29;8:20. doi: 10.1186/1478-7547-8-20.

BACKGROUND: Total hip replacement surgery places a considerable financial burden on health services and society. Given the large number of hip prostheses available to surgeons, reliable economic evidence is crucial to inform resource allocation decisions. This review summarises published...

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Davies C, Lorgelly P, Shemilt I, et al. Can choices between alternative hip prostheses be evidence based? a review of the economic evaluation literature. Cost Eff Resour Alloc. 2010;8:20doi: 10.1186/1478-7547-8-20.
Davies, C., Lorgelly, P., Shemilt, I., Mugford, M., Tucker, K., & Macgregor, A. (2010). Can choices between alternative hip prostheses be evidence based? a review of the economic evaluation literature. Cost effectiveness and resource allocation : C/E, 820. https://doi.org/10.1186/1478-7547-8-20
Davies, Charlotte, et al. "Can choices between alternative hip prostheses be evidence based? a review of the economic evaluation literature." Cost effectiveness and resource allocation : C/E vol. 8 (2010): 20. doi: https://doi.org/10.1186/1478-7547-8-20
Davies C, Lorgelly P, Shemilt I, Mugford M, Tucker K, Macgregor A. Can choices between alternative hip prostheses be evidence based? a review of the economic evaluation literature. Cost Eff Resour Alloc. 2010 Oct 29;8:20. doi: 10.1186/1478-7547-8-20. PMID: 21034434; PMCID: PMC2984411.
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Showing 1 to 12 of 566 entries