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Coordination of KrF.

Angewandte Chemie (International ed. in English)

Lozinšek M, Mercier HPA, Brock DS, Žemva B, Schrobilgen GJ.
PMID: 28079307
Angew Chem Int Ed Engl. 2017 May 22;56(22):6251-6254. doi: 10.1002/anie.201611534. Epub 2017 Jan 12.

Examples of coordination compounds in which KrF

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Lozinšek M, Mercier HPA, Brock DS, et al. Coordination of KrF. Angew Chem Int Ed Engl. 2017;56(22):6251-6254doi: 10.1002/anie.201611534.
Lozinšek, M., Mercier, H. P. A., Brock, D. S., Žemva, B., & Schrobilgen, G. J. (2017). Coordination of KrF. Angewandte Chemie (International ed. in English), 56(22), 6251-6254. https://doi.org/10.1002/anie.201611534
Lozinšek, Matic, et al. "Coordination of KrF." Angewandte Chemie (International ed. in English) vol. 56,22 (2017): 6251-6254. doi: https://doi.org/10.1002/anie.201611534
Lozinšek M, Mercier HPA, Brock DS, Žemva B, Schrobilgen GJ. Coordination of KrF. Angew Chem Int Ed Engl. 2017 May 22;56(22):6251-6254. doi: 10.1002/anie.201611534. Epub 2017 Jan 12. PMID: 28079307.
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The chemistry of xenon(IV).

Chemical reviews

Haner J, Schrobilgen GJ.
PMID: 25559700
Chem Rev. 2015 Jan 28;115(2):1255-95. doi: 10.1021/cr500427p. Epub 2015 Jan 05.

No abstract available.

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Haner J, Schrobilgen GJ. The chemistry of xenon(IV). Chem Rev. 2015;115(2):1255-95doi: 10.1021/cr500427p.
Haner, J., & Schrobilgen, G. J. (2015). The chemistry of xenon(IV). Chemical reviews, 115(2), 1255-95. https://doi.org/10.1021/cr500427p
Haner, Jamie, and Schrobilgen, Gary J. "The chemistry of xenon(IV)." Chemical reviews vol. 115,2 (2015): 1255-95. doi: https://doi.org/10.1021/cr500427p
Haner J, Schrobilgen GJ. The chemistry of xenon(IV). Chem Rev. 2015 Jan 28;115(2):1255-95. doi: 10.1021/cr500427p. Epub 2015 Jan 05. PMID: 25559700.
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Syntheses and Structures of Xenon Trioxide Alkylnitrile Adducts.

Angewandte Chemie (International ed. in English)

Goettel JT, Matsumoto K, Mercier HP, Schrobilgen GJ.
PMID: 27689342
Angew Chem Int Ed Engl. 2016 Oct 24;55(44):13780-13783. doi: 10.1002/anie.201607583. Epub 2016 Sep 30.

The potent oxidizer and highly shock-sensitive binary noble-gas oxide XeO

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Goettel JT, Matsumoto K, Mercier HP, et al. Syntheses and Structures of Xenon Trioxide Alkylnitrile Adducts. Angew Chem Int Ed Engl. 2016;55(44):13780-13783doi: 10.1002/anie.201607583.
Goettel, J. T., Matsumoto, K., Mercier, H. P., & Schrobilgen, G. J. (2016). Syntheses and Structures of Xenon Trioxide Alkylnitrile Adducts. Angewandte Chemie (International ed. in English), 55(44), 13780-13783. https://doi.org/10.1002/anie.201607583
Goettel, James T, et al. "Syntheses and Structures of Xenon Trioxide Alkylnitrile Adducts." Angewandte Chemie (International ed. in English) vol. 55,44 (2016): 13780-13783. doi: https://doi.org/10.1002/anie.201607583
Goettel JT, Matsumoto K, Mercier HP, Schrobilgen GJ. Syntheses and Structures of Xenon Trioxide Alkylnitrile Adducts. Angew Chem Int Ed Engl. 2016 Oct 24;55(44):13780-13783. doi: 10.1002/anie.201607583. Epub 2016 Sep 30. PMID: 27689342.
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Trigonal Bipyramidal M(2)Ch(3)(2)(-) (M = Sn, Pb; Ch = S, Se, Te) and TlMTe(3)(3)(-) Anions: Multinuclear Magnetic Resonance, Raman Spectroscopic, and Theoretical Studies, and the X-ray Crystal Structures of (2,2,2-crypt-K(+))(3)TlPbTe(3)(3)(-).2en and (2,2,2-crypt-K(+))(2)Pb(2)Ch(3)(2)(-).0.5en (Ch = S, Se).

Inorganic chemistry

Borrmann H, Campbell J, Dixon DA, Mercier HP, Pirani AM, Schrobilgen GJ.
PMID: 11670797
Inorg Chem. 1998 Dec 28;37(26):6656-6674. doi: 10.1021/ic980574t.

The series of group 14 metal trigonal bipyramidal anions has been extended to the mixed group 13/group 14 metal TlMTe(3)(3)(-) anions (M = Sn, Pb), obtained by the reaction of Tl(2)M(2)Te(3) and K(2)Te in en or in en/ethylamine mixtures...

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Borrmann H, Campbell J, Dixon DA, et al. Trigonal Bipyramidal M(2)Ch(3)(2)(-) (M = Sn, Pb; Ch = S, Se, Te) and TlMTe(3)(3)(-) Anions: Multinuclear Magnetic Resonance, Raman Spectroscopic, and Theoretical Studies, and the X-ray Crystal Structures of (2,2,2-crypt-K(+))(3)TlPbTe(3)(3)(-).2en and (2,2,2-crypt-K(+))(2)Pb(2)Ch(3)(2)(-).0.5en (Ch = S, Se). Inorg Chem. 1998;37(26):6656-6674doi: 10.1021/ic980574t.
Borrmann, H., Campbell, J., Dixon, D. A., Mercier, H. P., Pirani, A. M., & Schrobilgen, G. J. (1998). Trigonal Bipyramidal M(2)Ch(3)(2)(-) (M = Sn, Pb; Ch = S, Se, Te) and TlMTe(3)(3)(-) Anions: Multinuclear Magnetic Resonance, Raman Spectroscopic, and Theoretical Studies, and the X-ray Crystal Structures of (2,2,2-crypt-K(+))(3)TlPbTe(3)(3)(-).2en and (2,2,2-crypt-K(+))(2)Pb(2)Ch(3)(2)(-).0.5en (Ch = S, Se). Inorganic chemistry, 37(26), 6656-6674. https://doi.org/10.1021/ic980574t
Borrmann, Horst, et al. "Trigonal Bipyramidal M(2)Ch(3)(2)(-) (M = Sn, Pb; Ch = S, Se, Te) and TlMTe(3)(3)(-) Anions: Multinuclear Magnetic Resonance, Raman Spectroscopic, and Theoretical Studies, and the X-ray Crystal Structures of (2,2,2-crypt-K(+))(3)TlPbTe(3)(3)(-).2en and (2,2,2-crypt-K(+))(2)Pb(2)Ch(3)(2)(-).0.5en (Ch = S, Se)." Inorganic chemistry vol. 37,26 (1998): 6656-6674. doi: https://doi.org/10.1021/ic980574t
Borrmann H, Campbell J, Dixon DA, Mercier HP, Pirani AM, Schrobilgen GJ. Trigonal Bipyramidal M(2)Ch(3)(2)(-) (M = Sn, Pb; Ch = S, Se, Te) and TlMTe(3)(3)(-) Anions: Multinuclear Magnetic Resonance, Raman Spectroscopic, and Theoretical Studies, and the X-ray Crystal Structures of (2,2,2-crypt-K(+))(3)TlPbTe(3)(3)(-).2en and (2,2,2-crypt-K(+))(2)Pb(2)Ch(3)(2)(-).0.5en (Ch = S, Se). Inorg Chem. 1998 Dec 28;37(26):6656-6674. doi: 10.1021/ic980574t. PMID: 11670797.
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Synthesis, characterization, and computational study of the trans-IO2F5(2-) anion.

Inorganic chemistry

Boatz JA, Christe KO, Dixon DA, Fir BA, Gerken M, Gnann RZ, Mercier HP, Schrobilgen GJ.
PMID: 12924900
Inorg Chem. 2003 Aug 25;42(17):5282-92. doi: 10.1021/ic034457w.

The combination of CH(3)CN solutions of [N(CH(3))(4)][F] and a mixture of cis- and trans-[N(CH(3))(4)][IO(2)F(4)] produces the novel trans-IO(2)F(5)(2)(-) anion. Under the given conditions, only the trans-IO(2)F(4)(-) anion acts as a fluoride ion acceptor, thus allowing the separation of isomerically...

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Boatz JA, Christe KO, Dixon DA, et al. Synthesis, characterization, and computational study of the trans-IO2F5(2-) anion. Inorg Chem. 2003;42(17):5282-92doi: 10.1021/ic034457w.
Boatz, J. A., Christe, K. O., Dixon, D. A., Fir, B. A., Gerken, M., Gnann, R. Z., Mercier, H. P., & Schrobilgen, G. J. (2003). Synthesis, characterization, and computational study of the trans-IO2F5(2-) anion. Inorganic chemistry, 42(17), 5282-92. https://doi.org/10.1021/ic034457w
Boatz, Jerry A, et al. "Synthesis, characterization, and computational study of the trans-IO2F5(2-) anion." Inorganic chemistry vol. 42,17 (2003): 5282-92. doi: https://doi.org/10.1021/ic034457w
Boatz JA, Christe KO, Dixon DA, Fir BA, Gerken M, Gnann RZ, Mercier HP, Schrobilgen GJ. Synthesis, characterization, and computational study of the trans-IO2F5(2-) anion. Inorg Chem. 2003 Aug 25;42(17):5282-92. doi: 10.1021/ic034457w. PMID: 12924900.
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On the XeF+/H2O system: synthesis and characterization of the xenon(II) oxide fluoride cation, FXeOXeFXeF+.

Journal of the American Chemical Society

Gerken M, Moran MD, Mercier HP, Pointner BE, Schrobilgen GJ, Hoge B, Christe KO, Boatz JA.
PMID: 19708668
J Am Chem Soc. 2009 Sep 23;131(37):13474-89. doi: 10.1021/ja905060v.

The reported synthesis of the H(2)OF(+) cation as a product of the oxidative fluorination of H(2)O by [XeF][PnF(6)] (Pn = As, Sb) in HF solution has been reinvestigated. The system exhibits complex equilibria, producing two new Xe(II) compounds, [Xe(3)OF(3)][PnF(6)]...

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Gerken M, Moran MD, Mercier HP, et al. On the XeF+/H2O system: synthesis and characterization of the xenon(II) oxide fluoride cation, FXeOXeFXeF+. J Am Chem Soc. 2009;131(37):13474-89doi: 10.1021/ja905060v.
Gerken, M., Moran, M. D., Mercier, H. P., Pointner, B. E., Schrobilgen, G. J., Hoge, B., Christe, K. O., & Boatz, J. A. (2009). On the XeF+/H2O system: synthesis and characterization of the xenon(II) oxide fluoride cation, FXeOXeFXeF+. Journal of the American Chemical Society, 131(37), 13474-89. https://doi.org/10.1021/ja905060v
Gerken, Michael, et al. "On the XeF+/H2O system: synthesis and characterization of the xenon(II) oxide fluoride cation, FXeOXeFXeF+." Journal of the American Chemical Society vol. 131,37 (2009): 13474-89. doi: https://doi.org/10.1021/ja905060v
Gerken M, Moran MD, Mercier HP, Pointner BE, Schrobilgen GJ, Hoge B, Christe KO, Boatz JA. On the XeF+/H2O system: synthesis and characterization of the xenon(II) oxide fluoride cation, FXeOXeFXeF+. J Am Chem Soc. 2009 Sep 23;131(37):13474-89. doi: 10.1021/ja905060v. PMID: 19708668.
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The ionic isomegethic rule and additivity relationships: estimation of ion volumes. A route to the energetics and entropics of new, traditional, hypothetical, and counterintuitive ionic materials.

Inorganic chemistry

Jenkins HD, Glasser L, Klapötke TM, Crawford MJ, Bhasin KK, Lee J, Schrobilgen GJ, Sunderlin LS, Liebman JF.
PMID: 15446869
Inorg Chem. 2004 Oct 04;43(20):6238-48. doi: 10.1021/ic049186j.

By virtue of our recently established relationships, knowledge of the formula unit volume, V(m), of a solid ionic material permits estimation of thermodynamic properties such as standard entropy, lattice potential energy, and, hence, enthalpy and Gibbs energy changes for...

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Jenkins HD, Glasser L, Klapötke TM, et al. The ionic isomegethic rule and additivity relationships: estimation of ion volumes. A route to the energetics and entropics of new, traditional, hypothetical, and counterintuitive ionic materials. Inorg Chem. 2004;43(20):6238-48doi: 10.1021/ic049186j.
Jenkins, H. D., Glasser, L., Klapötke, T. M., Crawford, M. J., Bhasin, K. K., Lee, J., Schrobilgen, G. J., Sunderlin, L. S., & Liebman, J. F. (2004). The ionic isomegethic rule and additivity relationships: estimation of ion volumes. A route to the energetics and entropics of new, traditional, hypothetical, and counterintuitive ionic materials. Inorganic chemistry, 43(20), 6238-48. https://doi.org/10.1021/ic049186j
Jenkins, H Donald Brooke, et al. "The ionic isomegethic rule and additivity relationships: estimation of ion volumes. A route to the energetics and entropics of new, traditional, hypothetical, and counterintuitive ionic materials." Inorganic chemistry vol. 43,20 (2004): 6238-48. doi: https://doi.org/10.1021/ic049186j
Jenkins HD, Glasser L, Klapötke TM, Crawford MJ, Bhasin KK, Lee J, Schrobilgen GJ, Sunderlin LS, Liebman JF. The ionic isomegethic rule and additivity relationships: estimation of ion volumes. A route to the energetics and entropics of new, traditional, hypothetical, and counterintuitive ionic materials. Inorg Chem. 2004 Oct 04;43(20):6238-48. doi: 10.1021/ic049186j. PMID: 15446869.
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XeOF2, F2OXeN identical with CCH3, and XeOF2.nHF: rare examples of Xe(IV) oxide fluorides.

Journal of the American Chemical Society

Brock DS, Bilir V, Mercier HP, Schrobilgen GJ.
PMID: 17335282
J Am Chem Soc. 2007 Mar 28;129(12):3598-611. doi: 10.1021/ja0673480. Epub 2007 Mar 03.

The syntheses of XeOF2, F2OXeNCCH3, and XeOF2.nHF and their structural characterizations are described in this study. All three compounds are explosive at temperatures approaching 0 degrees C. Although XeOF2 had been previously reported, it had not been isolated as...

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Brock DS, Bilir V, Mercier HP, et al. XeOF2, F2OXeN identical with CCH3, and XeOF2.nHF: rare examples of Xe(IV) oxide fluorides. J Am Chem Soc. 2007;129(12):3598-611doi: 10.1021/ja0673480.
Brock, D. S., Bilir, V., Mercier, H. P., & Schrobilgen, G. J. (2007). XeOF2, F2OXeN identical with CCH3, and XeOF2.nHF: rare examples of Xe(IV) oxide fluorides. Journal of the American Chemical Society, 129(12), 3598-611. https://doi.org/10.1021/ja0673480
Brock, David S, et al. "XeOF2, F2OXeN identical with CCH3, and XeOF2.nHF: rare examples of Xe(IV) oxide fluorides." Journal of the American Chemical Society vol. 129,12 (2007): 3598-611. doi: https://doi.org/10.1021/ja0673480
Brock DS, Bilir V, Mercier HP, Schrobilgen GJ. XeOF2, F2OXeN identical with CCH3, and XeOF2.nHF: rare examples of Xe(IV) oxide fluorides. J Am Chem Soc. 2007 Mar 28;129(12):3598-611. doi: 10.1021/ja0673480. Epub 2007 Mar 03. PMID: 17335282.
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A rare example of a krypton difluoride coordination compound: [BrOF2][AsF6] x 2 KrF2.

Journal of the American Chemical Society

Brock DS, de Pury JJ, Mercier HP, Schrobilgen GJ, Silvi B.
PMID: 20170204
J Am Chem Soc. 2010 Mar 17;132(10):3533-42. doi: 10.1021/ja9098559.

The synthesis of [BrOF(2)][AsF(6)] x 2 KrF(2), its structural characterization, and bonding are described in this study. Although several KrF(2) adducts with transition metal centers have been previously reported, none have been crystallographically characterized. The solid-state Raman spectrum of...

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Brock DS, de Pury JJ, Mercier HP, et al. A rare example of a krypton difluoride coordination compound: [BrOF2][AsF6] x 2 KrF2. J Am Chem Soc. 2010;132(10):3533-42doi: 10.1021/ja9098559.
Brock, D. S., de Pury, J. J., Mercier, H. P., Schrobilgen, G. J., & Silvi, B. (2010). A rare example of a krypton difluoride coordination compound: [BrOF2][AsF6] x 2 KrF2. Journal of the American Chemical Society, 132(10), 3533-42. https://doi.org/10.1021/ja9098559
Brock, David S, et al. "A rare example of a krypton difluoride coordination compound: [BrOF2][AsF6] x 2 KrF2." Journal of the American Chemical Society vol. 132,10 (2010): 3533-42. doi: https://doi.org/10.1021/ja9098559
Brock DS, de Pury JJ, Mercier HP, Schrobilgen GJ, Silvi B. A rare example of a krypton difluoride coordination compound: [BrOF2][AsF6] x 2 KrF2. J Am Chem Soc. 2010 Mar 17;132(10):3533-42. doi: 10.1021/ja9098559. PMID: 20170204.
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Syntheses and X-ray crystal structures of alpha- and beta-[XeO2F][SbF6], [XeO2F][AsF6], [FO2XeFXeO2F][AsF6], and [XeF5][SbF6)].XeOF4 and computational studies of the XeO2F+ and FO2XeFXeO2F+ cations and related species.

Inorganic chemistry

Pointner BE, Suontamo RJ, Schrobilgen GJ.
PMID: 16471963
Inorg Chem. 2006 Feb 20;45(4):1517-34. doi: 10.1021/ic0510260.

Reactions of XeO2F2 with the strong fluoride ion acceptors, AsF5 and SbF5, in anhydrous HF solvent give rise to alpha- and beta-[XeO2F][SbF6], [XeO2F][AsF6], and [FO2XeFXeO2F][AsF6]. The crystal structures of alpha-[XeO2F][SbF6] and [XeO2F][AsF6] consist of trigonal-pyramidal XeO2F+ cations, which are...

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Pointner BE, Suontamo RJ, Schrobilgen GJ. Syntheses and X-ray crystal structures of alpha- and beta-[XeO2F][SbF6], [XeO2F][AsF6], [FO2XeFXeO2F][AsF6], and [XeF5][SbF6)].XeOF4 and computational studies of the XeO2F+ and FO2XeFXeO2F+ cations and related species. Inorg Chem. 2006;45(4):1517-34doi: 10.1021/ic0510260.
Pointner, B. E., Suontamo, R. J., & Schrobilgen, G. J. (2006). Syntheses and X-ray crystal structures of alpha- and beta-[XeO2F][SbF6], [XeO2F][AsF6], [FO2XeFXeO2F][AsF6], and [XeF5][SbF6)].XeOF4 and computational studies of the XeO2F+ and FO2XeFXeO2F+ cations and related species. Inorganic chemistry, 45(4), 1517-34. https://doi.org/10.1021/ic0510260
Pointner, Bernard E, et al. "Syntheses and X-ray crystal structures of alpha- and beta-[XeO2F][SbF6], [XeO2F][AsF6], [FO2XeFXeO2F][AsF6], and [XeF5][SbF6)].XeOF4 and computational studies of the XeO2F+ and FO2XeFXeO2F+ cations and related species." Inorganic chemistry vol. 45,4 (2006): 1517-34. doi: https://doi.org/10.1021/ic0510260
Pointner BE, Suontamo RJ, Schrobilgen GJ. Syntheses and X-ray crystal structures of alpha- and beta-[XeO2F][SbF6], [XeO2F][AsF6], [FO2XeFXeO2F][AsF6], and [XeF5][SbF6)].XeOF4 and computational studies of the XeO2F+ and FO2XeFXeO2F+ cations and related species. Inorg Chem. 2006 Feb 20;45(4):1517-34. doi: 10.1021/ic0510260. PMID: 16471963.
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On the reactivity of F(3)S[triple bond]NXeF(+): syntheses and structural characterizations of [F(4)S=N-Xe---N[triple bond]SF(3)][AsF(6)], a rare example of a N-Xe-N linkage, and [F(3)S(N[triple bond]SF(3))(2)][AsF(6)].

Inorganic chemistry

Smith GL, Schrobilgen GJ.
PMID: 19621882
Inorg Chem. 2009 Aug 17;48(16):7714-28. doi: 10.1021/ic900651n.

The F(4)S=N-Xe---N[triple bond]SF(3)(+) cation has been synthesized as the AsF(6)(-) salt by rearrangement of [F(3)S[triple bond]NXeF][AsF(6)] in N[triple bond]SF(3) solvent at 0 degrees C. Deep yellow [F(4)S=N-Xe---N[triple bond]SF(3)][AsF(6)], which crystallized from a N[triple bond]SF(3) solution at -10 degrees C,...

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Smith GL, Schrobilgen GJ. On the reactivity of F(3)S[triple bond]NXeF(+): syntheses and structural characterizations of [F(4)S=N-Xe---N[triple bond]SF(3)][AsF(6)], a rare example of a N-Xe-N linkage, and [F(3)S(N[triple bond]SF(3))(2)][AsF(6)]. Inorg Chem. 2009;48(16):7714-28doi: 10.1021/ic900651n.
Smith, G. L., & Schrobilgen, G. J. (2009). On the reactivity of F(3)S[triple bond]NXeF(+): syntheses and structural characterizations of [F(4)S=N-Xe---N[triple bond]SF(3)][AsF(6)], a rare example of a N-Xe-N linkage, and [F(3)S(N[triple bond]SF(3))(2)][AsF(6)]. Inorganic chemistry, 48(16), 7714-28. https://doi.org/10.1021/ic900651n
Smith, Gregory L, and Schrobilgen, Gary J. "On the reactivity of F(3)S[triple bond]NXeF(+): syntheses and structural characterizations of [F(4)S=N-Xe---N[triple bond]SF(3)][AsF(6)], a rare example of a N-Xe-N linkage, and [F(3)S(N[triple bond]SF(3))(2)][AsF(6)]." Inorganic chemistry vol. 48,16 (2009): 7714-28. doi: https://doi.org/10.1021/ic900651n
Smith GL, Schrobilgen GJ. On the reactivity of F(3)S[triple bond]NXeF(+): syntheses and structural characterizations of [F(4)S=N-Xe---N[triple bond]SF(3)][AsF(6)], a rare example of a N-Xe-N linkage, and [F(3)S(N[triple bond]SF(3))(2)][AsF(6)]. Inorg Chem. 2009 Aug 17;48(16):7714-28. doi: 10.1021/ic900651n. PMID: 19621882.
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Chromium Oxide Tetrafluoride and Its Reactions with Xenon Hexafluoride; the [XeF.

Chemistry (Weinheim an der Bergstrasse, Germany)

Goettel JT, Bortolus MR, Stuart DG, Mercier HPA, Schrobilgen GJ.
PMID: 31437313
Chemistry. 2019 Dec 10;25(69):15815-15829. doi: 10.1002/chem.201903135. Epub 2019 Nov 14.

Molten mixtures of XeF

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Goettel JT, Bortolus MR, Stuart DG, et al. Chromium Oxide Tetrafluoride and Its Reactions with Xenon Hexafluoride; the [XeF. Chemistry. 2019;25(69):15815-15829doi: 10.1002/chem.201903135.
Goettel, J. T., Bortolus, M. R., Stuart, D. G., Mercier, H. P. A., & Schrobilgen, G. J. (2019). Chromium Oxide Tetrafluoride and Its Reactions with Xenon Hexafluoride; the [XeF. Chemistry (Weinheim an der Bergstrasse, Germany), 25(69), 15815-15829. https://doi.org/10.1002/chem.201903135
Goettel, James T, et al. "Chromium Oxide Tetrafluoride and Its Reactions with Xenon Hexafluoride; the [XeF." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 25,69 (2019): 15815-15829. doi: https://doi.org/10.1002/chem.201903135
Goettel JT, Bortolus MR, Stuart DG, Mercier HPA, Schrobilgen GJ. Chromium Oxide Tetrafluoride and Its Reactions with Xenon Hexafluoride; the [XeF. Chemistry. 2019 Dec 10;25(69):15815-15829. doi: 10.1002/chem.201903135. Epub 2019 Nov 14. PMID: 31437313.
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