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Structure and Reactivity of X-ray Amorphous Uranyl Peroxide, U2O7.

Inorganic chemistry

Odoh SO, Shamblin J, Colla CA, Hickam S, Lobeck HL, Lopez RA, Olds T, Szymanowski JE, Sigmon GE, Neuefeind J, Casey WH, Lang M, Gagliardi L, Burns PC.
PMID: 26974702
Inorg Chem. 2016 Apr 04;55(7):3541-6. doi: 10.1021/acs.inorgchem.6b00017. Epub 2016 Mar 14.

Recent accidents resulting in worker injury and radioactive contamination occurred due to pressurization of uranium yellowcake drums produced in the western U.S.A. The drums contained an X-ray amorphous reactive form of uranium oxide that may have contributed to the...

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Odoh SO, Shamblin J, Colla CA, et al. Structure and Reactivity of X-ray Amorphous Uranyl Peroxide, U2O7. Inorg Chem. 2016;55(7):3541-6doi: 10.1021/acs.inorgchem.6b00017.
Odoh, S. O., Shamblin, J., Colla, C. A., Hickam, S., Lobeck, H. L., Lopez, R. A., Olds, T., Szymanowski, J. E., Sigmon, G. E., Neuefeind, J., Casey, W. H., Lang, M., Gagliardi, L., & Burns, P. C. (2016). Structure and Reactivity of X-ray Amorphous Uranyl Peroxide, U2O7. Inorganic chemistry, 55(7), 3541-6. https://doi.org/10.1021/acs.inorgchem.6b00017
Odoh, Samuel O, et al. "Structure and Reactivity of X-ray Amorphous Uranyl Peroxide, U2O7." Inorganic chemistry vol. 55,7 (2016): 3541-6. doi: https://doi.org/10.1021/acs.inorgchem.6b00017
Odoh SO, Shamblin J, Colla CA, Hickam S, Lobeck HL, Lopez RA, Olds T, Szymanowski JE, Sigmon GE, Neuefeind J, Casey WH, Lang M, Gagliardi L, Burns PC. Structure and Reactivity of X-ray Amorphous Uranyl Peroxide, U2O7. Inorg Chem. 2016 Apr 04;55(7):3541-6. doi: 10.1021/acs.inorgchem.6b00017. Epub 2016 Mar 14. PMID: 26974702.
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Hybrid uranyl-vanadium nano-wheels.

Chemical communications (Cambridge, England)

Senchyk GA, Wylie EM, Prizio S, Szymanowski JE, Sigmon GE, Burns PC.
PMID: 26008125
Chem Commun (Camb). 2015 Jun 25;51(50):10134-7. doi: 10.1039/c5cc01524c.

Hybrid uranyl-vanadium oxide clusters intermediate between transition metal polyoxometalates and uranyl peroxide cage clusters were obtained by dissolving uranyl nitrate in the ionic liquid 3-ethyl-1-methylimidazolium ethyl sulfate mixed with an aqueous solution containing vanadium. Where sulfate was present, wheel-shaped...

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Senchyk GA, Wylie EM, Prizio S, et al. Hybrid uranyl-vanadium nano-wheels. Chem Commun (Camb). 2015;51(50):10134-7doi: 10.1039/c5cc01524c.
Senchyk, G. A., Wylie, E. M., Prizio, S., Szymanowski, J. E., Sigmon, G. E., & Burns, P. C. (2015). Hybrid uranyl-vanadium nano-wheels. Chemical communications (Cambridge, England), 51(50), 10134-7. https://doi.org/10.1039/c5cc01524c
Senchyk, G A, et al. "Hybrid uranyl-vanadium nano-wheels." Chemical communications (Cambridge, England) vol. 51,50 (2015): 10134-7. doi: https://doi.org/10.1039/c5cc01524c
Senchyk GA, Wylie EM, Prizio S, Szymanowski JE, Sigmon GE, Burns PC. Hybrid uranyl-vanadium nano-wheels. Chem Commun (Camb). 2015 Jun 25;51(50):10134-7. doi: 10.1039/c5cc01524c. PMID: 26008125.
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Separation of phenols from aqueous micellar solutions by cloud point extraction.

Journal of colloid and interface science

Materna K, Szymanowski J.
PMID: 12702385
J Colloid Interface Sci. 2002 Nov 01;255(1):195-201. doi: 10.1006/jcis.2002.8613.

The cloud point technique was used to recover phenol, 4-methylphenol, and 4-nitrophenol from aqueous solutions using oxyethylated methyl dodecanoates as nonionic surfactants. Oxyethylated methyl dodecanoates are convenient nonionic surfactants for such separations. Their cloud points can be easily modified...

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Materna K, Szymanowski J. Separation of phenols from aqueous micellar solutions by cloud point extraction. J Colloid Interface Sci. 2002;255(1):195-201doi: 10.1006/jcis.2002.8613.
Materna, K., & Szymanowski, J. (2002). Separation of phenols from aqueous micellar solutions by cloud point extraction. Journal of colloid and interface science, 255(1), 195-201. https://doi.org/10.1006/jcis.2002.8613
Materna, K, and Szymanowski, J. "Separation of phenols from aqueous micellar solutions by cloud point extraction." Journal of colloid and interface science vol. 255,1 (2002): 195-201. doi: https://doi.org/10.1006/jcis.2002.8613
Materna K, Szymanowski J. Separation of phenols from aqueous micellar solutions by cloud point extraction. J Colloid Interface Sci. 2002 Nov 01;255(1):195-201. doi: 10.1006/jcis.2002.8613. PMID: 12702385.
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Hybrid uranium-oxalate fullerene topology cage clusters.

Angewandte Chemie (International ed. in English)

Ling J, Wallace CM, Szymanowski JE, Burns PC.
PMID: 20740514
Angew Chem Int Ed Engl. 2010 Sep 24;49(40):7271-3. doi: 10.1002/anie.201003197.

No abstract available.

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Ling J, Wallace CM, Szymanowski JE, et al. Hybrid uranium-oxalate fullerene topology cage clusters. Angew Chem Int Ed Engl. 2010;49(40):7271-3doi: 10.1002/anie.201003197.
Ling, J., Wallace, C. M., Szymanowski, J. E., & Burns, P. C. (2010). Hybrid uranium-oxalate fullerene topology cage clusters. Angewandte Chemie (International ed. in English), 49(40), 7271-3. https://doi.org/10.1002/anie.201003197
Ling, Jie, et al. "Hybrid uranium-oxalate fullerene topology cage clusters." Angewandte Chemie (International ed. in English) vol. 49,40 (2010): 7271-3. doi: https://doi.org/10.1002/anie.201003197
Ling J, Wallace CM, Szymanowski JE, Burns PC. Hybrid uranium-oxalate fullerene topology cage clusters. Angew Chem Int Ed Engl. 2010 Sep 24;49(40):7271-3. doi: 10.1002/anie.201003197. PMID: 20740514.
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Low-symmetry uranyl pyrophosphate cage clusters.

Chemistry (Weinheim an der Bergstrasse, Germany)

Ling J, Qiu J, Szymanowski JE, Burns PC.
PMID: 21280110
Chemistry. 2011 Feb 25;17(9):2571-4. doi: 10.1002/chem.201003481. Epub 2011 Jan 30.

No abstract available.

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Ling J, Qiu J, Szymanowski JE, et al. Low-symmetry uranyl pyrophosphate cage clusters. Chemistry. 2011;17(9):2571-4doi: 10.1002/chem.201003481.
Ling, J., Qiu, J., Szymanowski, J. E., & Burns, P. C. (2011). Low-symmetry uranyl pyrophosphate cage clusters. Chemistry (Weinheim an der Bergstrasse, Germany), 17(9), 2571-4. https://doi.org/10.1002/chem.201003481
Ling, Jie, et al. "Low-symmetry uranyl pyrophosphate cage clusters." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 17,9 (2011): 2571-4. doi: https://doi.org/10.1002/chem.201003481
Ling J, Qiu J, Szymanowski JE, Burns PC. Low-symmetry uranyl pyrophosphate cage clusters. Chemistry. 2011 Feb 25;17(9):2571-4. doi: 10.1002/chem.201003481. Epub 2011 Jan 30. PMID: 21280110.
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Expanding the Schulze-Hardy Rule and the Hofmeister Series to Nanometer-Scaled Hydrophilic Macroions.

Chemistry (Weinheim an der Bergstrasse, Germany)

Chu Y, Chen J, Haso F, Gao Y, Szymanowski JES, Burns PC, Liu T.
PMID: 29582490
Chemistry. 2018 Apr 11;24(21):5479-5483. doi: 10.1002/chem.201706101. Epub 2018 Mar 26.

The Schulze-Hardy rule is a well-established observation in colloid science (can be derived from the DLVO theory) that demonstrates the relationship between the critical coagulation concentration (CCC) of colloids and the valence of extra counterionic electrolytes (z), with a...

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Chu Y, Chen J, Haso F, et al. Expanding the Schulze-Hardy Rule and the Hofmeister Series to Nanometer-Scaled Hydrophilic Macroions. Chemistry. 2018;24(21):5479-5483doi: 10.1002/chem.201706101.
Chu, Y., Chen, J., Haso, F., Gao, Y., Szymanowski, J. E. S., Burns, P. C., & Liu, T. (2018). Expanding the Schulze-Hardy Rule and the Hofmeister Series to Nanometer-Scaled Hydrophilic Macroions. Chemistry (Weinheim an der Bergstrasse, Germany), 24(21), 5479-5483. https://doi.org/10.1002/chem.201706101
Chu, Yang, et al. "Expanding the Schulze-Hardy Rule and the Hofmeister Series to Nanometer-Scaled Hydrophilic Macroions." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 24,21 (2018): 5479-5483. doi: https://doi.org/10.1002/chem.201706101
Chu Y, Chen J, Haso F, Gao Y, Szymanowski JES, Burns PC, Liu T. Expanding the Schulze-Hardy Rule and the Hofmeister Series to Nanometer-Scaled Hydrophilic Macroions. Chemistry. 2018 Apr 11;24(21):5479-5483. doi: 10.1002/chem.201706101. Epub 2018 Mar 26. PMID: 29582490.
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Sulfate-Centered Sodium-Icosahedron-Templated Uranyl Peroxide Phosphate Cages with Uranyl Bridged by μ-η.

Inorganic chemistry

Qiu J, Spano TL, Dembowski M, Kokot AM, Szymanowski JE, Burns PC.
PMID: 28134511
Inorg Chem. 2017 Feb 20;56(4):1874-1880. doi: 10.1021/acs.inorgchem.6b02429. Epub 2017 Jan 30.

Two novel hybrid uranyl peroxide phosphate cage clusters, designated U

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Qiu J, Spano TL, Dembowski M, et al. Sulfate-Centered Sodium-Icosahedron-Templated Uranyl Peroxide Phosphate Cages with Uranyl Bridged by μ-η. Inorg Chem. 2017;56(4):1874-1880doi: 10.1021/acs.inorgchem.6b02429.
Qiu, J., Spano, T. L., Dembowski, M., Kokot, A. M., Szymanowski, J. E., & Burns, P. C. (2017). Sulfate-Centered Sodium-Icosahedron-Templated Uranyl Peroxide Phosphate Cages with Uranyl Bridged by μ-η. Inorganic chemistry, 56(4), 1874-1880. https://doi.org/10.1021/acs.inorgchem.6b02429
Qiu, Jie, et al. "Sulfate-Centered Sodium-Icosahedron-Templated Uranyl Peroxide Phosphate Cages with Uranyl Bridged by μ-η." Inorganic chemistry vol. 56,4 (2017): 1874-1880. doi: https://doi.org/10.1021/acs.inorgchem.6b02429
Qiu J, Spano TL, Dembowski M, Kokot AM, Szymanowski JE, Burns PC. Sulfate-Centered Sodium-Icosahedron-Templated Uranyl Peroxide Phosphate Cages with Uranyl Bridged by μ-η. Inorg Chem. 2017 Feb 20;56(4):1874-1880. doi: 10.1021/acs.inorgchem.6b02429. Epub 2017 Jan 30. PMID: 28134511.
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Hybrid Lanthanide-Actinide Peroxide Cage Clusters.

Inorganic chemistry

Sigmon GE, Szymanowski JE, Carter KP, Cahill CL, Burns PC.
PMID: 26923457
Inorg Chem. 2016 Mar 21;55(6):2682-4. doi: 10.1021/acs.inorgchem.6b00207. Epub 2016 Feb 29.

A cage cluster consisting of 31 uranyl and 9 Sm(3+) polyhedra self-assembles in an alkaline aqueous peroxide solution and crystallizes (U31Sm9). Trimers of Sm(3+) polyhedra are templated by μ3-η(2):η(2):η(2)-peroxide groups and link to oxo atoms of uranyl ions. Three...

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Sigmon GE, Szymanowski JE, Carter KP, et al. Hybrid Lanthanide-Actinide Peroxide Cage Clusters. Inorg Chem. 2016;55(6):2682-4doi: 10.1021/acs.inorgchem.6b00207.
Sigmon, G. E., Szymanowski, J. E., Carter, K. P., Cahill, C. L., & Burns, P. C. (2016). Hybrid Lanthanide-Actinide Peroxide Cage Clusters. Inorganic chemistry, 55(6), 2682-4. https://doi.org/10.1021/acs.inorgchem.6b00207
Sigmon, Ginger E, et al. "Hybrid Lanthanide-Actinide Peroxide Cage Clusters." Inorganic chemistry vol. 55,6 (2016): 2682-4. doi: https://doi.org/10.1021/acs.inorgchem.6b00207
Sigmon GE, Szymanowski JE, Carter KP, Cahill CL, Burns PC. Hybrid Lanthanide-Actinide Peroxide Cage Clusters. Inorg Chem. 2016 Mar 21;55(6):2682-4. doi: 10.1021/acs.inorgchem.6b00207. Epub 2016 Feb 29. PMID: 26923457.
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FLUKA Simulations of .

Materials (Basel, Switzerland)

Gójska AM, Kozioł K, Wasilewski A, Miśta-Jakubowska EA, Mazerewicz P, Szymanowski J.
PMID: 34442984
Materials (Basel). 2021 Aug 09;14(16). doi: 10.3390/ma14164462.

The numerical simulations of Cu Kα and Cu Kβ fluorescence lines induced by Rh X-ray tube and by monoenergetic radiation have been presented. The copper Kβ/Kα intensity ratios for pure elements as well as for Ag-Cu alloys have been...

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Gójska AM, Kozioł K, Wasilewski A, et al. FLUKA Simulations of . Materials (Basel). 2021;14(16)doi: 10.3390/ma14164462.
Gójska, A. M., Kozioł, K., Wasilewski, A., Miśta-Jakubowska, E. A., Mazerewicz, P., & Szymanowski, J. (2021). FLUKA Simulations of . Materials (Basel, Switzerland), 14(16), . https://doi.org/10.3390/ma14164462
Gójska, Aneta Maria, et al. "FLUKA Simulations of ." Materials (Basel, Switzerland) vol. 14,16 (2021). doi: https://doi.org/10.3390/ma14164462
Gójska AM, Kozioł K, Wasilewski A, Miśta-Jakubowska EA, Mazerewicz P, Szymanowski J. FLUKA Simulations of . Materials (Basel). 2021 Aug 09;14(16). doi: 10.3390/ma14164462. PMID: 34442984; PMCID: PMC8398866.
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Neptunyl Peroxide Chemistry: Synthesis and Spectroscopic Characterization of a Neptunyl Triperoxide Compound, Ca.

Inorganic chemistry

Hickam S, Ray D, Szymanowski JES, Li RY, Dembowski M, Smith P, Gagliardi L, Burns PC.
PMID: 31448599
Inorg Chem. 2019 Sep 16;58(18):12264-12271. doi: 10.1021/acs.inorgchem.9b01712. Epub 2019 Aug 26.

Little is known about the crystal chemistry of neptunyl peroxide compounds compared to uranyl peroxide compounds, for which dozens of structures have been described. Uranyl peroxides are formed over a broad range of pH and solution conditions, but neptunyl...

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Hickam S, Ray D, Szymanowski JES, et al. Neptunyl Peroxide Chemistry: Synthesis and Spectroscopic Characterization of a Neptunyl Triperoxide Compound, Ca. Inorg Chem. 2019;58(18):12264-12271doi: 10.1021/acs.inorgchem.9b01712.
Hickam, S., Ray, D., Szymanowski, J. E. S., Li, R. Y., Dembowski, M., Smith, P., Gagliardi, L., & Burns, P. C. (2019). Neptunyl Peroxide Chemistry: Synthesis and Spectroscopic Characterization of a Neptunyl Triperoxide Compound, Ca. Inorganic chemistry, 58(18), 12264-12271. https://doi.org/10.1021/acs.inorgchem.9b01712
Hickam, Sarah, et al. "Neptunyl Peroxide Chemistry: Synthesis and Spectroscopic Characterization of a Neptunyl Triperoxide Compound, Ca." Inorganic chemistry vol. 58,18 (2019): 12264-12271. doi: https://doi.org/10.1021/acs.inorgchem.9b01712
Hickam S, Ray D, Szymanowski JES, Li RY, Dembowski M, Smith P, Gagliardi L, Burns PC. Neptunyl Peroxide Chemistry: Synthesis and Spectroscopic Characterization of a Neptunyl Triperoxide Compound, Ca. Inorg Chem. 2019 Sep 16;58(18):12264-12271. doi: 10.1021/acs.inorgchem.9b01712. Epub 2019 Aug 26. PMID: 31448599.
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Radiation-Induced Solid-State Transformations of Uranyl Peroxides.

Inorganic chemistry

Fairley M, Felton DE, Sigmon GE, Szymanowski JES, Poole NA, Nyman M, Burns PC, LaVerne JA.
PMID: 34965099
Inorg Chem. 2022 Jan 17;61(2):882-889. doi: 10.1021/acs.inorgchem.1c02603. Epub 2021 Dec 29.

Single-crystal X-ray diffraction studies of pristine and γ-irradiated Ca

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Fairley M, Felton DE, Sigmon GE, et al. Radiation-Induced Solid-State Transformations of Uranyl Peroxides. Inorg Chem. 2021;61(2):882-889doi: 10.1021/acs.inorgchem.1c02603.
Fairley, M., Felton, D. E., Sigmon, G. E., Szymanowski, J. E. S., Poole, N. A., Nyman, M., Burns, P. C., & LaVerne, J. A. (2022). Radiation-Induced Solid-State Transformations of Uranyl Peroxides. Inorganic chemistry, 61(2), 882-889. https://doi.org/10.1021/acs.inorgchem.1c02603
Fairley, Melissa, et al. "Radiation-Induced Solid-State Transformations of Uranyl Peroxides." Inorganic chemistry vol. 61,2 (2022): 882-889. doi: https://doi.org/10.1021/acs.inorgchem.1c02603
Fairley M, Felton DE, Sigmon GE, Szymanowski JES, Poole NA, Nyman M, Burns PC, LaVerne JA. Radiation-Induced Solid-State Transformations of Uranyl Peroxides. Inorg Chem. 2022 Jan 17;61(2):882-889. doi: 10.1021/acs.inorgchem.1c02603. Epub 2021 Dec 29. PMID: 34965099.
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Expanding the crystal chemistry of uranyl peroxides: four hybrid uranyl-peroxide structures containing EDTA.

Inorganic chemistry

Qiu J, Ling J, Sieradzki C, Nguyen K, Wylie EM, Szymanowski JE, Burns PC.
PMID: 25350361
Inorg Chem. 2014 Nov 17;53(22):12084-91. doi: 10.1021/ic5018906. Epub 2014 Oct 28.

The first four uranyl peroxide compounds containing ethylenediaminetetra-acetate (EDTA) were synthesized and characterized from aqueous uranyl peroxide nitrate solutions with a pH range of 5-7. Raman spectra demonstrated that reaction solutions that crystallized [NaK15[(UO2)8(O2)8(C10H12O10N2)2(C2O4)4]·(H2O)14] (1) and [Li4K6[(UO2)8(O2)6(C10H12O10N2)2(NO3)6]·(H2O)26] (2) contained...

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Qiu J, Ling J, Sieradzki C, et al. Expanding the crystal chemistry of uranyl peroxides: four hybrid uranyl-peroxide structures containing EDTA. Inorg Chem. 2014;53(22):12084-91doi: 10.1021/ic5018906.
Qiu, J., Ling, J., Sieradzki, C., Nguyen, K., Wylie, E. M., Szymanowski, J. E., & Burns, P. C. (2014). Expanding the crystal chemistry of uranyl peroxides: four hybrid uranyl-peroxide structures containing EDTA. Inorganic chemistry, 53(22), 12084-91. https://doi.org/10.1021/ic5018906
Qiu, Jie, et al. "Expanding the crystal chemistry of uranyl peroxides: four hybrid uranyl-peroxide structures containing EDTA." Inorganic chemistry vol. 53,22 (2014): 12084-91. doi: https://doi.org/10.1021/ic5018906
Qiu J, Ling J, Sieradzki C, Nguyen K, Wylie EM, Szymanowski JE, Burns PC. Expanding the crystal chemistry of uranyl peroxides: four hybrid uranyl-peroxide structures containing EDTA. Inorg Chem. 2014 Nov 17;53(22):12084-91. doi: 10.1021/ic5018906. Epub 2014 Oct 28. PMID: 25350361.
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Showing 1 to 12 of 51 entries