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Development of Sensitive and Specific Analysis of Vildagliptin in Pharmaceutical Formulation by Gas Chromatography-Mass Spectrometry.

Journal of analytical methods in chemistry

Uçaktürk E.
PMID: 26682085
J Anal Methods Chem. 2015;2015:707414. doi: 10.1155/2015/707414. Epub 2015 Nov 22.

A sensitive and selective gas chromatography-mass spectrometry (GC-MS) method was developed and fully validated for the determination of vildagliptin (VIL) in pharmaceutical formulation. Prior to GC-MS analysis, VIL was efficiently derivatized with MSTFA/NH4I/β-mercaptoethanol at 60°C for 30 min. The...

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Uçaktürk E. Development of Sensitive and Specific Analysis of Vildagliptin in Pharmaceutical Formulation by Gas Chromatography-Mass Spectrometry. J Anal Methods Chem. 2015;2015:707414doi: 10.1155/2015/707414.
Uçaktürk, E. (2015). Development of Sensitive and Specific Analysis of Vildagliptin in Pharmaceutical Formulation by Gas Chromatography-Mass Spectrometry. Journal of analytical methods in chemistry, 2015707414. https://doi.org/10.1155/2015/707414
Uçaktürk, Ebru. "Development of Sensitive and Specific Analysis of Vildagliptin in Pharmaceutical Formulation by Gas Chromatography-Mass Spectrometry." Journal of analytical methods in chemistry vol. 2015 (2015): 707414. doi: https://doi.org/10.1155/2015/707414
Uçaktürk E. Development of Sensitive and Specific Analysis of Vildagliptin in Pharmaceutical Formulation by Gas Chromatography-Mass Spectrometry. J Anal Methods Chem. 2015;2015:707414. doi: 10.1155/2015/707414. Epub 2015 Nov 22. PMID: 26682085; PMCID: PMC4670650.
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The impact of nandrolone decanoate administration on ovarian and uterine tissues in rat: Luteinizing hormone profile, histopathological and morphometric assessment.

Saudi journal of biological sciences

Saddick SY.
PMID: 29692652
Saudi J Biol Sci. 2018 Mar;25(3):507-512. doi: 10.1016/j.sjbs.2017.08.015. Epub 2017 Aug 26.

The study had been conducted to evaluate the effects of nandrolone decanoate (abused repeated doses) on female rat's ovary and uterus during administration and withdrawal. The study included 18 rats that were divided into control group (n = 6)...

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Saddick SY. The impact of nandrolone decanoate administration on ovarian and uterine tissues in rat: Luteinizing hormone profile, histopathological and morphometric assessment. Saudi J Biol Sci. 2017;25(3):507-512doi: 10.1016/j.sjbs.2017.08.015.
Saddick, S. Y. (2018). The impact of nandrolone decanoate administration on ovarian and uterine tissues in rat: Luteinizing hormone profile, histopathological and morphometric assessment. Saudi journal of biological sciences, 25(3), 507-512. https://doi.org/10.1016/j.sjbs.2017.08.015
Saddick, Salina Y. "The impact of nandrolone decanoate administration on ovarian and uterine tissues in rat: Luteinizing hormone profile, histopathological and morphometric assessment." Saudi journal of biological sciences vol. 25,3 (2018): 507-512. doi: https://doi.org/10.1016/j.sjbs.2017.08.015
Saddick SY. The impact of nandrolone decanoate administration on ovarian and uterine tissues in rat: Luteinizing hormone profile, histopathological and morphometric assessment. Saudi J Biol Sci. 2018 Mar;25(3):507-512. doi: 10.1016/j.sjbs.2017.08.015. Epub 2017 Aug 26. PMID: 29692652; PMCID: PMC5911639.
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Heart Reaction to Nandrolone Decanoate plus Two Different Intensities of Endurance Exercise: Electrocardiography and Stereological Approach.

Addiction & health

Joukar S, Yoosefnia M, Naderi-Boldaji V, Nasri H, Rafie F.
PMID: 31105916
Addict Health. 2018 Jul;10(3):180-189. doi: 10.22122/ahj.v10i3.587.

BACKGROUND: Regarding the negative effects of androgenic anabolic steroids (AASs) abuse, the long-term effect of nandrolone decanoate with/without two intensities of endurance exercise training was investigated on heart tissue and electrocardiogram (ECG) in rats.METHODS: The experiment was conducted on...

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Joukar S, Yoosefnia M, Naderi-Boldaji V, et al. Heart Reaction to Nandrolone Decanoate plus Two Different Intensities of Endurance Exercise: Electrocardiography and Stereological Approach. Addict Health. 2018;10(3):180-189doi: 10.22122/ahj.v10i3.587.
Joukar, S., Yoosefnia, M., Naderi-Boldaji, V., Nasri, H., & Rafie, F. (2018). Heart Reaction to Nandrolone Decanoate plus Two Different Intensities of Endurance Exercise: Electrocardiography and Stereological Approach. Addiction & health, 10(3), 180-189. https://doi.org/10.22122/ahj.v10i3.587
Joukar, Siyavash, et al. "Heart Reaction to Nandrolone Decanoate plus Two Different Intensities of Endurance Exercise: Electrocardiography and Stereological Approach." Addiction & health vol. 10,3 (2018): 180-189. doi: https://doi.org/10.22122/ahj.v10i3.587
Joukar S, Yoosefnia M, Naderi-Boldaji V, Nasri H, Rafie F. Heart Reaction to Nandrolone Decanoate plus Two Different Intensities of Endurance Exercise: Electrocardiography and Stereological Approach. Addict Health. 2018 Jul;10(3):180-189. doi: 10.22122/ahj.v10i3.587. PMID: 31105916; PMCID: PMC6511393.
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Nandrolone decanoate and resistance exercise affect body composition and energy metabolism.

Steroids

Pozzi R, Fernandes L, Cavalcante da Silva V, D'Almeida V.
PMID: 34358557
Steroids. 2021 Oct;174:108899. doi: 10.1016/j.steroids.2021.108899. Epub 2021 Aug 03.

Our aim was to evaluate the independent and associated effects of nandrolone decanoate (DECA) and resistance exercise (REx) on central and peripheral hormones and neuropeptides related to energy balance in male rats. The experimental protocol was performed for eight...

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Pozzi R, Fernandes L, Cavalcante da Silva V, et al. Nandrolone decanoate and resistance exercise affect body composition and energy metabolism. Steroids. 2021;174:108899doi: 10.1016/j.steroids.2021.108899.
Pozzi, R., Fernandes, L., Cavalcante da Silva, V., & D'Almeida, V. (2021). Nandrolone decanoate and resistance exercise affect body composition and energy metabolism. Steroids, 174108899. https://doi.org/10.1016/j.steroids.2021.108899
Pozzi, Renan, et al. "Nandrolone decanoate and resistance exercise affect body composition and energy metabolism." Steroids vol. 174 (2021): 108899. doi: https://doi.org/10.1016/j.steroids.2021.108899
Pozzi R, Fernandes L, Cavalcante da Silva V, D'Almeida V. Nandrolone decanoate and resistance exercise affect body composition and energy metabolism. Steroids. 2021 Oct;174:108899. doi: 10.1016/j.steroids.2021.108899. Epub 2021 Aug 03. PMID: 34358557.
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Assessment of testicular steroidogenic enzymes expression in experimental animal model following withdrawal of nandrolone decanoate.

Journal of animal science and technology

Min T, Karthikeyan A, Lee KH.
PMID: 34957441
J Anim Sci Technol. 2021 Nov;63(6):1247-1264. doi: 10.5187/jast.2021.e102. Epub 2021 Nov 30.

Anabolic steroids are frequently used to increase the growth rate of meat-producing animals. Exposure to an anabolic-androgenic steroid, nandrolone decanoate (ND), is associated with expressional reduction of testicular steroidogenic enzymes. However, the effect of withdrawal of ND exposure on...

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Min T, Karthikeyan A, Lee KH. Assessment of testicular steroidogenic enzymes expression in experimental animal model following withdrawal of nandrolone decanoate. J Anim Sci Technol. 2021;63(6):1247-1264doi: 10.5187/jast.2021.e102.
Min, T., Karthikeyan, A., & Lee, K. H. (2021). Assessment of testicular steroidogenic enzymes expression in experimental animal model following withdrawal of nandrolone decanoate. Journal of animal science and technology, 63(6), 1247-1264. https://doi.org/10.5187/jast.2021.e102
Min, TaeSun, et al. "Assessment of testicular steroidogenic enzymes expression in experimental animal model following withdrawal of nandrolone decanoate." Journal of animal science and technology vol. 63,6 (2021): 1247-1264. doi: https://doi.org/10.5187/jast.2021.e102
Min T, Karthikeyan A, Lee KH. Assessment of testicular steroidogenic enzymes expression in experimental animal model following withdrawal of nandrolone decanoate. J Anim Sci Technol. 2021 Nov;63(6):1247-1264. doi: 10.5187/jast.2021.e102. Epub 2021 Nov 30. PMID: 34957441; PMCID: PMC8672267.
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Effects of androgen and progestin on the proliferation and differentiation of osteoblasts.

Experimental and therapeutic medicine

Wu X, Zhang M.
PMID: 30542427
Exp Ther Med. 2018 Dec;16(6):4722-4728. doi: 10.3892/etm.2018.6772. Epub 2018 Sep 19.

Osteoporosis is liable to affect patients with gonadal hormone deficiency, and a supplement of androgens may be used to increase bone density of patients with osteoporosis. Since the androgens currently used may cause severe side effects, it is useful...

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Wu X, Zhang M. Effects of androgen and progestin on the proliferation and differentiation of osteoblasts. Exp Ther Med. 2018;16(6):4722-4728doi: 10.3892/etm.2018.6772.
Wu, X., & Zhang, M. (2018). Effects of androgen and progestin on the proliferation and differentiation of osteoblasts. Experimental and therapeutic medicine, 16(6), 4722-4728. https://doi.org/10.3892/etm.2018.6772
Wu, Xinchen, and Zhang, Mengqi. "Effects of androgen and progestin on the proliferation and differentiation of osteoblasts." Experimental and therapeutic medicine vol. 16,6 (2018): 4722-4728. doi: https://doi.org/10.3892/etm.2018.6772
Wu X, Zhang M. Effects of androgen and progestin on the proliferation and differentiation of osteoblasts. Exp Ther Med. 2018 Dec;16(6):4722-4728. doi: 10.3892/etm.2018.6772. Epub 2018 Sep 19. PMID: 30542427; PMCID: PMC6257455.
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Anabolic-androgenic steroids impair mitochondrial function and redox status in the heart and liver of mice.

Steroids

Carteri RB, Kopczynski A, Rodolphi MS, Strogulski NR, Wannmacher CMD, Franceschi ID, Hammerschmitt ME, Driemeier D, Portela LV.
PMID: 33984388
Steroids. 2021 Aug;172:108861. doi: 10.1016/j.steroids.2021.108861. Epub 2021 May 11.

Supraphysiological doses of anabolic-androgenic steroids (AAS) may cause long-term functional abnormalities, particularly in the heart and liver, which may only represent the later-stage of the cumulative damage caused by dysfunctional organelles. We investigated whether mid-term supraphysiological doses of Testosterone...

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Carteri RB, Kopczynski A, Rodolphi MS, et al. Anabolic-androgenic steroids impair mitochondrial function and redox status in the heart and liver of mice. Steroids. 2021;172:108861doi: 10.1016/j.steroids.2021.108861.
Carteri, R. B., Kopczynski, A., Rodolphi, M. S., Strogulski, N. R., Wannmacher, C. M. D., Franceschi, I. D., Hammerschmitt, M. E., Driemeier, D., & Portela, L. V. (2021). Anabolic-androgenic steroids impair mitochondrial function and redox status in the heart and liver of mice. Steroids, 172108861. https://doi.org/10.1016/j.steroids.2021.108861
Carteri, Randhall B, et al. "Anabolic-androgenic steroids impair mitochondrial function and redox status in the heart and liver of mice." Steroids vol. 172 (2021): 108861. doi: https://doi.org/10.1016/j.steroids.2021.108861
Carteri RB, Kopczynski A, Rodolphi MS, Strogulski NR, Wannmacher CMD, Franceschi ID, Hammerschmitt ME, Driemeier D, Portela LV. Anabolic-androgenic steroids impair mitochondrial function and redox status in the heart and liver of mice. Steroids. 2021 Aug;172:108861. doi: 10.1016/j.steroids.2021.108861. Epub 2021 May 11. PMID: 33984388.
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OXER1 and RACK1-associated pathway: a promising drug target for breast cancer progression.

Oncogenesis

Masi M, Garattini E, Bolis M, Di Marino D, Maraccani L, Morelli E, Grolla AA, Fagiani F, Corsini E, Travelli C, Govoni S, Racchi M, Buoso E.
PMID: 33311444
Oncogenesis. 2020 Dec 11;9(12):105. doi: 10.1038/s41389-020-00291-x.

Recent data indicate that receptor for activated C kinase 1 (RACK1) is a putative prognostic marker and drug target in breast cancer (BC). High RACK1 expression is negatively associated with overall survival, as it seems to promote BC progression....

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Masi M, Garattini E, Bolis M, et al. OXER1 and RACK1-associated pathway: a promising drug target for breast cancer progression. Oncogenesis. 2020;9(12):105doi: 10.1038/s41389-020-00291-x.
Masi, M., Garattini, E., Bolis, M., Di Marino, D., Maraccani, L., Morelli, E., Grolla, A. A., Fagiani, F., Corsini, E., Travelli, C., Govoni, S., Racchi, M., & Buoso, E. (2020). OXER1 and RACK1-associated pathway: a promising drug target for breast cancer progression. Oncogenesis, 9(12), 105. https://doi.org/10.1038/s41389-020-00291-x
Masi, Mirco, et al. "OXER1 and RACK1-associated pathway: a promising drug target for breast cancer progression." Oncogenesis vol. 9,12 (2020): 105. doi: https://doi.org/10.1038/s41389-020-00291-x
Masi M, Garattini E, Bolis M, Di Marino D, Maraccani L, Morelli E, Grolla AA, Fagiani F, Corsini E, Travelli C, Govoni S, Racchi M, Buoso E. OXER1 and RACK1-associated pathway: a promising drug target for breast cancer progression. Oncogenesis. 2020 Dec 11;9(12):105. doi: 10.1038/s41389-020-00291-x. PMID: 33311444; PMCID: PMC7732991.
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5α-reductase inhibitors: Evaluation of their potential confounding effect on GC-C-IRMS doping analysis.

Drug testing and analysis

Iannella L, Colamonici C, Curcio D, Botrè F, de la Torre X.
PMID: 34318592
Drug Test Anal. 2021 Jul 27; doi: 10.1002/dta.3134. Epub 2021 Jul 27.

5α-reductase inhibitors (5-ARIs) are considered by the World Anti-doping Agency as potential confounding factors in evaluating the athlete steroid profile, since they may interfere with the urinary excretion of several diagnostic compounds. We herein investigated 5α-reductase inhibitors from a...

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Iannella L, Colamonici C, Curcio D, et al. 5α-reductase inhibitors: Evaluation of their potential confounding effect on GC-C-IRMS doping analysis. Drug Test Anal. 2021;doi: 10.1002/dta.3134.
Iannella, L., Colamonici, C., Curcio, D., Botrè, F., & de la Torre, X. (2021). 5α-reductase inhibitors: Evaluation of their potential confounding effect on GC-C-IRMS doping analysis. Drug testing and analysis, . https://doi.org/10.1002/dta.3134
Iannella, Loredana, et al. "5α-reductase inhibitors: Evaluation of their potential confounding effect on GC-C-IRMS doping analysis." Drug testing and analysis vol. (2021). doi: https://doi.org/10.1002/dta.3134
Iannella L, Colamonici C, Curcio D, Botrè F, de la Torre X. 5α-reductase inhibitors: Evaluation of their potential confounding effect on GC-C-IRMS doping analysis. Drug Test Anal. 2021 Jul 27; doi: 10.1002/dta.3134. Epub 2021 Jul 27. PMID: 34318592.
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Anabolic Steroids-Driven Regulation of Porcine Ovarian Putative Stem Cells Favors the Onset of Their Neoplastic Transformation.

International journal of molecular sciences

Gorczyca G, Wartalski K, Wiater J, Samiec M, Tabarowski Z, Duda M.
PMID: 34769230
Int J Mol Sci. 2021 Oct 30;22(21). doi: 10.3390/ijms222111800.

Nandrolone (Ndn) and boldenone (Bdn), the synthetic testosterone analogues with strong anabolic effects, despite being recognized as potentially carcinogenic compounds, are commonly abused by athletes and bodybuilders, which includes women, worldwide. This study tested the hypothesis that different doses...

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Gorczyca G, Wartalski K, Wiater J, et al. Anabolic Steroids-Driven Regulation of Porcine Ovarian Putative Stem Cells Favors the Onset of Their Neoplastic Transformation. Int J Mol Sci. 2021;22(21)doi: 10.3390/ijms222111800.
Gorczyca, G., Wartalski, K., Wiater, J., Samiec, M., Tabarowski, Z., & Duda, M. (2021). Anabolic Steroids-Driven Regulation of Porcine Ovarian Putative Stem Cells Favors the Onset of Their Neoplastic Transformation. International journal of molecular sciences, 22(21), . https://doi.org/10.3390/ijms222111800
Gorczyca, Gabriela, et al. "Anabolic Steroids-Driven Regulation of Porcine Ovarian Putative Stem Cells Favors the Onset of Their Neoplastic Transformation." International journal of molecular sciences vol. 22,21 (2021). doi: https://doi.org/10.3390/ijms222111800
Gorczyca G, Wartalski K, Wiater J, Samiec M, Tabarowski Z, Duda M. Anabolic Steroids-Driven Regulation of Porcine Ovarian Putative Stem Cells Favors the Onset of Their Neoplastic Transformation. Int J Mol Sci. 2021 Oct 30;22(21). doi: 10.3390/ijms222111800. PMID: 34769230; PMCID: PMC8583785.
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Association between nandrolone and behavioral alterations: A systematic review of preclinical studies.

Steroids

Niromand E, Javanmardy S, Salimi Z, Zarei F, Khazaei MR.
PMID: 34407462
Steroids. 2021 Oct;174:108901. doi: 10.1016/j.steroids.2021.108901. Epub 2021 Aug 15.

BACKGROUND AND AIM: In recent years the expanding misuse of Nandrolone among non-athletes, particularly adolescent males is a prevalent global concern due to its adverse effects. This article provides a summary of the experimental studies to clarify the relationship...

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Niromand E, Javanmardy S, Salimi Z, et al. Association between nandrolone and behavioral alterations: A systematic review of preclinical studies. Steroids. 2021;174:108901doi: 10.1016/j.steroids.2021.108901.
Niromand, E., Javanmardy, S., Salimi, Z., Zarei, F., & Khazaei, M. R. (2021). Association between nandrolone and behavioral alterations: A systematic review of preclinical studies. Steroids, 174108901. https://doi.org/10.1016/j.steroids.2021.108901
Niromand, Elham, et al. "Association between nandrolone and behavioral alterations: A systematic review of preclinical studies." Steroids vol. 174 (2021): 108901. doi: https://doi.org/10.1016/j.steroids.2021.108901
Niromand E, Javanmardy S, Salimi Z, Zarei F, Khazaei MR. Association between nandrolone and behavioral alterations: A systematic review of preclinical studies. Steroids. 2021 Oct;174:108901. doi: 10.1016/j.steroids.2021.108901. Epub 2021 Aug 15. PMID: 34407462.
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PDE7B is involved in nandrolone decanoate hydrolysis in liver cytosol and its transcription is up-regulated by androgens in HepG2.

Frontiers in pharmacology

Strahm E, Rane A, Ekström L.
PMID: 24910615
Front Pharmacol. 2014 May 30;5:132. doi: 10.3389/fphar.2014.00132. eCollection 2014.

Most androgenic drugs are available as esters for a prolonged depot action. However, the enzymes involved in the hydrolysis of the esters have not been identified. There is one study indicating that PDE7B may be involved in the activation...

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Strahm E, Rane A, Ekström L. PDE7B is involved in nandrolone decanoate hydrolysis in liver cytosol and its transcription is up-regulated by androgens in HepG2. Front Pharmacol. 2014;5:132doi: 10.3389/fphar.2014.00132.
Strahm, E., Rane, A., & Ekström, L. (2014). PDE7B is involved in nandrolone decanoate hydrolysis in liver cytosol and its transcription is up-regulated by androgens in HepG2. Frontiers in pharmacology, 5132. https://doi.org/10.3389/fphar.2014.00132
Strahm, Emmanuel, et al. "PDE7B is involved in nandrolone decanoate hydrolysis in liver cytosol and its transcription is up-regulated by androgens in HepG2." Frontiers in pharmacology vol. 5 (2014): 132. doi: https://doi.org/10.3389/fphar.2014.00132
Strahm E, Rane A, Ekström L. PDE7B is involved in nandrolone decanoate hydrolysis in liver cytosol and its transcription is up-regulated by androgens in HepG2. Front Pharmacol. 2014 May 30;5:132. doi: 10.3389/fphar.2014.00132. eCollection 2014. PMID: 24910615; PMCID: PMC4038775.
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