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Synthesis of enantiopure 1,2-azido and 1,2-amino alcohols .

Tetrahedron, asymmetry

Wang HY, Huang K, De Jesús M, Espinosa S, Piñero-Santiago LE, Barnes CL, Ortiz-Marciales M.
PMID: 26843787
Tetrahedron Asymmetry. 2016 Feb 15;27(2):91-100. doi: 10.1016/j.tetasy.2015.12.002.

A practical and convenient method for the efficient and regio- and stereoselective ring-opening of enantiopure monosubstituted epoxides by sodium azide under hydrolytic conditions is reported. The ring-opening of enantiopure styryl and pyridyl (

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Wang HY, Huang K, De Jesús M, et al. Synthesis of enantiopure 1,2-azido and 1,2-amino alcohols . Tetrahedron Asymmetry. 2016;27(2):91-100doi: 10.1016/j.tetasy.2015.12.002.
Wang, H. Y., Huang, K., De Jesús, M., Espinosa, S., Piñero-Santiago, L. E., Barnes, C. L., & Ortiz-Marciales, M. (2016). Synthesis of enantiopure 1,2-azido and 1,2-amino alcohols . Tetrahedron, asymmetry, 27(2), 91-100. https://doi.org/10.1016/j.tetasy.2015.12.002
Wang, Hai-Yang, et al. "Synthesis of enantiopure 1,2-azido and 1,2-amino alcohols ." Tetrahedron, asymmetry vol. 27,2 (2016): 91-100. doi: https://doi.org/10.1016/j.tetasy.2015.12.002
Wang HY, Huang K, De Jesús M, Espinosa S, Piñero-Santiago LE, Barnes CL, Ortiz-Marciales M. Synthesis of enantiopure 1,2-azido and 1,2-amino alcohols . Tetrahedron Asymmetry. 2016 Feb 15;27(2):91-100. doi: 10.1016/j.tetasy.2015.12.002. PMID: 26843787; PMCID: PMC4733893.
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The Mechanism Underlying the Antibacterial Activity of Shikonin against Methicillin-Resistant Staphylococcus aureus.

Evidence-based complementary and alternative medicine : eCAM

Lee YS, Lee DY, Kim YB, Lee SW, Cha SW, Park HW, Kim GS, Kwon DY, Lee MH, Han SH.
PMID: 26265924
Evid Based Complement Alternat Med. 2015;2015:520578. doi: 10.1155/2015/520578. Epub 2015 Jul 21.

Shikonin (SKN), a highly liposoluble naphthoquinone pigment isolated from the roots of Lithospermum erythrorhizon, is known to exert antibacterial, wound-healing, anti-inflammatory, antithrombotic, and antitumor effects. The aim of this study was to examine SKN antibacterial activity against methicillin-resistant Staphylococcus...

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Lee YS, Lee DY, Kim YB, et al. The Mechanism Underlying the Antibacterial Activity of Shikonin against Methicillin-Resistant Staphylococcus aureus. Evid Based Complement Alternat Med. 2015;2015:520578doi: 10.1155/2015/520578.
Lee, Y. S., Lee, D. Y., Kim, Y. B., Lee, S. W., Cha, S. W., Park, H. W., Kim, G. S., Kwon, D. Y., Lee, M. H., & Han, S. H. (2015). The Mechanism Underlying the Antibacterial Activity of Shikonin against Methicillin-Resistant Staphylococcus aureus. Evidence-based complementary and alternative medicine : eCAM, 2015520578. https://doi.org/10.1155/2015/520578
Lee, Young-Seob, et al. "The Mechanism Underlying the Antibacterial Activity of Shikonin against Methicillin-Resistant Staphylococcus aureus." Evidence-based complementary and alternative medicine : eCAM vol. 2015 (2015): 520578. doi: https://doi.org/10.1155/2015/520578
Lee YS, Lee DY, Kim YB, Lee SW, Cha SW, Park HW, Kim GS, Kwon DY, Lee MH, Han SH. The Mechanism Underlying the Antibacterial Activity of Shikonin against Methicillin-Resistant Staphylococcus aureus. Evid Based Complement Alternat Med. 2015;2015:520578. doi: 10.1155/2015/520578. Epub 2015 Jul 21. PMID: 26265924; PMCID: PMC4523682.
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[No title available]

Frontiers in plant science

Szurman-Zubrzycka ME, Zbieszczyk J, Marzec M, Jelonek J, Chmielewska B, Kurowska MM, Krok M, Daszkowska-Golec A, Guzy-Wrobelska J, Gruszka D, Gajecka M, Gajewska P, Stolarek M, Tylec P, Sega P, Lip S, Kudełko M, Lorek M, Gorniak-Walas M, Malolepszy A, Podsiadlo N, Szyrajew KP, Keisa A, Mbambo Z, Todorowska E, Gaj M, Nita Z, Orlowska-Job W, Maluszynski M, Szarejko I.
PMID: 29515615
Front Plant Sci. 2018 Feb 21;9:216. doi: 10.3389/fpls.2018.00216. eCollection 2018.

TILLING (Targeting Induced Local Lesions IN Genomes) is a strategy used for functional analysis of genes that combines the classical mutagenesis and a rapid, high-throughput identification of mutations within a gene of interest. TILLING has been initially developed as...

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Szurman-Zubrzycka ME, Zbieszczyk J, Marzec M, et al. . Front Plant Sci. 2018;9:216doi: 10.3389/fpls.2018.00216.
Szurman-Zubrzycka, M. E., Zbieszczyk, J., Marzec, M., Jelonek, J., Chmielewska, B., Kurowska, M. M., Krok, M., Daszkowska-Golec, A., Guzy-Wrobelska, J., Gruszka, D., Gajecka, M., Gajewska, P., Stolarek, M., Tylec, P., Sega, P., Lip, S., Kudełko, M., Lorek, M., Gorniak-Walas, M., Malolepszy, A., Podsiadlo, N., Szyrajew, K. P., Keisa, A., Mbambo, Z., Todorowska, E., Gaj, M., Nita, Z., Orlowska-Job, W., Maluszynski, M., & Szarejko, I. (2018). . Frontiers in plant science, 9216. https://doi.org/10.3389/fpls.2018.00216
Szurman-Zubrzycka, Miriam E, et al. "." Frontiers in plant science vol. 9 (2018): 216. doi: https://doi.org/10.3389/fpls.2018.00216
Szurman-Zubrzycka ME, Zbieszczyk J, Marzec M, Jelonek J, Chmielewska B, Kurowska MM, Krok M, Daszkowska-Golec A, Guzy-Wrobelska J, Gruszka D, Gajecka M, Gajewska P, Stolarek M, Tylec P, Sega P, Lip S, Kudełko M, Lorek M, Gorniak-Walas M, Malolepszy A, Podsiadlo N, Szyrajew KP, Keisa A, Mbambo Z, Todorowska E, Gaj M, Nita Z, Orlowska-Job W, Maluszynski M, Szarejko I. . Front Plant Sci. 2018 Feb 21;9:216. doi: 10.3389/fpls.2018.00216. eCollection 2018. PMID: 29515615; PMCID: PMC5826354.
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The determination of ionic transport properties at high pressures in a diamond anvil cell.

The Review of scientific instruments

Wang Q, Liu C, Han Y, Gao C, Ma Y.
PMID: 28040923
Rev Sci Instrum. 2016 Dec;87(12):123904. doi: 10.1063/1.4971304.

A two-electrode configuration was adopted in an in situ impedance measurement system to determine the ionic conductivity at high pressures in a diamond anvil cell. In the experimental measurements, Mo thin-films were specifically coated on tops of the diamond...

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Wang Q, Liu C, Han Y, et al. The determination of ionic transport properties at high pressures in a diamond anvil cell. Rev Sci Instrum. 2016;87(12):123904doi: 10.1063/1.4971304.
Wang, Q., Liu, C., Han, Y., Gao, C., & Ma, Y. (2016). The determination of ionic transport properties at high pressures in a diamond anvil cell. The Review of scientific instruments, 87(12), 123904. https://doi.org/10.1063/1.4971304
Wang, Qinglin, et al. "The determination of ionic transport properties at high pressures in a diamond anvil cell." The Review of scientific instruments vol. 87,12 (2016): 123904. doi: https://doi.org/10.1063/1.4971304
Wang Q, Liu C, Han Y, Gao C, Ma Y. The determination of ionic transport properties at high pressures in a diamond anvil cell. Rev Sci Instrum. 2016 Dec;87(12):123904. doi: 10.1063/1.4971304. PMID: 28040923.
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Crystal structure of 4,5-bis-(3,4,5-tri-meth-oxy-phen-yl)-2H-1,2,3-triazole methanol monosolvate.

Acta crystallographica. Section E, Structure reports online

Madadi NR, Penthala NR, Bommagani S, Parkin S, Crooks PA.
PMID: 25484710
Acta Crystallogr Sect E Struct Rep Online. 2014 Sep 24;70:o1128-9. doi: 10.1107/S1600536814020911. eCollection 2014 Oct 01.

The title compound, C20H23N3O6·CH3OH, was synthesized by [3 + 2] cyclo-addition of (Z)-2,3-bis-(3,4,5-tri-meth-oxy-phen-yl)acrylo-nitrile with sodium azide and ammonium chloride in DMF/water. The central nitro-gen of the triazole ring is protonated. The dihedral angles between the triazole ring and the...

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Madadi NR, Penthala NR, Bommagani S, et al. Crystal structure of 4,5-bis-(3,4,5-tri-meth-oxy-phen-yl)-2H-1,2,3-triazole methanol monosolvate. Acta Crystallogr Sect E Struct Rep Online. 2014;70:o1128-9doi: 10.1107/S1600536814020911.
Madadi, N. R., Penthala, N. R., Bommagani, S., Parkin, S., & Crooks, P. A. (2014). Crystal structure of 4,5-bis-(3,4,5-tri-meth-oxy-phen-yl)-2H-1,2,3-triazole methanol monosolvate. Acta crystallographica. Section E, Structure reports online, 70o1128-9. https://doi.org/10.1107/S1600536814020911
Madadi, Nikhil Reddy, et al. "Crystal structure of 4,5-bis-(3,4,5-tri-meth-oxy-phen-yl)-2H-1,2,3-triazole methanol monosolvate." Acta crystallographica. Section E, Structure reports online vol. 70 (2014): o1128-9. doi: https://doi.org/10.1107/S1600536814020911
Madadi NR, Penthala NR, Bommagani S, Parkin S, Crooks PA. Crystal structure of 4,5-bis-(3,4,5-tri-meth-oxy-phen-yl)-2H-1,2,3-triazole methanol monosolvate. Acta Crystallogr Sect E Struct Rep Online. 2014 Sep 24;70:o1128-9. doi: 10.1107/S1600536814020911. eCollection 2014 Oct 01. PMID: 25484710; PMCID: PMC4257191.
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Taming chlorine azide: access to 1,2-azidochlorides from alkenes.

The Journal of organic chemistry

Valiulin RA, Mamidyala S, Finn MG.
PMID: 25719396
J Org Chem. 2015 Mar 06;80(5):2740-55. doi: 10.1021/acs.joc.5b00009. Epub 2015 Feb 26.

The in situ preparation and trapping of chlorine azide provided a versatile one-pot method for the azidochlorination of alkenes. Gaseous ClN3 generated from sodium azide, hypochlorite, and acetic acid can be explosive if isolation is attempted. Instead, we generated...

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Valiulin RA, Mamidyala S, Finn MG. Taming chlorine azide: access to 1,2-azidochlorides from alkenes. J Org Chem. 2015;80(5):2740-55doi: 10.1021/acs.joc.5b00009.
Valiulin, R. A., Mamidyala, S., & Finn, M. G. (2015). Taming chlorine azide: access to 1,2-azidochlorides from alkenes. The Journal of organic chemistry, 80(5), 2740-55. https://doi.org/10.1021/acs.joc.5b00009
Valiulin, Roman A, et al. "Taming chlorine azide: access to 1,2-azidochlorides from alkenes." The Journal of organic chemistry vol. 80,5 (2015): 2740-55. doi: https://doi.org/10.1021/acs.joc.5b00009
Valiulin RA, Mamidyala S, Finn MG. Taming chlorine azide: access to 1,2-azidochlorides from alkenes. J Org Chem. 2015 Mar 06;80(5):2740-55. doi: 10.1021/acs.joc.5b00009. Epub 2015 Feb 26. PMID: 25719396.
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Abiotic reversible self-assembly of fulvic and humic acid aggregates in low electrolytic conductivity solutions by dynamic light scattering and zeta potential investigation.

The Science of the total environment

Esfahani MR, Stretz HA, Wells MJ.
PMID: 26282742
Sci Total Environ. 2015 Dec 15;537:81-92. doi: 10.1016/j.scitotenv.2015.08.001. Epub 2015 Aug 14.

The aggregation of humic substances and their interaction with filtration media (membranes, soils) has implications for our understanding of membrane fouling during water treatment, the facilitated transport of contaminants, and the transport of organic matter through the microbial loop....

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Esfahani MR, Stretz HA, Wells MJ. Abiotic reversible self-assembly of fulvic and humic acid aggregates in low electrolytic conductivity solutions by dynamic light scattering and zeta potential investigation. Sci Total Environ. 2015;537:81-92doi: 10.1016/j.scitotenv.2015.08.001.
Esfahani, M. R., Stretz, H. A., & Wells, M. J. (2015). Abiotic reversible self-assembly of fulvic and humic acid aggregates in low electrolytic conductivity solutions by dynamic light scattering and zeta potential investigation. The Science of the total environment, 53781-92. https://doi.org/10.1016/j.scitotenv.2015.08.001
Esfahani, Milad Rabbani, et al. "Abiotic reversible self-assembly of fulvic and humic acid aggregates in low electrolytic conductivity solutions by dynamic light scattering and zeta potential investigation." The Science of the total environment vol. 537 (2015): 81-92. doi: https://doi.org/10.1016/j.scitotenv.2015.08.001
Esfahani MR, Stretz HA, Wells MJ. Abiotic reversible self-assembly of fulvic and humic acid aggregates in low electrolytic conductivity solutions by dynamic light scattering and zeta potential investigation. Sci Total Environ. 2015 Dec 15;537:81-92. doi: 10.1016/j.scitotenv.2015.08.001. Epub 2015 Aug 14. PMID: 26282742.
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The breakdown of malathion in soil and soil components.

Microbial ecology

Gibson WP, Burns RG.
PMID: 24233575
Microb Ecol. 1977 Sep;3(3):219-30. doi: 10.1007/BF02010619.

The disappearance of the organophosphorus insecticide, malathion, from a silt loam soil and from its organic and inorganic components was examined. Half-lives and the time taken for 90% decomposition in nonsterile, sodium azide-treated, and 2.5 Mrad-irradiated soils were similar...

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Gibson WP, Burns RG. The breakdown of malathion in soil and soil components. Microb Ecol. 1977;3(3):219-30doi: 10.1007/BF02010619.
Gibson, W. P., & Burns, R. G. (1977). The breakdown of malathion in soil and soil components. Microbial ecology, 3(3), 219-30. https://doi.org/10.1007/BF02010619
Gibson, W P, and Burns, R G. "The breakdown of malathion in soil and soil components." Microbial ecology vol. 3,3 (1977): 219-30. doi: https://doi.org/10.1007/BF02010619
Gibson WP, Burns RG. The breakdown of malathion in soil and soil components. Microb Ecol. 1977 Sep;3(3):219-30. doi: 10.1007/BF02010619. PMID: 24233575.
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Singlet oxygen production in thylakoid membranes during photoinhibition as detected by EPR spectroscopy.

Photosynthesis research

Hideg E, Spetea C, Vass I.
PMID: 24311071
Photosynth Res. 1994 Feb;39(2):191-9. doi: 10.1007/BF00029386.

Exposure of isolated spinach thylakoids to high intensity illumination (photoinhibition) results in the well-characterized impairment of Photosystem II electron transport, followed by degradation of the D1 reaction centre protein. In the present study we demonstrate that this process is...

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Hideg E, Spetea C, Vass I. Singlet oxygen production in thylakoid membranes during photoinhibition as detected by EPR spectroscopy. Photosynth Res. 1994;39(2):191-9doi: 10.1007/BF00029386.
Hideg, E., Spetea, C., & Vass, I. (1994). Singlet oxygen production in thylakoid membranes during photoinhibition as detected by EPR spectroscopy. Photosynthesis research, 39(2), 191-9. https://doi.org/10.1007/BF00029386
Hideg, E, et al. "Singlet oxygen production in thylakoid membranes during photoinhibition as detected by EPR spectroscopy." Photosynthesis research vol. 39,2 (1994): 191-9. doi: https://doi.org/10.1007/BF00029386
Hideg E, Spetea C, Vass I. Singlet oxygen production in thylakoid membranes during photoinhibition as detected by EPR spectroscopy. Photosynth Res. 1994 Feb;39(2):191-9. doi: 10.1007/BF00029386. PMID: 24311071.
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Regio- and Stereocontrolled Formation of Chiral Epoxy Oxazolidines via Bromocarbamation of N-Boc Alkenyl Oxazolidines. Application to Asymmetric Synthesis.

The Journal of organic chemistry

Agami C, Couty F, Hamon L, Venier O.
PMID: 11671515
J Org Chem. 1997 Apr 04;62(7):2106-2112. doi: 10.1021/jo962277g.

Treatment of alpha-alkenyl N-Boc oxazolidines with N-bromosuccinimide leads to epoxy oxazolidines via a bromocyclocarbamation reaction which is completely stereoselective. Action of sodium azide on these epoxides, followed by a few functional group manipulations, eventually affords chiral beta-amino alcohols which...

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Agami C, Couty F, Hamon L, et al. Regio- and Stereocontrolled Formation of Chiral Epoxy Oxazolidines via Bromocarbamation of N-Boc Alkenyl Oxazolidines. Application to Asymmetric Synthesis. J Org Chem. 1997;62(7):2106-2112doi: 10.1021/jo962277g.
Agami, C., Couty, F., Hamon, L., & Venier, O. (1997). Regio- and Stereocontrolled Formation of Chiral Epoxy Oxazolidines via Bromocarbamation of N-Boc Alkenyl Oxazolidines. Application to Asymmetric Synthesis. The Journal of organic chemistry, 62(7), 2106-2112. https://doi.org/10.1021/jo962277g
Agami, Claude, et al. "Regio- and Stereocontrolled Formation of Chiral Epoxy Oxazolidines via Bromocarbamation of N-Boc Alkenyl Oxazolidines. Application to Asymmetric Synthesis." The Journal of organic chemistry vol. 62,7 (1997): 2106-2112. doi: https://doi.org/10.1021/jo962277g
Agami C, Couty F, Hamon L, Venier O. Regio- and Stereocontrolled Formation of Chiral Epoxy Oxazolidines via Bromocarbamation of N-Boc Alkenyl Oxazolidines. Application to Asymmetric Synthesis. J Org Chem. 1997 Apr 04;62(7):2106-2112. doi: 10.1021/jo962277g. PMID: 11671515.
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Synthesis of Cyclopropyl-Fused Carbocyclic Nucleosides via the Regioselective Opening of Cyclic Sulfites.

The Journal of organic chemistry

Moon HR, Kim HO, Chun MW, Jeong LS, Marquez VE.
PMID: 11674546
J Org Chem. 1999 Jun 25;64(13):4733-4741. doi: 10.1021/jo990010m.

The syntheses of some carbocyclic nucleosides that are conformationally locked as "northern" mimics of antiviral active, ring-expanded oxetanocin analogues are reported. The target compounds derived their rigid conformation from a common bicyclo[3.1.0]hexane template. The uracil (3a), cytosine (3b), and...

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Moon HR, Kim HO, Chun MW, et al. Synthesis of Cyclopropyl-Fused Carbocyclic Nucleosides via the Regioselective Opening of Cyclic Sulfites. J Org Chem. 1999;64(13):4733-4741doi: 10.1021/jo990010m.
Moon, H. R., Kim, H. O., Chun, M. W., Jeong, L. S., & Marquez, V. E. (1999). Synthesis of Cyclopropyl-Fused Carbocyclic Nucleosides via the Regioselective Opening of Cyclic Sulfites. The Journal of organic chemistry, 64(13), 4733-4741. https://doi.org/10.1021/jo990010m
Moon, Hyung Ryong, et al. "Synthesis of Cyclopropyl-Fused Carbocyclic Nucleosides via the Regioselective Opening of Cyclic Sulfites." The Journal of organic chemistry vol. 64,13 (1999): 4733-4741. doi: https://doi.org/10.1021/jo990010m
Moon HR, Kim HO, Chun MW, Jeong LS, Marquez VE. Synthesis of Cyclopropyl-Fused Carbocyclic Nucleosides via the Regioselective Opening of Cyclic Sulfites. J Org Chem. 1999 Jun 25;64(13):4733-4741. doi: 10.1021/jo990010m. PMID: 11674546.
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Antioxidant effect of red wine anthocyanins in normal and catalase-inactive human erythrocytes.

The Journal of nutritional biochemistry

Tedesco I, Luigi Russo G, Nazzaro F, Russo M, Palumbo R.
PMID: 11834210
J Nutr Biochem. 2001 Sep;12(9):505-511. doi: 10.1016/s0955-2863(01)00164-4.

Previous studies reported that aged red wine, but not novel red wine or white wine protects human red blood cells from oxidative damage induced in vitro by H(2)O(2.) Here, we demonstrate that the beneficial properties of aged red wine...

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Tedesco I, Luigi Russo G, Nazzaro F, et al. Antioxidant effect of red wine anthocyanins in normal and catalase-inactive human erythrocytes. J Nutr Biochem. 2001;12(9):505-511doi: 10.1016/s0955-2863(01)00164-4.
Tedesco, I., Luigi Russo, G., Nazzaro, F., Russo, M., & Palumbo, R. (2001). Antioxidant effect of red wine anthocyanins in normal and catalase-inactive human erythrocytes. The Journal of nutritional biochemistry, 12(9), 505-511. https://doi.org/10.1016/s0955-2863(01)00164-4
Tedesco, I, et al. "Antioxidant effect of red wine anthocyanins in normal and catalase-inactive human erythrocytes." The Journal of nutritional biochemistry vol. 12,9 (2001): 505-511. doi: https://doi.org/10.1016/s0955-2863(01)00164-4
Tedesco I, Luigi Russo G, Nazzaro F, Russo M, Palumbo R. Antioxidant effect of red wine anthocyanins in normal and catalase-inactive human erythrocytes. J Nutr Biochem. 2001 Sep;12(9):505-511. doi: 10.1016/s0955-2863(01)00164-4. PMID: 11834210.
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