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Zhou J, Kuntze-Fechner MW, Bertermann R, et al. Preparing (Multi)Fluoroarenes as Building Blocks for Synthesis: Nickel-Catalyzed Borylation of Polyfluoroarenes via C-F Bond Cleavage. J Am Chem Soc. 2016;138(16):5250-3doi: 10.1021/jacs.6b02337.
Zhou, J., Kuntze-Fechner, M. W., Bertermann, R., Paul, U. S., Berthel, J. H., Friedrich, A., Du, Z., Marder, T. B., & Radius, U. (2016). Preparing (Multi)Fluoroarenes as Building Blocks for Synthesis: Nickel-Catalyzed Borylation of Polyfluoroarenes via C-F Bond Cleavage. Journal of the American Chemical Society, 138(16), 5250-3. https://doi.org/10.1021/jacs.6b02337
Zhou, Jing, et al. "Preparing (Multi)Fluoroarenes as Building Blocks for Synthesis: Nickel-Catalyzed Borylation of Polyfluoroarenes via C-F Bond Cleavage." Journal of the American Chemical Society vol. 138,16 (2016): 5250-3. doi: https://doi.org/10.1021/jacs.6b02337
Zhou J, Kuntze-Fechner MW, Bertermann R, Paul US, Berthel JH, Friedrich A, Du Z, Marder TB, Radius U. Preparing (Multi)Fluoroarenes as Building Blocks for Synthesis: Nickel-Catalyzed Borylation of Polyfluoroarenes via C-F Bond Cleavage. J Am Chem Soc. 2016 Apr 27;138(16):5250-3. doi: 10.1021/jacs.6b02337. Epub 2016 Apr 18. PMID: 27070867.
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J Am Chem Soc. 2016 Apr 27;138(16):5250-3. doi: 10.1021/jacs.6b02337. Epub 2016 Apr 18.

Preparing (Multi)Fluoroarenes as Building Blocks for Synthesis: Nickel-Catalyzed Borylation of Polyfluoroarenes via C-F Bond Cleavage.

Journal of the American Chemical Society

Jing Zhou, Maximilian W Kuntze-Fechner, Rüdiger Bertermann, Ursula S D Paul, Johannes H J Berthel, Alexandra Friedrich, Zhenting Du, Todd B Marder, Udo Radius

Affiliations

  1. College of Science, Northwest A&F University , Yangling, Shaanxi 712100, P. R. China.
  2. Institut für Anorganische Chemie, Julius-Maximilians-Universität Würzburg , Am Hubland, 97074 Würzburg, Germany.

PMID: 27070867 DOI: 10.1021/jacs.6b02337

Abstract

The [Ni(IMes)2]-catalyzed transformation of fluoroarenes into arylboronic acid pinacol esters via C-F bond activation and transmetalation with bis(pinacolato)diboron (B2pin2) is reported. Various partially fluorinated arenes with different degrees of fluorination were converted into their corresponding boronate esters.

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