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Early-Late Heterometallic Complexes of Gold and Zirconium: Photoluminescence and Reactivity.

Chemistry (Weinheim an der Bergstrasse, Germany)

Bestgen S, Schoo C, Zovko C, Köppe R, Kelly RP, Lebedkin S, Kappes MM, Roesky PW.
PMID: 27062296
Chemistry. 2016 May 17;22(21):7115-26. doi: 10.1002/chem.201600476. Epub 2016 Apr 08.

OH functionalized triarylphosphines were used to assemble zirconocene-based metalloligands with phosphine donor sites in varying positions. These complexes were subsequently treated with different gold precursors to obtain early-late heterometallic compounds in which the metal atoms exhibit different intermetallic distances....

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Bestgen S, Schoo C, Zovko C, et al. Early-Late Heterometallic Complexes of Gold and Zirconium: Photoluminescence and Reactivity. Chemistry. 2016;22(21):7115-26doi: 10.1002/chem.201600476.
Bestgen, S., Schoo, C., Zovko, C., Köppe, R., Kelly, R. P., Lebedkin, S., Kappes, M. M., & Roesky, P. W. (2016). Early-Late Heterometallic Complexes of Gold and Zirconium: Photoluminescence and Reactivity. Chemistry (Weinheim an der Bergstrasse, Germany), 22(21), 7115-26. https://doi.org/10.1002/chem.201600476
Bestgen, Sebastian, et al. "Early-Late Heterometallic Complexes of Gold and Zirconium: Photoluminescence and Reactivity." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 22,21 (2016): 7115-26. doi: https://doi.org/10.1002/chem.201600476
Bestgen S, Schoo C, Zovko C, Köppe R, Kelly RP, Lebedkin S, Kappes MM, Roesky PW. Early-Late Heterometallic Complexes of Gold and Zirconium: Photoluminescence and Reactivity. Chemistry. 2016 May 17;22(21):7115-26. doi: 10.1002/chem.201600476. Epub 2016 Apr 08. PMID: 27062296.
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[Ag.

Chemical science

Bestgen S, Fuhr O, Breitung B, Kiran Chakravadhanula VS, Guthausen G, Hennrich F, Yu W, Kappes MM, Roesky PW, Fenske D.
PMID: 28507679
Chem Sci. 2017 Mar 01;8(3):2235-2240. doi: 10.1039/c6sc04578b. Epub 2016 Dec 15.

With the aim to synthesize soluble cluster molecules, the silver salt of (4-(

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Bestgen S, Fuhr O, Breitung B, et al. [Ag. Chem Sci. 2016;8(3):2235-2240doi: 10.1039/c6sc04578b.
Bestgen, S., Fuhr, O., Breitung, B., Kiran Chakravadhanula, V. S., Guthausen, G., Hennrich, F., Yu, W., Kappes, M. M., Roesky, P. W., & Fenske, D. (2017). [Ag. Chemical science, 8(3), 2235-2240. https://doi.org/10.1039/c6sc04578b
Bestgen, Sebastian, et al. "[Ag." Chemical science vol. 8,3 (2017): 2235-2240. doi: https://doi.org/10.1039/c6sc04578b
Bestgen S, Fuhr O, Breitung B, Kiran Chakravadhanula VS, Guthausen G, Hennrich F, Yu W, Kappes MM, Roesky PW, Fenske D. [Ag. Chem Sci. 2017 Mar 01;8(3):2235-2240. doi: 10.1039/c6sc04578b. Epub 2016 Dec 15. PMID: 28507679; PMCID: PMC5408567.
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Addition Reactions of Me3 SiCN with Aldehydes Catalyzed by Aluminum Complexes Containing in their Coordination Sphere O, S, and N Ligands.

Chemistry (Weinheim an der Bergstrasse, Germany)

Yang Z, Yi Y, Zhong M, De S, Mondal T, Koley D, Ma X, Zhang D, Roesky HW.
PMID: 27062461
Chemistry. 2016 May 10;22(20):6932-8. doi: 10.1002/chem.201505162. Epub 2016 Apr 08.

The reaction of one equivalent of LAlH2 (1; L=HC(CMeNAr)2 , Ar=2,6-iPr2 C6 H3 , β-diketiminate ligand) with two equivalents of 2-mercapto-4,6-dimethylpyrimidine hydrate resulted in LAl[(μ-S)(m-C4 N2 H)(CH2 )2 ]2 (2) in good yield. Similarly, when N-2-pyridylsalicylideneamine, N-(2,6-diisopropylphenyl)salicylaldimine, and ethyl...

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Yang Z, Yi Y, Zhong M, et al. Addition Reactions of Me3 SiCN with Aldehydes Catalyzed by Aluminum Complexes Containing in their Coordination Sphere O, S, and N Ligands. Chemistry. 2016;22(20):6932-8doi: 10.1002/chem.201505162.
Yang, Z., Yi, Y., Zhong, M., De, S., Mondal, T., Koley, D., Ma, X., Zhang, D., & Roesky, H. W. (2016). Addition Reactions of Me3 SiCN with Aldehydes Catalyzed by Aluminum Complexes Containing in their Coordination Sphere O, S, and N Ligands. Chemistry (Weinheim an der Bergstrasse, Germany), 22(20), 6932-8. https://doi.org/10.1002/chem.201505162
Yang, Zhi, et al. "Addition Reactions of Me3 SiCN with Aldehydes Catalyzed by Aluminum Complexes Containing in their Coordination Sphere O, S, and N Ligands." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 22,20 (2016): 6932-8. doi: https://doi.org/10.1002/chem.201505162
Yang Z, Yi Y, Zhong M, De S, Mondal T, Koley D, Ma X, Zhang D, Roesky HW. Addition Reactions of Me3 SiCN with Aldehydes Catalyzed by Aluminum Complexes Containing in their Coordination Sphere O, S, and N Ligands. Chemistry. 2016 May 10;22(20):6932-8. doi: 10.1002/chem.201505162. Epub 2016 Apr 08. PMID: 27062461.
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Ultrafast Magic-Angle Spinning: Benefits for the Acquisition of Ultrawide-Line NMR Spectra of Heavy Spin-1/2 Nuclei.

Chemphyschem : a European journal of chemical physics and physical chemistry

Pöppler AC, Demers JP, Malon M, Singh AP, Roesky HW, Nishiyama Y, Lange A.
PMID: 26699375
Chemphyschem. 2016 Mar 16;17(6):812-6. doi: 10.1002/cphc.201501136. Epub 2016 Jan 28.

The benefits of the ultrafast magic-angle spinning (MAS) approach for the acquisition of ultrawide-line NMR spectra-spectral simplification, increased mass sensitivity allowing the fast study of small amounts of material, efficient excitation, and application to multiple heavy nuclei-are demonstrated for...

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Pöppler AC, Demers JP, Malon M, et al. Ultrafast Magic-Angle Spinning: Benefits for the Acquisition of Ultrawide-Line NMR Spectra of Heavy Spin-1/2 Nuclei. Chemphyschem. 2016;17(6):812-6doi: 10.1002/cphc.201501136.
Pöppler, A. C., Demers, J. P., Malon, M., Singh, A. P., Roesky, H. W., Nishiyama, Y., & Lange, A. (2016). Ultrafast Magic-Angle Spinning: Benefits for the Acquisition of Ultrawide-Line NMR Spectra of Heavy Spin-1/2 Nuclei. Chemphyschem : a European journal of chemical physics and physical chemistry, 17(6), 812-6. https://doi.org/10.1002/cphc.201501136
Pöppler, Ann-Christin, et al. "Ultrafast Magic-Angle Spinning: Benefits for the Acquisition of Ultrawide-Line NMR Spectra of Heavy Spin-1/2 Nuclei." Chemphyschem : a European journal of chemical physics and physical chemistry vol. 17,6 (2016): 812-6. doi: https://doi.org/10.1002/cphc.201501136
Pöppler AC, Demers JP, Malon M, Singh AP, Roesky HW, Nishiyama Y, Lange A. Ultrafast Magic-Angle Spinning: Benefits for the Acquisition of Ultrawide-Line NMR Spectra of Heavy Spin-1/2 Nuclei. Chemphyschem. 2016 Mar 16;17(6):812-6. doi: 10.1002/cphc.201501136. Epub 2016 Jan 28. PMID: 26699375.
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Correction: Alkynyl-functionalized gold NHC complexes and their coinage metal clusters.

Dalton transactions (Cambridge, England : 2003)

Kiefer C, Bestgen S, Gamer MT, Lebedkin S, Kappes MM, Roesky PW.
PMID: 26815948
Dalton Trans. 2016 Feb 21;45(7):3182. doi: 10.1039/c6dt90020h. Epub 2016 Jan 27.

No abstract available.

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Kiefer C, Bestgen S, Gamer MT, et al. Correction: Alkynyl-functionalized gold NHC complexes and their coinage metal clusters. Dalton Trans. 2016;45(7):3182doi: 10.1039/c6dt90020h.
Kiefer, C., Bestgen, S., Gamer, M. T., Lebedkin, S., Kappes, M. M., & Roesky, P. W. (2016). Correction: Alkynyl-functionalized gold NHC complexes and their coinage metal clusters. Dalton transactions (Cambridge, England : 2003), 45(7), 3182. https://doi.org/10.1039/c6dt90020h
Kiefer, Claude, et al. "Correction: Alkynyl-functionalized gold NHC complexes and their coinage metal clusters." Dalton transactions (Cambridge, England : 2003) vol. 45,7 (2016): 3182. doi: https://doi.org/10.1039/c6dt90020h
Kiefer C, Bestgen S, Gamer MT, Lebedkin S, Kappes MM, Roesky PW. Correction: Alkynyl-functionalized gold NHC complexes and their coinage metal clusters. Dalton Trans. 2016 Feb 21;45(7):3182. doi: 10.1039/c6dt90020h. Epub 2016 Jan 27. PMID: 26815948.
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An open route to asymmetric substituted Al-Al bonds using Al(i)- and Al(iii)-precursors.

Chemical communications (Cambridge, England)

Li B, Kundu S, Zhu H, Keil H, Herbst-Irmer R, Stalke D, Frenking G, Andrada DM, Roesky HW.
PMID: 28180224
Chem Commun (Camb). 2017 Feb 23;53(17):2543-2546. doi: 10.1039/c7cc00325k.

The reaction of LAl: (L = HC[C(Me)N(Ar)]

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Li B, Kundu S, Zhu H, et al. An open route to asymmetric substituted Al-Al bonds using Al(i)- and Al(iii)-precursors. Chem Commun (Camb). 2017;53(17):2543-2546doi: 10.1039/c7cc00325k.
Li, B., Kundu, S., Zhu, H., Keil, H., Herbst-Irmer, R., Stalke, D., Frenking, G., Andrada, D. M., & Roesky, H. W. (2017). An open route to asymmetric substituted Al-Al bonds using Al(i)- and Al(iii)-precursors. Chemical communications (Cambridge, England), 53(17), 2543-2546. https://doi.org/10.1039/c7cc00325k
Li, Bin, et al. "An open route to asymmetric substituted Al-Al bonds using Al(i)- and Al(iii)-precursors." Chemical communications (Cambridge, England) vol. 53,17 (2017): 2543-2546. doi: https://doi.org/10.1039/c7cc00325k
Li B, Kundu S, Zhu H, Keil H, Herbst-Irmer R, Stalke D, Frenking G, Andrada DM, Roesky HW. An open route to asymmetric substituted Al-Al bonds using Al(i)- and Al(iii)-precursors. Chem Commun (Camb). 2017 Feb 23;53(17):2543-2546. doi: 10.1039/c7cc00325k. PMID: 28180224.
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Monomeric siliconthiodichloride trapped by a Lewis base.

Dalton transactions (Cambridge, England : 2003)

Roy S, Mondal KC, Mondal T, Koley D, Dittrich B, Roesky HW.
PMID: 26515288
Dalton Trans. 2015 Dec 14;44(46):19942-7. doi: 10.1039/c5dt03742e.

Thiophosgene (CSCl2), a chemical reagent used in numerous organic syntheses, exists in the monomeric form while its heavier silicon analogue [siliconthiodichloride (SiSCl2)] has been isolated so far as a dimer at room temperature and as a tetramer at 180...

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Roy S, Mondal KC, Mondal T, et al. Monomeric siliconthiodichloride trapped by a Lewis base. Dalton Trans. 2015;44(46):19942-7doi: 10.1039/c5dt03742e.
Roy, S., Mondal, K. C., Mondal, T., Koley, D., Dittrich, B., & Roesky, H. W. (2015). Monomeric siliconthiodichloride trapped by a Lewis base. Dalton transactions (Cambridge, England : 2003), 44(46), 19942-7. https://doi.org/10.1039/c5dt03742e
Roy, Sudipta, et al. "Monomeric siliconthiodichloride trapped by a Lewis base." Dalton transactions (Cambridge, England : 2003) vol. 44,46 (2015): 19942-7. doi: https://doi.org/10.1039/c5dt03742e
Roy S, Mondal KC, Mondal T, Koley D, Dittrich B, Roesky HW. Monomeric siliconthiodichloride trapped by a Lewis base. Dalton Trans. 2015 Dec 14;44(46):19942-7. doi: 10.1039/c5dt03742e. PMID: 26515288.
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Synthesis and characterization of a two-coordinate manganese complex and its reaction with molecular hydrogen at room temperature.

Angewandte Chemie (International ed. in English)

Samuel PP, Mondal KC, Roesky HW, Hermann M, Frenking G, Demeshko S, Meyer F, Stückl AC, Christian JH, Dalal NS, Ungur L, Chibotaru LF, Pröpper K, Meents A, Dittrich B.
PMID: 24038991
Angew Chem Int Ed Engl. 2013 Nov 04;52(45):11817-21. doi: 10.1002/anie.201304642. Epub 2013 Sep 13.

No abstract available.

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Samuel PP, Mondal KC, Roesky HW, et al. Synthesis and characterization of a two-coordinate manganese complex and its reaction with molecular hydrogen at room temperature. Angew Chem Int Ed Engl. 2013;52(45):11817-21doi: 10.1002/anie.201304642.
Samuel, P. P., Mondal, K. C., Roesky, H. W., Hermann, M., Frenking, G., Demeshko, S., Meyer, F., Stückl, A. C., Christian, J. H., Dalal, N. S., Ungur, L., Chibotaru, L. F., Pröpper, K., Meents, A., & Dittrich, B. (2013). Synthesis and characterization of a two-coordinate manganese complex and its reaction with molecular hydrogen at room temperature. Angewandte Chemie (International ed. in English), 52(45), 11817-21. https://doi.org/10.1002/anie.201304642
Samuel, Prinson P, et al. "Synthesis and characterization of a two-coordinate manganese complex and its reaction with molecular hydrogen at room temperature." Angewandte Chemie (International ed. in English) vol. 52,45 (2013): 11817-21. doi: https://doi.org/10.1002/anie.201304642
Samuel PP, Mondal KC, Roesky HW, Hermann M, Frenking G, Demeshko S, Meyer F, Stückl AC, Christian JH, Dalal NS, Ungur L, Chibotaru LF, Pröpper K, Meents A, Dittrich B. Synthesis and characterization of a two-coordinate manganese complex and its reaction with molecular hydrogen at room temperature. Angew Chem Int Ed Engl. 2013 Nov 04;52(45):11817-21. doi: 10.1002/anie.201304642. Epub 2013 Sep 13. PMID: 24038991.
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Stabilization of a two-coordinate mononuclear cobalt(0) compound.

Chemistry (Weinheim an der Bergstrasse, Germany)

Mondal KC, Roy S, De S, Parameswaran P, Dittrich B, Ehret F, Kaim W, Roesky HW.
PMID: 25047010
Chemistry. 2014 Sep 08;20(37):11646-9. doi: 10.1002/chem.201403525. Epub 2014 Jul 22.

Compound (Me2 -cAAC:)2 Co(0) (2; Me2 -cAAC:=cyclic (alkyl) amino carbene; :C(CH2 )(CMe2 )2 N-2,6-iPr2 C6 H3 ) was synthesized by the reduction of the precursor (Me2 -cAAC:)2 Co(I) Cl (1) with KC8 in THF. The cyclic voltammogram of 1...

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Mondal KC, Roy S, De S, et al. Stabilization of a two-coordinate mononuclear cobalt(0) compound. Chemistry. 2014;20(37):11646-9doi: 10.1002/chem.201403525.
Mondal, K. C., Roy, S., De, S., Parameswaran, P., Dittrich, B., Ehret, F., Kaim, W., & Roesky, H. W. (2014). Stabilization of a two-coordinate mononuclear cobalt(0) compound. Chemistry (Weinheim an der Bergstrasse, Germany), 20(37), 11646-9. https://doi.org/10.1002/chem.201403525
Mondal, Kartik Chandra, et al. "Stabilization of a two-coordinate mononuclear cobalt(0) compound." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 20,37 (2014): 11646-9. doi: https://doi.org/10.1002/chem.201403525
Mondal KC, Roy S, De S, Parameswaran P, Dittrich B, Ehret F, Kaim W, Roesky HW. Stabilization of a two-coordinate mononuclear cobalt(0) compound. Chemistry. 2014 Sep 08;20(37):11646-9. doi: 10.1002/chem.201403525. Epub 2014 Jul 22. PMID: 25047010.
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6-(Tetrazol-5-yl)-2,2'-bipyridine: a highly selective ligand for the separation of lanthanides(III) and actinides(III).

Inorganic chemistry

Kratsch J, Beele BB, Koke C, Denecke MA, Geist A, Panak PJ, Roesky PW.
PMID: 24967733
Inorg Chem. 2014 Sep 02;53(17):8949-58. doi: 10.1021/ic5007549. Epub 2014 Jun 26.

The coordination structure in the solid state and solution complexation behavior of 6-(tetrazol-5-yl)-2,2'-bipyridine (HN4bipy) with samarium(III) was investigated as a model system for actinide(III)/lanthanide(III) separations. Two different solid 1:2 complexes, [Sm(N4bipy)2(OH)(H2O)2] (1) and [Sm(N4bipy)2(HCOO)(H2O)2] (2), were obtained from the...

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Kratsch J, Beele BB, Koke C, et al. 6-(Tetrazol-5-yl)-2,2'-bipyridine: a highly selective ligand for the separation of lanthanides(III) and actinides(III). Inorg Chem. 2014;53(17):8949-58doi: 10.1021/ic5007549.
Kratsch, J., Beele, B. B., Koke, C., Denecke, M. A., Geist, A., Panak, P. J., & Roesky, P. W. (2014). 6-(Tetrazol-5-yl)-2,2'-bipyridine: a highly selective ligand for the separation of lanthanides(III) and actinides(III). Inorganic chemistry, 53(17), 8949-58. https://doi.org/10.1021/ic5007549
Kratsch, Jochen, et al. "6-(Tetrazol-5-yl)-2,2'-bipyridine: a highly selective ligand for the separation of lanthanides(III) and actinides(III)." Inorganic chemistry vol. 53,17 (2014): 8949-58. doi: https://doi.org/10.1021/ic5007549
Kratsch J, Beele BB, Koke C, Denecke MA, Geist A, Panak PJ, Roesky PW. 6-(Tetrazol-5-yl)-2,2'-bipyridine: a highly selective ligand for the separation of lanthanides(III) and actinides(III). Inorg Chem. 2014 Sep 02;53(17):8949-58. doi: 10.1021/ic5007549. Epub 2014 Jun 26. PMID: 24967733.
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Cationic zinc organyls as precatalysts for hydroamination reactions.

Chemistry (Weinheim an der Bergstrasse, Germany)

Chilleck MA, Hartenstein L, Braun T, Roesky PW, Braun B.
PMID: 25522205
Chemistry. 2015 Feb 02;21(6):2594-602. doi: 10.1002/chem.201405662. Epub 2014 Dec 17.

The cationic zinc triple-decker complex [Zn2 Cp*3 ](+) [BAr(F) 4 ](-) (BAr(F) 4 =B(3,5-(CF3 )2 C6 H3 )4 ) exhibits catalytic activity in intra- and intermolecular hydroamination reactions in the absence of a cocatalyst. These hydroaminations presumably proceed through...

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Chilleck MA, Hartenstein L, Braun T, et al. Cationic zinc organyls as precatalysts for hydroamination reactions. Chemistry. 2014;21(6):2594-602doi: 10.1002/chem.201405662.
Chilleck, M. A., Hartenstein, L., Braun, T., Roesky, P. W., & Braun, B. (2015). Cationic zinc organyls as precatalysts for hydroamination reactions. Chemistry (Weinheim an der Bergstrasse, Germany), 21(6), 2594-602. https://doi.org/10.1002/chem.201405662
Chilleck, Maren A, et al. "Cationic zinc organyls as precatalysts for hydroamination reactions." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 21,6 (2015): 2594-602. doi: https://doi.org/10.1002/chem.201405662
Chilleck MA, Hartenstein L, Braun T, Roesky PW, Braun B. Cationic zinc organyls as precatalysts for hydroamination reactions. Chemistry. 2015 Feb 02;21(6):2594-602. doi: 10.1002/chem.201405662. Epub 2014 Dec 17. PMID: 25522205.
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Investigations of the Nature of Zn(II) -Si(II) Bonds.

Chemistry (Weinheim an der Bergstrasse, Germany)

Schäfer S, Köppe R, Roesky PW.
PMID: 27072620
Chemistry. 2016 May 17;22(21):7127-33. doi: 10.1002/chem.201505001. Epub 2016 Apr 13.

A series of zinc(II) silylenes was prepared by using the silylene {PhC(NtBu)2 }(C5 Me5 )Si. Whereas reaction of the silylene with ZnX2 (X=Cl, I) gave the halide-bridged dimers [{PhC(NtBu)2 }(C5 Me5 )SiZnX(μ-X)]2 , with ZnR2 (R=Ph, Et, C6 F5...

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Schäfer S, Köppe R, Roesky PW. Investigations of the Nature of Zn(II) -Si(II) Bonds. Chemistry. 2016;22(21):7127-33doi: 10.1002/chem.201505001.
Schäfer, S., Köppe, R., & Roesky, P. W. (2016). Investigations of the Nature of Zn(II) -Si(II) Bonds. Chemistry (Weinheim an der Bergstrasse, Germany), 22(21), 7127-33. https://doi.org/10.1002/chem.201505001
Schäfer, Sebastian, et al. "Investigations of the Nature of Zn(II) -Si(II) Bonds." Chemistry (Weinheim an der Bergstrasse, Germany) vol. 22,21 (2016): 7127-33. doi: https://doi.org/10.1002/chem.201505001
Schäfer S, Köppe R, Roesky PW. Investigations of the Nature of Zn(II) -Si(II) Bonds. Chemistry. 2016 May 17;22(21):7127-33. doi: 10.1002/chem.201505001. Epub 2016 Apr 13. PMID: 27072620.
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Showing 1 to 12 of 474 entries