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Single and Twofold Metal- and Reagent-Free Anodic C-C Cross-Coupling of Phenols with Thiophenes.

Angewandte Chemie (International ed. in English)

Wiebe A, Lips S, Schollmeyer D, Franke R, Waldvogel SR.
PMID: 28967700
Angew Chem Int Ed Engl. 2017 Nov 13;56(46):14727-14731. doi: 10.1002/anie.201708946. Epub 2017 Oct 20.

The first electrochemical dehydrogenative C-C cross-coupling of thiophenes with phenols has been realized. This sustainable and very simple to perform anodic coupling reaction enables access to two classes of compounds of significant interest. The scope for electrochemical C-H-activating cross-coupling...

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Wiebe A, Lips S, Schollmeyer D, et al. Single and Twofold Metal- and Reagent-Free Anodic C-C Cross-Coupling of Phenols with Thiophenes. Angew Chem Int Ed Engl. 2017;56(46):14727-14731doi: 10.1002/anie.201708946.
Wiebe, A., Lips, S., Schollmeyer, D., Franke, R., & Waldvogel, S. R. (2017). Single and Twofold Metal- and Reagent-Free Anodic C-C Cross-Coupling of Phenols with Thiophenes. Angewandte Chemie (International ed. in English), 56(46), 14727-14731. https://doi.org/10.1002/anie.201708946
Wiebe, Anton, et al. "Single and Twofold Metal- and Reagent-Free Anodic C-C Cross-Coupling of Phenols with Thiophenes." Angewandte Chemie (International ed. in English) vol. 56,46 (2017): 14727-14731. doi: https://doi.org/10.1002/anie.201708946
Wiebe A, Lips S, Schollmeyer D, Franke R, Waldvogel SR. Single and Twofold Metal- and Reagent-Free Anodic C-C Cross-Coupling of Phenols with Thiophenes. Angew Chem Int Ed Engl. 2017 Nov 13;56(46):14727-14731. doi: 10.1002/anie.201708946. Epub 2017 Oct 20. PMID: 28967700.
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Novel Stannatrane N(CH.

Inorganic chemistry

Glowacki B, Lutter M, Schollmeyer D, Hiller W, Jurkschat K.
PMID: 27673366
Inorg Chem. 2016 Oct 17;55(20):10218-10228. doi: 10.1021/acs.inorgchem.6b01429. Epub 2016 Sep 27.

The syntheses of the alkanolamine N(CH

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Glowacki B, Lutter M, Schollmeyer D, et al. Novel Stannatrane N(CH. Inorg Chem. 2016;55(20):10218-10228doi: 10.1021/acs.inorgchem.6b01429.
Glowacki, B., Lutter, M., Schollmeyer, D., Hiller, W., & Jurkschat, K. (2016). Novel Stannatrane N(CH. Inorganic chemistry, 55(20), 10218-10228. https://doi.org/10.1021/acs.inorgchem.6b01429
Glowacki, Britta, et al. "Novel Stannatrane N(CH." Inorganic chemistry vol. 55,20 (2016): 10218-10228. doi: https://doi.org/10.1021/acs.inorgchem.6b01429
Glowacki B, Lutter M, Schollmeyer D, Hiller W, Jurkschat K. Novel Stannatrane N(CH. Inorg Chem. 2016 Oct 17;55(20):10218-10228. doi: 10.1021/acs.inorgchem.6b01429. Epub 2016 Sep 27. PMID: 27673366.
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Functionalized Tellurium(II) Thiolates: Tellurium Bis(2-hydroxyethanethiolate) Hydrate, the First H(2)O-Te(II) Complex This work was supported by the Fonds der Chemischen Industrie.

Angewandte Chemie (International ed. in English)

Fleischer H, Schollmeyer D.
PMID: 11091448
Angew Chem Int Ed Engl. 2000 Oct 16;39(20):3705-3706. doi: 10.1002/1521-3773(20001016)39:20<3705::aid-anie3705>3.0.co;2-y.

No abstract available.

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Fleischer H, Schollmeyer D. Functionalized Tellurium(II) Thiolates: Tellurium Bis(2-hydroxyethanethiolate) Hydrate, the First H(2)O-Te(II) Complex This work was supported by the Fonds der Chemischen Industrie. Angew Chem Int Ed Engl. 2000;39(20):3705-3706doi: 10.1002/1521-3773(20001016)39:20<3705::aid-anie3705>3.0.co;2-y.
Fleischer, H., & Schollmeyer, D. (2000). Functionalized Tellurium(II) Thiolates: Tellurium Bis(2-hydroxyethanethiolate) Hydrate, the First H(2)O-Te(II) Complex This work was supported by the Fonds der Chemischen Industrie. Angewandte Chemie (International ed. in English), 39(20), 3705-3706. https://doi.org/10.1002/1521-3773(20001016)39:20<3705::aid-anie3705>3.0.co;2-y
Fleischer, and Schollmeyer. "Functionalized Tellurium(II) Thiolates: Tellurium Bis(2-hydroxyethanethiolate) Hydrate, the First H(2)O-Te(II) Complex This work was supported by the Fonds der Chemischen Industrie." Angewandte Chemie (International ed. in English) vol. 39,20 (2000): 3705-3706. doi: https://doi.org/10.1002/1521-3773(20001016)39:20<3705::aid-anie3705>3.0.co;2-y
Fleischer H, Schollmeyer D. Functionalized Tellurium(II) Thiolates: Tellurium Bis(2-hydroxyethanethiolate) Hydrate, the First H(2)O-Te(II) Complex This work was supported by the Fonds der Chemischen Industrie. Angew Chem Int Ed Engl. 2000 Oct 16;39(20):3705-3706. doi: 10.1002/1521-3773(20001016)39:20<3705::aid-anie3705>3.0.co;2-y. PMID: 11091448.
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The determination of complex stabilities with nearly insoluble host molecules. Complexation of barium(II) with substituted diaza-18-crown-6 ligands in aqueous and methanolic solutions.

Talanta

Buschmann HJ, Cleve E, Torkler S, Schollmeyer E.
PMID: 18967846
Talanta. 2000 Jan 24;51(1):145-9. doi: 10.1016/s0039-9140(99)00255-6.

The complex formation between Ba(2+) and different diaza-18-crown-6 ligands has been studied using a new spectrophotometric method. In the presence of undissolved solid ligand the concentration of the dissolved ligand increases in salt containing solutions due to complex formation....

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Buschmann HJ, Cleve E, Torkler S, et al. The determination of complex stabilities with nearly insoluble host molecules. Complexation of barium(II) with substituted diaza-18-crown-6 ligands in aqueous and methanolic solutions. Talanta. 2000;51(1):145-9doi: 10.1016/s0039-9140(99)00255-6.
Buschmann, H. J., Cleve, E., Torkler, S., & Schollmeyer, E. (2000). The determination of complex stabilities with nearly insoluble host molecules. Complexation of barium(II) with substituted diaza-18-crown-6 ligands in aqueous and methanolic solutions. Talanta, 51(1), 145-9. https://doi.org/10.1016/s0039-9140(99)00255-6
Buschmann, H J, et al. "The determination of complex stabilities with nearly insoluble host molecules. Complexation of barium(II) with substituted diaza-18-crown-6 ligands in aqueous and methanolic solutions." Talanta vol. 51,1 (2000): 145-9. doi: https://doi.org/10.1016/s0039-9140(99)00255-6
Buschmann HJ, Cleve E, Torkler S, Schollmeyer E. The determination of complex stabilities with nearly insoluble host molecules. Complexation of barium(II) with substituted diaza-18-crown-6 ligands in aqueous and methanolic solutions. Talanta. 2000 Jan 24;51(1):145-9. doi: 10.1016/s0039-9140(99)00255-6. PMID: 18967846.
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Nanoscale wettability of self-assembled monolayers investigated by noncontact atomic force microscopy.

Langmuir : the ACS journal of surfaces and colloids

Checco A, Schollmeyer H, Daillant J, Guenoun P, Boukherroub R.
PMID: 16378409
Langmuir. 2006 Jan 03;22(1):116-26. doi: 10.1021/la051419b.

We report on a novel technique to nucleate nanometer-sized droplets on a solid substrate and to image them with minimal perturbation by noncontact atomic force microscopy (NC-AFM). The drop size can be accurately controlled, thus permitting hysteresis measurements. We...

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Checco A, Schollmeyer H, Daillant J, et al. Nanoscale wettability of self-assembled monolayers investigated by noncontact atomic force microscopy. Langmuir. 2006;22(1):116-26doi: 10.1021/la051419b.
Checco, A., Schollmeyer, H., Daillant, J., Guenoun, P., & Boukherroub, R. (2006). Nanoscale wettability of self-assembled monolayers investigated by noncontact atomic force microscopy. Langmuir : the ACS journal of surfaces and colloids, 22(1), 116-26. https://doi.org/10.1021/la051419b
Checco, Antonio, et al. "Nanoscale wettability of self-assembled monolayers investigated by noncontact atomic force microscopy." Langmuir : the ACS journal of surfaces and colloids vol. 22,1 (2006): 116-26. doi: https://doi.org/10.1021/la051419b
Checco A, Schollmeyer H, Daillant J, Guenoun P, Boukherroub R. Nanoscale wettability of self-assembled monolayers investigated by noncontact atomic force microscopy. Langmuir. 2006 Jan 03;22(1):116-26. doi: 10.1021/la051419b. PMID: 16378409.
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Development and calibration of a Thomson parabola with microchannel plate for the detection of laser-accelerated MeV ions.

The Review of scientific instruments

Harres K, Schollmeier M, Brambrink E, Audebert P, Blazević A, Flippo K, Gautier DC, Geissel M, Hegelich BM, Nürnberg F, Schreiber J, Wahl H, Roth M.
PMID: 19044406
Rev Sci Instrum. 2008 Sep;79(9):093306. doi: 10.1063/1.2987687.

This article reports on the development and application of a Thomson parabola (TP) equipped with a (90x70) mm(2) microchannel-plate (MCP) for the analysis of laser-accelerated ions, produced by a high-energy, high-intensity laser system. The MCP allows an online measurement...

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Harres K, Schollmeier M, Brambrink E, et al. Development and calibration of a Thomson parabola with microchannel plate for the detection of laser-accelerated MeV ions. Rev Sci Instrum. 2008;79(9):093306doi: 10.1063/1.2987687.
Harres, K., Schollmeier, M., Brambrink, E., Audebert, P., Blazević, A., Flippo, K., Gautier, D. C., Geissel, M., Hegelich, B. M., Nürnberg, F., Schreiber, J., Wahl, H., & Roth, M. (2008). Development and calibration of a Thomson parabola with microchannel plate for the detection of laser-accelerated MeV ions. The Review of scientific instruments, 79(9), 093306. https://doi.org/10.1063/1.2987687
Harres, K, et al. "Development and calibration of a Thomson parabola with microchannel plate for the detection of laser-accelerated MeV ions." The Review of scientific instruments vol. 79,9 (2008): 093306. doi: https://doi.org/10.1063/1.2987687
Harres K, Schollmeier M, Brambrink E, Audebert P, Blazević A, Flippo K, Gautier DC, Geissel M, Hegelich BM, Nürnberg F, Schreiber J, Wahl H, Roth M. Development and calibration of a Thomson parabola with microchannel plate for the detection of laser-accelerated MeV ions. Rev Sci Instrum. 2008 Sep;79(9):093306. doi: 10.1063/1.2987687. PMID: 19044406.
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Dimeric capsules formed by tetra-CMPO derivatives of (thia)calix[4]arenes.

Chemistry, an Asian journal

Rudzevich V, Kasyan O, Drapailo A, Bolte M, Schollmeyer D, Böhmer V.
PMID: 20397187
Chem Asian J. 2010 Jun 01;5(6):1347-55. doi: 10.1002/asia.200900607.

Thiacalix[4]arene 2, calix[4]arene 3a and its tetraether fixed in the cone conformation 3b form homo- and heterodimeric capsules in apolar solvents, which are held together by a seam of NH...O=P hydrogen bonds between carbamoylmethyl phosphine oxide functions attached to...

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Rudzevich V, Kasyan O, Drapailo A, et al. Dimeric capsules formed by tetra-CMPO derivatives of (thia)calix[4]arenes. Chem Asian J. 2010;5(6):1347-55doi: 10.1002/asia.200900607.
Rudzevich, V., Kasyan, O., Drapailo, A., Bolte, M., Schollmeyer, D., & Böhmer, V. (2010). Dimeric capsules formed by tetra-CMPO derivatives of (thia)calix[4]arenes. Chemistry, an Asian journal, 5(6), 1347-55. https://doi.org/10.1002/asia.200900607
Rudzevich, Valentyn, et al. "Dimeric capsules formed by tetra-CMPO derivatives of (thia)calix[4]arenes." Chemistry, an Asian journal vol. 5,6 (2010): 1347-55. doi: https://doi.org/10.1002/asia.200900607
Rudzevich V, Kasyan O, Drapailo A, Bolte M, Schollmeyer D, Böhmer V. Dimeric capsules formed by tetra-CMPO derivatives of (thia)calix[4]arenes. Chem Asian J. 2010 Jun 01;5(6):1347-55. doi: 10.1002/asia.200900607. PMID: 20397187.
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Tetra-kis{2,4-bis-[(1-oxo-2-pyridyl)-sulfanyl-methyl]mesitylene} acetone hemisolvate 11.5-hydrate.

Acta crystallographica. Section E, Structure reports online

Ravindran Durai Nayagam B, Jebas SR, Selvarathy Grace P, Schollmeyer D.
PMID: 21581590
Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 17;65:o129-30. doi: 10.1107/S1600536808040233.

In the crystal structure of the title compound, 4C(21)H(22)N(2)O(2)S(2)·0.5C(3)H(6)O·11.5H(2)O, there are four crystallographically independent mol-ecules (A, B, C, D) with similar geometries, 11 water mol-ecules and a solvent acetone mol-ecule which is disordered with a water mol-ecule with occupancy...

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Ravindran Durai Nayagam B, Jebas SR, Selvarathy Grace P, et al. Tetra-kis{2,4-bis-[(1-oxo-2-pyridyl)-sulfanyl-methyl]mesitylene} acetone hemisolvate 11.5-hydrate. Acta Crystallogr Sect E Struct Rep Online. 2008;65:o129-30doi: 10.1107/S1600536808040233.
Ravindran Durai Nayagam, B., Jebas, S. R., Selvarathy Grace, P., & Schollmeyer, D. (2008). Tetra-kis{2,4-bis-[(1-oxo-2-pyridyl)-sulfanyl-methyl]mesitylene} acetone hemisolvate 11.5-hydrate. Acta crystallographica. Section E, Structure reports online, 65o129-30. https://doi.org/10.1107/S1600536808040233
Ravindran Durai Nayagam, B, et al. "Tetra-kis{2,4-bis-[(1-oxo-2-pyridyl)-sulfanyl-methyl]mesitylene} acetone hemisolvate 11.5-hydrate." Acta crystallographica. Section E, Structure reports online vol. 65 (2008): o129-30. doi: https://doi.org/10.1107/S1600536808040233
Ravindran Durai Nayagam B, Jebas SR, Selvarathy Grace P, Schollmeyer D. Tetra-kis{2,4-bis-[(1-oxo-2-pyridyl)-sulfanyl-methyl]mesitylene} acetone hemisolvate 11.5-hydrate. Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 17;65:o129-30. doi: 10.1107/S1600536808040233. PMID: 21581590; PMCID: PMC2968049.
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2-(4-Fluoro-phen-yl)-N-{4-[6-(4-fluoro-phen-yl)-2,3-dihydro-imidazo[2,1-b][1,3]thia-zol-5-yl]pyridin-2-yl}acetamide.

Acta crystallographica. Section E, Structure reports online

Selig R, Schollmeyer D, Albrecht W, Laufer S.
PMID: 21579181
Acta Crystallogr Sect E Struct Rep Online. 2010 Apr 21;66:o1132. doi: 10.1107/S1600536810012766.

In the crystal structure of the title compound, C(24)H(18)F(2)N(4)OS, the imidazole system makes dihedral angles of 34.3 (1) and 43.9 (1)°, respectively, with the directly attached 4-fluoro-phenyl and pyridine rings. The crystal structure is stabilized by inter-molecular N-H⋯N hydrogen...

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Selig R, Schollmeyer D, Albrecht W, et al. 2-(4-Fluoro-phen-yl)-N-{4-[6-(4-fluoro-phen-yl)-2,3-dihydro-imidazo[2,1-b][1,3]thia-zol-5-yl]pyridin-2-yl}acetamide. Acta Crystallogr Sect E Struct Rep Online. 2010;66:o1132doi: 10.1107/S1600536810012766.
Selig, R., Schollmeyer, D., Albrecht, W., & Laufer, S. (2010). 2-(4-Fluoro-phen-yl)-N-{4-[6-(4-fluoro-phen-yl)-2,3-dihydro-imidazo[2,1-b][1,3]thia-zol-5-yl]pyridin-2-yl}acetamide. Acta crystallographica. Section E, Structure reports online, 66o1132. https://doi.org/10.1107/S1600536810012766
Selig, Roland, et al. "2-(4-Fluoro-phen-yl)-N-{4-[6-(4-fluoro-phen-yl)-2,3-dihydro-imidazo[2,1-b][1,3]thia-zol-5-yl]pyridin-2-yl}acetamide." Acta crystallographica. Section E, Structure reports online vol. 66 (2010): o1132. doi: https://doi.org/10.1107/S1600536810012766
Selig R, Schollmeyer D, Albrecht W, Laufer S. 2-(4-Fluoro-phen-yl)-N-{4-[6-(4-fluoro-phen-yl)-2,3-dihydro-imidazo[2,1-b][1,3]thia-zol-5-yl]pyridin-2-yl}acetamide. Acta Crystallogr Sect E Struct Rep Online. 2010 Apr 21;66:o1132. doi: 10.1107/S1600536810012766. PMID: 21579181; PMCID: PMC2979114.
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3-(4-Fluoro-phen-yl)-6-meth-oxy-2-(4-pyrid-yl)quinoxaline.

Acta crystallographica. Section E, Structure reports online

Jahns H, Koch P, Schollmeyer D, Laufer S.
PMID: 21582893
Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 20;65:o1626. doi: 10.1107/S1600536809022119.

In the title compound, C(20)H(14)FN(3)O, the quinoxaline system makes dihedral angles of 32.38 (7) and 48.04 (7)° with the 4-fluoro-phenyl and pyridine rings, respectively. The 4-fluoro-phenyl ring makes a dihedral angle of 57.77 (9)° with the pyridine ring. In...

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Jahns H, Koch P, Schollmeyer D, et al. 3-(4-Fluoro-phen-yl)-6-meth-oxy-2-(4-pyrid-yl)quinoxaline. Acta Crystallogr Sect E Struct Rep Online. 2009;65:o1626doi: 10.1107/S1600536809022119.
Jahns, H., Koch, P., Schollmeyer, D., & Laufer, S. (2009). 3-(4-Fluoro-phen-yl)-6-meth-oxy-2-(4-pyrid-yl)quinoxaline. Acta crystallographica. Section E, Structure reports online, 65o1626. https://doi.org/10.1107/S1600536809022119
Jahns, Hartmut, et al. "3-(4-Fluoro-phen-yl)-6-meth-oxy-2-(4-pyrid-yl)quinoxaline." Acta crystallographica. Section E, Structure reports online vol. 65 (2009): o1626. doi: https://doi.org/10.1107/S1600536809022119
Jahns H, Koch P, Schollmeyer D, Laufer S. 3-(4-Fluoro-phen-yl)-6-meth-oxy-2-(4-pyrid-yl)quinoxaline. Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 20;65:o1626. doi: 10.1107/S1600536809022119. PMID: 21582893; PMCID: PMC2969274.
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1-[2-(Benzyl-amino)-4-pyrid-yl]-2-(4-fluoro-phen-yl)ethane-1,2-dione.

Acta crystallographica. Section E, Structure reports online

Jahns H, Koch P, Schollmeyer D, Laufer S.
PMID: 21583289
Acta Crystallogr Sect E Struct Rep Online. 2009 May 29;65:o1451. doi: 10.1107/S1600536809019801.

The crystal structure of the title compound, C(20)H(15)FN(2)O(2), contains two crystallographically independent mol-ecules, which are related by a pseudo-inversion center and linked into dimers via inter-molecular N-H⋯N hydrogen bonds. The 4-fluoro-phenyl ring of mol-ecule A makes dihedral angles of...

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Jahns H, Koch P, Schollmeyer D, et al. 1-[2-(Benzyl-amino)-4-pyrid-yl]-2-(4-fluoro-phen-yl)ethane-1,2-dione. Acta Crystallogr Sect E Struct Rep Online. 2009;65:o1451doi: 10.1107/S1600536809019801.
Jahns, H., Koch, P., Schollmeyer, D., & Laufer, S. (2009). 1-[2-(Benzyl-amino)-4-pyrid-yl]-2-(4-fluoro-phen-yl)ethane-1,2-dione. Acta crystallographica. Section E, Structure reports online, 65o1451. https://doi.org/10.1107/S1600536809019801
Jahns, Hartmut, et al. "1-[2-(Benzyl-amino)-4-pyrid-yl]-2-(4-fluoro-phen-yl)ethane-1,2-dione." Acta crystallographica. Section E, Structure reports online vol. 65 (2009): o1451. doi: https://doi.org/10.1107/S1600536809019801
Jahns H, Koch P, Schollmeyer D, Laufer S. 1-[2-(Benzyl-amino)-4-pyrid-yl]-2-(4-fluoro-phen-yl)ethane-1,2-dione. Acta Crystallogr Sect E Struct Rep Online. 2009 May 29;65:o1451. doi: 10.1107/S1600536809019801. PMID: 21583289; PMCID: PMC2969582.
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N-{4-[3-(4-Fluoro-phen-yl)pyrido[2,3-b]pyrazin-2-yl]-2-pyrid-yl}isopropyl-amine.

Acta crystallographica. Section E, Structure reports online

Koch P, Schollmeyer D, Laufer S.
PMID: 21577998
Acta Crystallogr Sect E Struct Rep Online. 2009 Sep 26;65:o2557. doi: 10.1107/S1600536809038173.

In the crystal structure of the title compound, C(21)H(18)FN(5), the pyridopyrazine ring system forms dihedral angles of 33.27 (7) and 48.69 (9)° with the 4-fluoro-phenyl and pyridine ring, respectively. The dihedral angle of the 4-fluoro-phenyl and pyridine rings is...

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Koch P, Schollmeyer D, Laufer S. N-{4-[3-(4-Fluoro-phen-yl)pyrido[2,3-b]pyrazin-2-yl]-2-pyrid-yl}isopropyl-amine. Acta Crystallogr Sect E Struct Rep Online. 2009;65:o2557doi: 10.1107/S1600536809038173.
Koch, P., Schollmeyer, D., & Laufer, S. (2009). N-{4-[3-(4-Fluoro-phen-yl)pyrido[2,3-b]pyrazin-2-yl]-2-pyrid-yl}isopropyl-amine. Acta crystallographica. Section E, Structure reports online, 65o2557. https://doi.org/10.1107/S1600536809038173
Koch, Pierre, et al. "N-{4-[3-(4-Fluoro-phen-yl)pyrido[2,3-b]pyrazin-2-yl]-2-pyrid-yl}isopropyl-amine." Acta crystallographica. Section E, Structure reports online vol. 65 (2009): o2557. doi: https://doi.org/10.1107/S1600536809038173
Koch P, Schollmeyer D, Laufer S. N-{4-[3-(4-Fluoro-phen-yl)pyrido[2,3-b]pyrazin-2-yl]-2-pyrid-yl}isopropyl-amine. Acta Crystallogr Sect E Struct Rep Online. 2009 Sep 26;65:o2557. doi: 10.1107/S1600536809038173. PMID: 21577998; PMCID: PMC2970374.
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