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Six-membered cyclic nitronates as 1,3-dipoles in formal [3 + 3]-cycloaddition with donor-acceptor cyclopropanes. Synthesis of new type of bicyclic nitrosoacetals.

Organic letters

Gorbacheva EO, Tabolin AA, Novikov RA, Khomutova YA, Nelyubina YV, Tomilov YV, Ioffe SL.
PMID: 23293920
Org Lett. 2013 Jan 18;15(2):350-3. doi: 10.1021/ol303292c. Epub 2013 Jan 07.

The first formal [3 + 3]-cycloaddition of nitronates with donor-acceptor cyclopropanes is reported. The reaction is catalyzed by ytterbium trifluoromethanesulfonate and leads to hitherto unknown bicyclic nitrosoacetals, possessing two annelated six-membered rings.

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Gorbacheva EO, Tabolin AA, Novikov RA, et al. Six-membered cyclic nitronates as 1,3-dipoles in formal [3 + 3]-cycloaddition with donor-acceptor cyclopropanes. Synthesis of new type of bicyclic nitrosoacetals. Org Lett. 2013;15(2):350-3doi: 10.1021/ol303292c.
Gorbacheva, E. O., Tabolin, A. A., Novikov, R. A., Khomutova, Y. A., Nelyubina, Y. V., Tomilov, Y. V., & Ioffe, S. L. (2013). Six-membered cyclic nitronates as 1,3-dipoles in formal [3 + 3]-cycloaddition with donor-acceptor cyclopropanes. Synthesis of new type of bicyclic nitrosoacetals. Organic letters, 15(2), 350-3. https://doi.org/10.1021/ol303292c
Gorbacheva, Evgenia O, et al. "Six-membered cyclic nitronates as 1,3-dipoles in formal [3 + 3]-cycloaddition with donor-acceptor cyclopropanes. Synthesis of new type of bicyclic nitrosoacetals." Organic letters vol. 15,2 (2013): 350-3. doi: https://doi.org/10.1021/ol303292c
Gorbacheva EO, Tabolin AA, Novikov RA, Khomutova YA, Nelyubina YV, Tomilov YV, Ioffe SL. Six-membered cyclic nitronates as 1,3-dipoles in formal [3 + 3]-cycloaddition with donor-acceptor cyclopropanes. Synthesis of new type of bicyclic nitrosoacetals. Org Lett. 2013 Jan 18;15(2):350-3. doi: 10.1021/ol303292c. Epub 2013 Jan 07. PMID: 23293920.
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Hexokinase as a versatile molecular genetic marker for Microsporidia.

Parasitology

Tokarev YS, Timofeev SA, Malysh JM, Tsarev AA, Ignatieva AN, Tomilova OG, Dolgikh VV.
PMID: 30319087
Parasitology. 2019 Apr;146(4):472-478. doi: 10.1017/S0031182018001737. Epub 2018 Oct 15.

Hexokinase (HK) is a core glycolytic enzyme of Microsporidia which regulates host cell metabolic processes. The goal of the present study was to test for the utility of HK for molecular phylogenetics, species identification and molecular detection of microsporidia...

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Tokarev YS, Timofeev SA, Malysh JM, et al. Hexokinase as a versatile molecular genetic marker for Microsporidia. Parasitology. 2018;146(4):472-478doi: 10.1017/S0031182018001737.
Tokarev, Y. S., Timofeev, S. A., Malysh, J. M., Tsarev, A. A., Ignatieva, A. N., Tomilova, O. G., & Dolgikh, V. V. (2019). Hexokinase as a versatile molecular genetic marker for Microsporidia. Parasitology, 146(4), 472-478. https://doi.org/10.1017/S0031182018001737
Tokarev, Yuri S, et al. "Hexokinase as a versatile molecular genetic marker for Microsporidia." Parasitology vol. 146,4 (2019): 472-478. doi: https://doi.org/10.1017/S0031182018001737
Tokarev YS, Timofeev SA, Malysh JM, Tsarev AA, Ignatieva AN, Tomilova OG, Dolgikh VV. Hexokinase as a versatile molecular genetic marker for Microsporidia. Parasitology. 2019 Apr;146(4):472-478. doi: 10.1017/S0031182018001737. Epub 2018 Oct 15. PMID: 30319087.
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Cascade Cleavage of Three-Membered Rings in the Reaction of D-A Cyclopropanes with 4,5-Diazaspiro[2.4]hept-4-enes: A Route to Highly Functionalized Pyrazolines.

The Journal of organic chemistry

Novikov RA, Borisov DD, Zotova MA, Denisov DA, Tkachev YV, Korolev VA, Shulishov EV, Tomilov YV.
PMID: 29873492
J Org Chem. 2018 Aug 03;83(15):7836-7851. doi: 10.1021/acs.joc.8b00725. Epub 2018 Jun 22.

A new cascade process for reactions of donor-acceptor cyclopropanes (DACs) with spiro[cyclopropanepyrazolines] in the presence of EtAlCl

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Novikov RA, Borisov DD, Zotova MA, et al. Cascade Cleavage of Three-Membered Rings in the Reaction of D-A Cyclopropanes with 4,5-Diazaspiro[2.4]hept-4-enes: A Route to Highly Functionalized Pyrazolines. J Org Chem. 2018;83(15):7836-7851doi: 10.1021/acs.joc.8b00725.
Novikov, R. A., Borisov, D. D., Zotova, M. A., Denisov, D. A., Tkachev, Y. V., Korolev, V. A., Shulishov, E. V., & Tomilov, Y. V. (2018). Cascade Cleavage of Three-Membered Rings in the Reaction of D-A Cyclopropanes with 4,5-Diazaspiro[2.4]hept-4-enes: A Route to Highly Functionalized Pyrazolines. The Journal of organic chemistry, 83(15), 7836-7851. https://doi.org/10.1021/acs.joc.8b00725
Novikov, Roman A, et al. "Cascade Cleavage of Three-Membered Rings in the Reaction of D-A Cyclopropanes with 4,5-Diazaspiro[2.4]hept-4-enes: A Route to Highly Functionalized Pyrazolines." The Journal of organic chemistry vol. 83,15 (2018): 7836-7851. doi: https://doi.org/10.1021/acs.joc.8b00725
Novikov RA, Borisov DD, Zotova MA, Denisov DA, Tkachev YV, Korolev VA, Shulishov EV, Tomilov YV. Cascade Cleavage of Three-Membered Rings in the Reaction of D-A Cyclopropanes with 4,5-Diazaspiro[2.4]hept-4-enes: A Route to Highly Functionalized Pyrazolines. J Org Chem. 2018 Aug 03;83(15):7836-7851. doi: 10.1021/acs.joc.8b00725. Epub 2018 Jun 22. PMID: 29873492.
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GaCl.

The Journal of organic chemistry

Zotova MA, Novikov RA, Shulishov EV, Tomilov YV.
PMID: 29961314
J Org Chem. 2018 Aug 03;83(15):8193-8207. doi: 10.1021/acs.joc.8b00959. Epub 2018 Jul 10.

A new process of "inverted" formal [3 + 2]-cycloaddition of donor-acceptor cyclopropanes (DACs) to allylic systems to give polyfunctionalized cyclopentanes has been developed. Unlike the classical version of formal [3 + 2]-cycloaddition, a DAC acts in this process as...

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Zotova MA, Novikov RA, Shulishov EV, et al. GaCl. J Org Chem. 2018;83(15):8193-8207doi: 10.1021/acs.joc.8b00959.
Zotova, M. A., Novikov, R. A., Shulishov, E. V., & Tomilov, Y. V. (2018). GaCl. The Journal of organic chemistry, 83(15), 8193-8207. https://doi.org/10.1021/acs.joc.8b00959
Zotova, Maria A, et al. "GaCl." The Journal of organic chemistry vol. 83,15 (2018): 8193-8207. doi: https://doi.org/10.1021/acs.joc.8b00959
Zotova MA, Novikov RA, Shulishov EV, Tomilov YV. GaCl. J Org Chem. 2018 Aug 03;83(15):8193-8207. doi: 10.1021/acs.joc.8b00959. Epub 2018 Jul 10. PMID: 29961314.
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The Role of Stem Cells in the Therapy of Stroke.

Current neuropharmacology

Ejma M, Madetko N, Brzecka A, Alster P, Budrewicz S, Koszewicz M, Misiuk-Hojło M, Tomilova IK, Somasundaram SG, Kirkland CE, Aliev G.
PMID: 34365923
Curr Neuropharmacol. 2021 Aug 06; doi: 10.2174/1570159X19666210806163352. Epub 2021 Aug 06.

BACKGROUND: Stroke is a major challenge in neurology due to its multifactorial genesis and irreversible consequences. Processes of endogenous post-stroke neurogenesis, although insufficient, may indicate possible direction of future therapy. Multiple research considers stem-cell-based approaches in order to maximize...

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Ejma M, Madetko N, Brzecka A, et al. The Role of Stem Cells in the Therapy of Stroke. Curr Neuropharmacol. 2021;doi: 10.2174/1570159X19666210806163352.
Ejma, M., Madetko, N., Brzecka, A., Alster, P., Budrewicz, S., Koszewicz, M., Misiuk-Hojło, M., Tomilova, I. K., Somasundaram, S. G., Kirkland, C. E., & Aliev, G. (2021). The Role of Stem Cells in the Therapy of Stroke. Current neuropharmacology, . https://doi.org/10.2174/1570159X19666210806163352
Ejma, Maria, et al. "The Role of Stem Cells in the Therapy of Stroke." Current neuropharmacology vol. (2021). doi: https://doi.org/10.2174/1570159X19666210806163352
Ejma M, Madetko N, Brzecka A, Alster P, Budrewicz S, Koszewicz M, Misiuk-Hojło M, Tomilova IK, Somasundaram SG, Kirkland CE, Aliev G. The Role of Stem Cells in the Therapy of Stroke. Curr Neuropharmacol. 2021 Aug 06; doi: 10.2174/1570159X19666210806163352. Epub 2021 Aug 06. PMID: 34365923.
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Three-Component Gallium(III)-Promoted Addition of Halide Anions and Acetylenes to Donor-Acceptor Cyclopropanes.

Angewandte Chemie (International ed. in English)

Novikov RA, Borisov DD, Tarasova AV, Tkachev YV, Tomilov YV.
PMID: 29897640
Angew Chem Int Ed Engl. 2018 Aug 06;57(32):10293-10298. doi: 10.1002/anie.201803541. Epub 2018 Jul 17.

A new strategy for the three-component addition of halide anions and acetylenes to donor-acceptor cyclopropanes (DACs) is presented. This reaction, which occurs with high E selectivity, is promoted by gallium(III) salts and based on the 1,2-zwitterionic reactivity of DACs....

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Novikov RA, Borisov DD, Tarasova AV, et al. Three-Component Gallium(III)-Promoted Addition of Halide Anions and Acetylenes to Donor-Acceptor Cyclopropanes. Angew Chem Int Ed Engl. 2018;57(32):10293-10298doi: 10.1002/anie.201803541.
Novikov, R. A., Borisov, D. D., Tarasova, A. V., Tkachev, Y. V., & Tomilov, Y. V. (2018). Three-Component Gallium(III)-Promoted Addition of Halide Anions and Acetylenes to Donor-Acceptor Cyclopropanes. Angewandte Chemie (International ed. in English), 57(32), 10293-10298. https://doi.org/10.1002/anie.201803541
Novikov, Roman A, et al. "Three-Component Gallium(III)-Promoted Addition of Halide Anions and Acetylenes to Donor-Acceptor Cyclopropanes." Angewandte Chemie (International ed. in English) vol. 57,32 (2018): 10293-10298. doi: https://doi.org/10.1002/anie.201803541
Novikov RA, Borisov DD, Tarasova AV, Tkachev YV, Tomilov YV. Three-Component Gallium(III)-Promoted Addition of Halide Anions and Acetylenes to Donor-Acceptor Cyclopropanes. Angew Chem Int Ed Engl. 2018 Aug 06;57(32):10293-10298. doi: 10.1002/anie.201803541. Epub 2018 Jul 17. PMID: 29897640.
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(2-Fluoroallyl)boration of Ketones with (2-Fluoroallyl)boronates.

The Journal of organic chemistry

Novikov MA, Bobrova AY, Mezentsev IA, Medvedev MG, Tomilov YV.
PMID: 32309945
J Org Chem. 2020 May 15;85(10):6295-6308. doi: 10.1021/acs.joc.9b03445. Epub 2020 May 05.

Efficient routes toward activation of

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Novikov MA, Bobrova AY, Mezentsev IA, et al. (2-Fluoroallyl)boration of Ketones with (2-Fluoroallyl)boronates. J Org Chem. 2020;85(10):6295-6308doi: 10.1021/acs.joc.9b03445.
Novikov, M. A., Bobrova, A. Y., Mezentsev, I. A., Medvedev, M. G., & Tomilov, Y. V. (2020). (2-Fluoroallyl)boration of Ketones with (2-Fluoroallyl)boronates. The Journal of organic chemistry, 85(10), 6295-6308. https://doi.org/10.1021/acs.joc.9b03445
Novikov, Maxim A, et al. "(2-Fluoroallyl)boration of Ketones with (2-Fluoroallyl)boronates." The Journal of organic chemistry vol. 85,10 (2020): 6295-6308. doi: https://doi.org/10.1021/acs.joc.9b03445
Novikov MA, Bobrova AY, Mezentsev IA, Medvedev MG, Tomilov YV. (2-Fluoroallyl)boration of Ketones with (2-Fluoroallyl)boronates. J Org Chem. 2020 May 15;85(10):6295-6308. doi: 10.1021/acs.joc.9b03445. Epub 2020 May 05. PMID: 32309945.
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GaCl3 -Mediated Reactions of Donor-Acceptor Cyclopropanes with Aromatic Aldehydes.

Angewandte Chemie (International ed. in English)

Borisov DD, Novikov RA, Tomilov YV.
PMID: 27573178
Angew Chem Int Ed Engl. 2016 Sep 26;55(40):12233-7. doi: 10.1002/anie.201603927. Epub 2016 Aug 30.

A new strategy for cascade assembly of substituted indenes and polycyclic lactones based on reactions of donor-acceptor cyclopropanes and styrylmalonates with aromatic aldehydes in the presence of GaCl3 has been developed. The use of GaCl3 makes it possible to...

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Borisov DD, Novikov RA, Tomilov YV. GaCl3 -Mediated Reactions of Donor-Acceptor Cyclopropanes with Aromatic Aldehydes. Angew Chem Int Ed Engl. 2016;55(40):12233-7doi: 10.1002/anie.201603927.
Borisov, D. D., Novikov, R. A., & Tomilov, Y. V. (2016). GaCl3 -Mediated Reactions of Donor-Acceptor Cyclopropanes with Aromatic Aldehydes. Angewandte Chemie (International ed. in English), 55(40), 12233-7. https://doi.org/10.1002/anie.201603927
Borisov, Denis D, et al. "GaCl3 -Mediated Reactions of Donor-Acceptor Cyclopropanes with Aromatic Aldehydes." Angewandte Chemie (International ed. in English) vol. 55,40 (2016): 12233-7. doi: https://doi.org/10.1002/anie.201603927
Borisov DD, Novikov RA, Tomilov YV. GaCl3 -Mediated Reactions of Donor-Acceptor Cyclopropanes with Aromatic Aldehydes. Angew Chem Int Ed Engl. 2016 Sep 26;55(40):12233-7. doi: 10.1002/anie.201603927. Epub 2016 Aug 30. PMID: 27573178.
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Interplay between Fungal Infection and Bacterial Associates in the Wax Moth .

Journal of fungi (Basel, Switzerland)

Kryukov VY, Kosman E, Tomilova O, Polenogova O, Rotskaya U, Tyurin M, Alikina T, Yaroslavtseva O, Kabilov M, Glupov V.
PMID: 32927906
J Fungi (Basel). 2020 Sep 10;6(3). doi: 10.3390/jof6030170.

Various insect bacterial associates are involved in pathogeneses caused by entomopathogenic fungi. The outcome of infection (fungal growth or decomposition) may depend on environmental factors such as temperature. The aim of this study was to analyze the bacterial communities...

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Kryukov VY, Kosman E, Tomilova O, et al. Interplay between Fungal Infection and Bacterial Associates in the Wax Moth . J Fungi (Basel). 2020;6(3)doi: 10.3390/jof6030170.
Kryukov, V. Y., Kosman, E., Tomilova, O., Polenogova, O., Rotskaya, U., Tyurin, M., Alikina, T., Yaroslavtseva, O., Kabilov, M., & Glupov, V. (2020). Interplay between Fungal Infection and Bacterial Associates in the Wax Moth . Journal of fungi (Basel, Switzerland), 6(3), . https://doi.org/10.3390/jof6030170
Kryukov, Vadim Yu, et al. "Interplay between Fungal Infection and Bacterial Associates in the Wax Moth ." Journal of fungi (Basel, Switzerland) vol. 6,3 (2020). doi: https://doi.org/10.3390/jof6030170
Kryukov VY, Kosman E, Tomilova O, Polenogova O, Rotskaya U, Tyurin M, Alikina T, Yaroslavtseva O, Kabilov M, Glupov V. Interplay between Fungal Infection and Bacterial Associates in the Wax Moth . J Fungi (Basel). 2020 Sep 10;6(3). doi: 10.3390/jof6030170. PMID: 32927906; PMCID: PMC7558722.
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An example of a possible leech-bryozoan association in freshwater.

ZooKeys

Klass AL, Sokolova SE, Kondakov AV, Bespalaya YV, Gofarov MY, Tomilova AA, Vikhrev IV, Bolotov IN.
PMID: 30416338
Zookeys. 2018 Nov 01;(794):23-30. doi: 10.3897/zookeys.794.28088. eCollection 2018.

Associations of various invertebrate species with bryozoans and sponges are a well-known marine phenomenon but such epizooic communities are far less diverse in freshwater environments. Here an occurrence of numerous leeches Alboglossiphoniacf.papillosa (Braun, 1805), in interstitial spaces between zooids...

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Klass AL, Sokolova SE, Kondakov AV, et al. An example of a possible leech-bryozoan association in freshwater. Zookeys. 2018;(794):23-30doi: 10.3897/zookeys.794.28088.
Klass, A. L., Sokolova, S. E., Kondakov, A. V., Bespalaya, Y. V., Gofarov, M. Y., Tomilova, A. A., Vikhrev, I. V., & Bolotov, I. N. (2018). An example of a possible leech-bryozoan association in freshwater. ZooKeys, (794), 23-30. https://doi.org/10.3897/zookeys.794.28088
Klass, Anna L, et al. "An example of a possible leech-bryozoan association in freshwater." ZooKeys vol. ,794 (2018): 23-30. doi: https://doi.org/10.3897/zookeys.794.28088
Klass AL, Sokolova SE, Kondakov AV, Bespalaya YV, Gofarov MY, Tomilova AA, Vikhrev IV, Bolotov IN. An example of a possible leech-bryozoan association in freshwater. Zookeys. 2018 Nov 01;(794):23-30. doi: 10.3897/zookeys.794.28088. eCollection 2018. PMID: 30416338; PMCID: PMC6224368.
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Optical readout of controlled monomer-dimer self-assembly.

Dalton transactions (Cambridge, England : 2003)

Tarakanov PA, Tarakanova EN, Dorovatovskii PV, Zubavichus YV, Khrustalev VN, Trashin SA, De Wael K, Neganova ME, Mischenko DV, Sessler JL, Stuzhin PA, Pushkarev VE, Tomilova LG.
PMID: 29664072
Dalton Trans. 2018 Oct 16;47(40):14169-14173. doi: 10.1039/c8dt00384j.

5,7-Substituted 1,4-diazepinoporphyrazine magnesium(ii) complexes were synthesized via Mg(ii)-alkoxide templated macrocyclization. A single crystal growth synchrotron diffraction analysis permitted what is to our knowledge the first structural characterization of a 1,4-diazepinoporphyrazine. It exists as a dimer in the solid state....

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Tarakanov PA, Tarakanova EN, Dorovatovskii PV, et al. Optical readout of controlled monomer-dimer self-assembly. Dalton Trans. 2018;47(40):14169-14173doi: 10.1039/c8dt00384j.
Tarakanov, P. A., Tarakanova, E. N., Dorovatovskii, P. V., Zubavichus, Y. V., Khrustalev, V. N., Trashin, S. A., De Wael, K., Neganova, M. E., Mischenko, D. V., Sessler, J. L., Stuzhin, P. A., Pushkarev, V. E., & Tomilova, L. G. (2018). Optical readout of controlled monomer-dimer self-assembly. Dalton transactions (Cambridge, England : 2003), 47(40), 14169-14173. https://doi.org/10.1039/c8dt00384j
Tarakanov, Pavel A, et al. "Optical readout of controlled monomer-dimer self-assembly." Dalton transactions (Cambridge, England : 2003) vol. 47,40 (2018): 14169-14173. doi: https://doi.org/10.1039/c8dt00384j
Tarakanov PA, Tarakanova EN, Dorovatovskii PV, Zubavichus YV, Khrustalev VN, Trashin SA, De Wael K, Neganova ME, Mischenko DV, Sessler JL, Stuzhin PA, Pushkarev VE, Tomilova LG. Optical readout of controlled monomer-dimer self-assembly. Dalton Trans. 2018 Oct 16;47(40):14169-14173. doi: 10.1039/c8dt00384j. PMID: 29664072.
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Styrylmalonates as an Alternative to Donor-Acceptor Cyclopropanes in the Reactions with Aldehydes: A Route to 5,6-Dihydropyran-2-ones.

Organic letters

Borisov DD, Novikov RA, Eltysheva AS, Tkachev YV, Tomilov YV.
PMID: 28661160
Org Lett. 2017 Jul 21;19(14):3731-3734. doi: 10.1021/acs.orglett.7b01556. Epub 2017 Jun 29.

A new strategy for modifying the reactivity of donor-acceptor cyclopropanes (DAC) has been suggested. It involves the use of isomeric styrylmalonates as alternative sources of reactive intermediates. The efficiency of the approach has been demonstrated in reactions with aromatic...

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Borisov DD, Novikov RA, Eltysheva AS, et al. Styrylmalonates as an Alternative to Donor-Acceptor Cyclopropanes in the Reactions with Aldehydes: A Route to 5,6-Dihydropyran-2-ones. Org Lett. 2017;19(14):3731-3734doi: 10.1021/acs.orglett.7b01556.
Borisov, D. D., Novikov, R. A., Eltysheva, A. S., Tkachev, Y. V., & Tomilov, Y. V. (2017). Styrylmalonates as an Alternative to Donor-Acceptor Cyclopropanes in the Reactions with Aldehydes: A Route to 5,6-Dihydropyran-2-ones. Organic letters, 19(14), 3731-3734. https://doi.org/10.1021/acs.orglett.7b01556
Borisov, Denis D, et al. "Styrylmalonates as an Alternative to Donor-Acceptor Cyclopropanes in the Reactions with Aldehydes: A Route to 5,6-Dihydropyran-2-ones." Organic letters vol. 19,14 (2017): 3731-3734. doi: https://doi.org/10.1021/acs.orglett.7b01556
Borisov DD, Novikov RA, Eltysheva AS, Tkachev YV, Tomilov YV. Styrylmalonates as an Alternative to Donor-Acceptor Cyclopropanes in the Reactions with Aldehydes: A Route to 5,6-Dihydropyran-2-ones. Org Lett. 2017 Jul 21;19(14):3731-3734. doi: 10.1021/acs.orglett.7b01556. Epub 2017 Jun 29. PMID: 28661160.
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