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Synthesis and structural characterization of functionalized dimeric aluminophosphonates and a monomeric gallophosphonate anion.

Inorganic chemistry

Chakraborty D, Horchler S, Krätzner R, Varkey SP, Pinkas J, Roesky HW, Usón I, Noltemeyer M, Schmidt HG.
PMID: 11350243
Inorg Chem. 2001 May 21;40(11):2620-4. doi: 10.1021/ic000797v.

Reaction of t-BuP(O)(OSiMe(3))(OH) with Me(3)Al leads to the formation of [Me(2)Al(mu-O)(2)P(OSiMe(3))(t-Bu)](2) (1) whereas Me(2)AlCl reacts with Ph(2)P(O)(OH) to yield [(Cl)(Me)Al(mu-O)(2)PPh(2)](2) (2). These compounds represent the first examples of functionalized dimeric four-ring type aluminophosphonate systems. The double four-ring type gallophosphonate,...

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Chakraborty D, Horchler S, Krätzner R, et al. Synthesis and structural characterization of functionalized dimeric aluminophosphonates and a monomeric gallophosphonate anion. Inorg Chem. 2001;40(11):2620-4doi: 10.1021/ic000797v.
Chakraborty, D., Horchler, S., Krätzner, R., Varkey, S. P., Pinkas, J., Roesky, H. W., Usón, I., Noltemeyer, M., & Schmidt, H. G. (2001). Synthesis and structural characterization of functionalized dimeric aluminophosphonates and a monomeric gallophosphonate anion. Inorganic chemistry, 40(11), 2620-4. https://doi.org/10.1021/ic000797v
Chakraborty, D, et al. "Synthesis and structural characterization of functionalized dimeric aluminophosphonates and a monomeric gallophosphonate anion." Inorganic chemistry vol. 40,11 (2001): 2620-4. doi: https://doi.org/10.1021/ic000797v
Chakraborty D, Horchler S, Krätzner R, Varkey SP, Pinkas J, Roesky HW, Usón I, Noltemeyer M, Schmidt HG. Synthesis and structural characterization of functionalized dimeric aluminophosphonates and a monomeric gallophosphonate anion. Inorg Chem. 2001 May 21;40(11):2620-4. doi: 10.1021/ic000797v. PMID: 11350243.
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A Facile Route to Group 13 Difluorodiorganometalates:.

Angewandte Chemie (International ed. in English)

Roesky HW, Stasch A, Hatop H, Rennekamp C, H Hamilton D, Noltemeyer M, Schmidt HG.
PMID: 10649364
Angew Chem Int Ed Engl. 2000 Jan;39(1):171-173.

A facile synthesis utilizing tetra-n-butylammonium hydrogen difluoride and Group 13 alkyl compounds leads to the soluble salts 1 - 4. Compound 1 is the smallest difluoro-diorganoaluminate so far characterized. The corresponding gallium and indium derivatives 3 and 4 are...

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Roesky HW, Stasch A, Hatop H, et al. A Facile Route to Group 13 Difluorodiorganometalates:. Angew Chem Int Ed Engl. 2000;39(1):171-173
Roesky, H. W., Stasch, A., Hatop, H., Rennekamp, C., H Hamilton D, Noltemeyer, M., & Schmidt, H. G. (2000). A Facile Route to Group 13 Difluorodiorganometalates:. Angewandte Chemie (International ed. in English), 39(1), 171-173.
Roesky, et al. "A Facile Route to Group 13 Difluorodiorganometalates:." Angewandte Chemie (International ed. in English) vol. 39,1 (2000): 171-173.
Roesky HW, Stasch A, Hatop H, Rennekamp C, H Hamilton D, Noltemeyer M, Schmidt HG. A Facile Route to Group 13 Difluorodiorganometalates:. Angew Chem Int Ed Engl. 2000 Jan;39(1):171-173. PMID: 10649364.
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Organometallic Fluorides of Zirconium and Hafnium in the Synthesis of Carboxylate Complexes: Molecular Structures of [{(eta(5)-C(5)Me(5))ZrF(OCOCF(3))(2)}(2)] and [(eta(5)-C(5)Me(5))(2)Zr(OCOCF(3))(2)].

Inorganic chemistry

Dorn H, Shah SA, Parisini E, Noltemeyer M, Schmidt HG, Roesky HW.
PMID: 11666903
Inorg Chem. 1996 Nov 20;35(24):7181-7184. doi: 10.1021/ic9604977.

The reaction of [(eta(5)-C(5)Me(5))ZrF(3)] and [(eta(5)-C(5)Me(5))HfF(3)] with Me(3)SiOCOCF(3) yields the dinuclear complexes [{(eta(5)-C(5)Me(5))ZrF(OCOCF(3))(2)}(2)] (1) and [{(eta(5)-C(5)Me(5))HfF(OCOCF(3))(2)}(2)] (2), regardless of the molar ratio employed. [(eta(5)-C(5)Me(5))(2)ZrF(2)] reacts with 1 and 2 equiv of Me(3)SiOCOCF(3) to form the mononuclear compounds [(eta(5)-C(5)Me(5))(2)Zr(OCOCF(3))(2)] (3)...

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Dorn H, Shah SA, Parisini E, et al. Organometallic Fluorides of Zirconium and Hafnium in the Synthesis of Carboxylate Complexes: Molecular Structures of [{(eta(5)-C(5)Me(5))ZrF(OCOCF(3))(2)}(2)] and [(eta(5)-C(5)Me(5))(2)Zr(OCOCF(3))(2)]. Inorg Chem. 1996;35(24):7181-7184doi: 10.1021/ic9604977.
Dorn, H., Shah, S. A., Parisini, E., Noltemeyer, M., Schmidt, H. G., & Roesky, H. W. (1996). Organometallic Fluorides of Zirconium and Hafnium in the Synthesis of Carboxylate Complexes: Molecular Structures of [{(eta(5)-C(5)Me(5))ZrF(OCOCF(3))(2)}(2)] and [(eta(5)-C(5)Me(5))(2)Zr(OCOCF(3))(2)]. Inorganic chemistry, 35(24), 7181-7184. https://doi.org/10.1021/ic9604977
Dorn, Hendrik, et al. "Organometallic Fluorides of Zirconium and Hafnium in the Synthesis of Carboxylate Complexes: Molecular Structures of [{(eta(5)-C(5)Me(5))ZrF(OCOCF(3))(2)}(2)] and [(eta(5)-C(5)Me(5))(2)Zr(OCOCF(3))(2)]." Inorganic chemistry vol. 35,24 (1996): 7181-7184. doi: https://doi.org/10.1021/ic9604977
Dorn H, Shah SA, Parisini E, Noltemeyer M, Schmidt HG, Roesky HW. Organometallic Fluorides of Zirconium and Hafnium in the Synthesis of Carboxylate Complexes: Molecular Structures of [{(eta(5)-C(5)Me(5))ZrF(OCOCF(3))(2)}(2)] and [(eta(5)-C(5)Me(5))(2)Zr(OCOCF(3))(2)]. Inorg Chem. 1996 Nov 20;35(24):7181-7184. doi: 10.1021/ic9604977. PMID: 11666903.
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Synthesis and characterization of HC[C(Me)N(C(6)H(3)-2,6-i-Pr(2))](2)MX(2) (M = Al, X = Cl, I; M = Ga, In, X = Me, Cl, I): sterically encumbered beta-diketiminate group 13 metal derivatives.

Inorganic chemistry

Stender M, Eichler BE, Hardman NJ, Power PP, Prust J, Noltemeyer M, Roesky HW.
PMID: 11375697
Inorg Chem. 2001 Jun 04;40(12):2794-9. doi: 10.1021/ic001311d.

A series of group 13 metal complexes featuring the beta-diketiminate ligand [[(C(6)H(3)-2,6-i-Pr(2))NC(Me)](2)CH](-) (i.e., [Dipp(2)nacnac](-), Dipp = C(6)H(3)-2,6-i-Pr(2)) have been prepared and spectroscopically and structurally characterized. The chloride derivatives Dipp(2)nacnacMCl(2) (M = Al (3), Ga (5), In (8)) were isolated...

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Stender M, Eichler BE, Hardman NJ, et al. Synthesis and characterization of HC[C(Me)N(C(6)H(3)-2,6-i-Pr(2))](2)MX(2) (M = Al, X = Cl, I; M = Ga, In, X = Me, Cl, I): sterically encumbered beta-diketiminate group 13 metal derivatives. Inorg Chem. 2001;40(12):2794-9doi: 10.1021/ic001311d.
Stender, M., Eichler, B. E., Hardman, N. J., Power, P. P., Prust, J., Noltemeyer, M., & Roesky, H. W. (2001). Synthesis and characterization of HC[C(Me)N(C(6)H(3)-2,6-i-Pr(2))](2)MX(2) (M = Al, X = Cl, I; M = Ga, In, X = Me, Cl, I): sterically encumbered beta-diketiminate group 13 metal derivatives. Inorganic chemistry, 40(12), 2794-9. https://doi.org/10.1021/ic001311d
Stender, M, et al. "Synthesis and characterization of HC[C(Me)N(C(6)H(3)-2,6-i-Pr(2))](2)MX(2) (M = Al, X = Cl, I; M = Ga, In, X = Me, Cl, I): sterically encumbered beta-diketiminate group 13 metal derivatives." Inorganic chemistry vol. 40,12 (2001): 2794-9. doi: https://doi.org/10.1021/ic001311d
Stender M, Eichler BE, Hardman NJ, Power PP, Prust J, Noltemeyer M, Roesky HW. Synthesis and characterization of HC[C(Me)N(C(6)H(3)-2,6-i-Pr(2))](2)MX(2) (M = Al, X = Cl, I; M = Ga, In, X = Me, Cl, I): sterically encumbered beta-diketiminate group 13 metal derivatives. Inorg Chem. 2001 Jun 04;40(12):2794-9. doi: 10.1021/ic001311d. PMID: 11375697.
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First Mixed Fluoro-Chloro Group 4 Organometallics: Synthesis and Spectroscopic and Structural Characterization of [{(C(5)Me(5))ZrF(2)Cl}(4)], [{(C(5)Me(5))HfF(2)Cl}(4)], [(C(5)Me(5))(4)Zr(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(5))(4)Hf(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(4)Et)(2)ZrClF], and [(C(5)Me(5))(2)HfClF].

Inorganic chemistry

Murphy EF, Lübben T, Herzog A, Roesky HW, Demsar A, Noltemeyer M, Schmidt HG.
PMID: 11666158
Inorg Chem. 1996 Jan 03;35(1):23-29. doi: 10.1021/ic950822a.

Tetrameric [{(C(5)Me(5))MF(3)}(4)] (M = Zr, Hf) react smoothly with Me(3)SiCl in CH(2)Cl(2) at room temperature to give [{(C(5)Me(5))ZrF(2)Cl}(4)] (1) and [{(C(5)Me(5))HfF(2)Cl}(4)] (2), respectively, in high yield. Treatment of [{(C(5)Me(5))MF(3)}(4)] (M = Zr, Hf) with Me(2)AlCl in toluene gives mixtures...

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Murphy EF, Lübben T, Herzog A, et al. First Mixed Fluoro-Chloro Group 4 Organometallics: Synthesis and Spectroscopic and Structural Characterization of [{(C(5)Me(5))ZrF(2)Cl}(4)], [{(C(5)Me(5))HfF(2)Cl}(4)], [(C(5)Me(5))(4)Zr(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(5))(4)Hf(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(4)Et)(2)ZrClF], and [(C(5)Me(5))(2)HfClF]. Inorg Chem. 1996;35(1):23-29doi: 10.1021/ic950822a.
Murphy, E. F., Lübben, T., Herzog, A., Roesky, H. W., Demsar, A., Noltemeyer, M., & Schmidt, H. G. (1996). First Mixed Fluoro-Chloro Group 4 Organometallics: Synthesis and Spectroscopic and Structural Characterization of [{(C(5)Me(5))ZrF(2)Cl}(4)], [{(C(5)Me(5))HfF(2)Cl}(4)], [(C(5)Me(5))(4)Zr(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(5))(4)Hf(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(4)Et)(2)ZrClF], and [(C(5)Me(5))(2)HfClF]. Inorganic chemistry, 35(1), 23-29. https://doi.org/10.1021/ic950822a
Murphy, Eamonn F., et al. "First Mixed Fluoro-Chloro Group 4 Organometallics: Synthesis and Spectroscopic and Structural Characterization of [{(C(5)Me(5))ZrF(2)Cl}(4)], [{(C(5)Me(5))HfF(2)Cl}(4)], [(C(5)Me(5))(4)Zr(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(5))(4)Hf(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(4)Et)(2)ZrClF], and [(C(5)Me(5))(2)HfClF]." Inorganic chemistry vol. 35,1 (1996): 23-29. doi: https://doi.org/10.1021/ic950822a
Murphy EF, Lübben T, Herzog A, Roesky HW, Demsar A, Noltemeyer M, Schmidt HG. First Mixed Fluoro-Chloro Group 4 Organometallics: Synthesis and Spectroscopic and Structural Characterization of [{(C(5)Me(5))ZrF(2)Cl}(4)], [{(C(5)Me(5))HfF(2)Cl}(4)], [(C(5)Me(5))(4)Zr(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(5))(4)Hf(4)(&mgr;-F)(2)(&mgr;-F(2))(2)(&mgr;-Cl)(2)Cl(4)], [(C(5)Me(4)Et)(2)ZrClF], and [(C(5)Me(5))(2)HfClF]. Inorg Chem. 1996 Jan 03;35(1):23-29. doi: 10.1021/ic950822a. PMID: 11666158.
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Organotitanoxanes [C(5)Me(5)TiMe(2)](2)(mu-O) and [(C(5)Me(5)(4)Ti(4)Me(2)](mu-O)(5): synthesis and crystal structures.

Inorganic chemistry

Varkey SP, Schormann M, Pape T, Roesky HW, Noltemeyer M, Herbst-Irmer R, Schmidt HG.
PMID: 11327924
Inorg Chem. 2001 May 07;40(10):2427-9. doi: 10.1021/ic0013072.

No abstract available.

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Varkey SP, Schormann M, Pape T, et al. Organotitanoxanes [C(5)Me(5)TiMe(2)](2)(mu-O) and [(C(5)Me(5)(4)Ti(4)Me(2)](mu-O)(5): synthesis and crystal structures. Inorg Chem. 2001;40(10):2427-9doi: 10.1021/ic0013072.
Varkey, S. P., Schormann, M., Pape, T., Roesky, H. W., Noltemeyer, M., Herbst-Irmer, R., & Schmidt, H. G. (2001). Organotitanoxanes [C(5)Me(5)TiMe(2)](2)(mu-O) and [(C(5)Me(5)(4)Ti(4)Me(2)](mu-O)(5): synthesis and crystal structures. Inorganic chemistry, 40(10), 2427-9. https://doi.org/10.1021/ic0013072
Varkey, S P, et al. "Organotitanoxanes [C(5)Me(5)TiMe(2)](2)(mu-O) and [(C(5)Me(5)(4)Ti(4)Me(2)](mu-O)(5): synthesis and crystal structures." Inorganic chemistry vol. 40,10 (2001): 2427-9. doi: https://doi.org/10.1021/ic0013072
Varkey SP, Schormann M, Pape T, Roesky HW, Noltemeyer M, Herbst-Irmer R, Schmidt HG. Organotitanoxanes [C(5)Me(5)TiMe(2)](2)(mu-O) and [(C(5)Me(5)(4)Ti(4)Me(2)](mu-O)(5): synthesis and crystal structures. Inorg Chem. 2001 May 07;40(10):2427-9. doi: 10.1021/ic0013072. PMID: 11327924.
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Aluminacyclopropene: syntheses, characterization, and reactivity toward terminal alkynes.

Journal of the American Chemical Society

Zhu H, Oswald RB, Fan H, Roesky HW, Ma Q, Yang Z, Schmidt HG, Noltemeyer M, Starke K, Hosmane NS.
PMID: 16608344
J Am Chem Soc. 2006 Apr 19;128(15):5100-8. doi: 10.1021/ja057731p.

Reactions of LAl with ethyne, mono- and disubstituted alkynes, and diyne to aluminacyclopropene LAl[eta2-C2(R1)(R2)] ((L = HC[(CMe)(NAr)]2, Ar = 2,6-iPr2C6H3); R1 = R2 = H, (1); R1 = H, R2 = Ph, (2); R1 = R2 = Me, (3);...

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Zhu H, Oswald RB, Fan H, et al. Aluminacyclopropene: syntheses, characterization, and reactivity toward terminal alkynes. J Am Chem Soc. 2006;128(15):5100-8doi: 10.1021/ja057731p.
Zhu, H., Oswald, R. B., Fan, H., Roesky, H. W., Ma, Q., Yang, Z., Schmidt, H. G., Noltemeyer, M., Starke, K., & Hosmane, N. S. (2006). Aluminacyclopropene: syntheses, characterization, and reactivity toward terminal alkynes. Journal of the American Chemical Society, 128(15), 5100-8. https://doi.org/10.1021/ja057731p
Zhu, Hongping, et al. "Aluminacyclopropene: syntheses, characterization, and reactivity toward terminal alkynes." Journal of the American Chemical Society vol. 128,15 (2006): 5100-8. doi: https://doi.org/10.1021/ja057731p
Zhu H, Oswald RB, Fan H, Roesky HW, Ma Q, Yang Z, Schmidt HG, Noltemeyer M, Starke K, Hosmane NS. Aluminacyclopropene: syntheses, characterization, and reactivity toward terminal alkynes. J Am Chem Soc. 2006 Apr 19;128(15):5100-8. doi: 10.1021/ja057731p. PMID: 16608344.
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Synthesis of an aluminum spirocyclic hybrid with an inorganic B2O3 and an organic C3N2 core.

Journal of the American Chemical Society

Yang Z, Ma X, Oswald RB, Roesky HW, Noltemeyer M.
PMID: 16984177
J Am Chem Soc. 2006 Sep 27;128(38):12406-7. doi: 10.1021/ja064035w.

The reaction of LAl (L = HC(CMeNAr)2, Ar = 2,6-iPr2C6H3) or LAlH2 with PhB(OH)2 yields the unprecedented spirocyclic LAl[(OBPh)2O] compound. The former reaction proceeds under hydrogen formation and simultaneous oxidation of the aluminum(I).

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Yang Z, Ma X, Oswald RB, et al. Synthesis of an aluminum spirocyclic hybrid with an inorganic B2O3 and an organic C3N2 core. J Am Chem Soc. 2006;128(38):12406-7doi: 10.1021/ja064035w.
Yang, Z., Ma, X., Oswald, R. B., Roesky, H. W., & Noltemeyer, M. (2006). Synthesis of an aluminum spirocyclic hybrid with an inorganic B2O3 and an organic C3N2 core. Journal of the American Chemical Society, 128(38), 12406-7. https://doi.org/10.1021/ja064035w
Yang, Zhi, et al. "Synthesis of an aluminum spirocyclic hybrid with an inorganic B2O3 and an organic C3N2 core." Journal of the American Chemical Society vol. 128,38 (2006): 12406-7. doi: https://doi.org/10.1021/ja064035w
Yang Z, Ma X, Oswald RB, Roesky HW, Noltemeyer M. Synthesis of an aluminum spirocyclic hybrid with an inorganic B2O3 and an organic C3N2 core. J Am Chem Soc. 2006 Sep 27;128(38):12406-7. doi: 10.1021/ja064035w. PMID: 16984177.
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Mononuclear aluminum hydroxide for the design of well-defined homogeneous catalysts.

Journal of the American Chemical Society

Bai G, Singh S, Roesky HW, Noltemeyer M, Schmidt HG.
PMID: 15755164
J Am Chem Soc. 2005 Mar 16;127(10):3449-55. doi: 10.1021/ja043585w.

An unprecedented aluminum hydroxide LAlMe(OH) (5; L = HC[(CMe)(2,6-iPr2C6H3N)]2) has been prepared by the hydrolysis of LAlMeCl (4). For the preparation of 5, the reagents of KOH, water, and KH, as well as the two-phase ammonia/toluene system, were used....

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Bai G, Singh S, Roesky HW, et al. Mononuclear aluminum hydroxide for the design of well-defined homogeneous catalysts. J Am Chem Soc. 2005;127(10):3449-55doi: 10.1021/ja043585w.
Bai, G., Singh, S., Roesky, H. W., Noltemeyer, M., & Schmidt, H. G. (2005). Mononuclear aluminum hydroxide for the design of well-defined homogeneous catalysts. Journal of the American Chemical Society, 127(10), 3449-55. https://doi.org/10.1021/ja043585w
Bai, Guangcai, et al. "Mononuclear aluminum hydroxide for the design of well-defined homogeneous catalysts." Journal of the American Chemical Society vol. 127,10 (2005): 3449-55. doi: https://doi.org/10.1021/ja043585w
Bai G, Singh S, Roesky HW, Noltemeyer M, Schmidt HG. Mononuclear aluminum hydroxide for the design of well-defined homogeneous catalysts. J Am Chem Soc. 2005 Mar 16;127(10):3449-55. doi: 10.1021/ja043585w. PMID: 15755164.
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Ultrafast intramolecular charge transfer and internal conversion with tetrafluoro-aminobenzonitriles.

Chemphyschem : a European journal of chemical physics and physical chemistry

Galievsky VA, Druzhinin SI, Demeter A, Jiang YB, Kovalenko SA, Pérez Lustres L, Venugopal K, Ernsting NP, Allonas X, Noltemeyer M, Machinek R, Zachariasse KA.
PMID: 16273565
Chemphyschem. 2005 Nov 11;6(11):2307-23. doi: 10.1002/cphc.200500267.

The five 2,3,5,6-tetrafluoro-4-aminobenzonitriles XABN4F with a dimethyl-amino (DMABN4F), diethyl-amino (DEABN4F), azetidinyl (AZABN4F), methyl-amino (MABN4F) or amino (ABN4F) group undergo ultrafast intramolecular charge transfer (ICT) at room temperature, in the polar solvent acetonitrile (MeCN) as well as in the nonpolar...

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Galievsky VA, Druzhinin SI, Demeter A, et al. Ultrafast intramolecular charge transfer and internal conversion with tetrafluoro-aminobenzonitriles. Chemphyschem. 2005;6(11):2307-23doi: 10.1002/cphc.200500267.
Galievsky, V. A., Druzhinin, S. I., Demeter, A., Jiang, Y. B., Kovalenko, S. A., Pérez Lustres, L., Venugopal, K., Ernsting, N. P., Allonas, X., Noltemeyer, M., Machinek, R., & Zachariasse, K. A. (2005). Ultrafast intramolecular charge transfer and internal conversion with tetrafluoro-aminobenzonitriles. Chemphyschem : a European journal of chemical physics and physical chemistry, 6(11), 2307-23. https://doi.org/10.1002/cphc.200500267
Galievsky, Victor A, et al. "Ultrafast intramolecular charge transfer and internal conversion with tetrafluoro-aminobenzonitriles." Chemphyschem : a European journal of chemical physics and physical chemistry vol. 6,11 (2005): 2307-23. doi: https://doi.org/10.1002/cphc.200500267
Galievsky VA, Druzhinin SI, Demeter A, Jiang YB, Kovalenko SA, Pérez Lustres L, Venugopal K, Ernsting NP, Allonas X, Noltemeyer M, Machinek R, Zachariasse KA. Ultrafast intramolecular charge transfer and internal conversion with tetrafluoro-aminobenzonitriles. Chemphyschem. 2005 Nov 11;6(11):2307-23. doi: 10.1002/cphc.200500267. PMID: 16273565.
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Pseudohelical and helical primary structures of 1,2-spiroannelated four- and five-membered rings: syntheses and chiroptical properties.

The Journal of organic chemistry

Widjaja T, Fitjer L, Pal A, Schmidt HG, Noltemeyer M, Diedrich C, Grimme S.
PMID: 17973532
J Org Chem. 2007 Nov 23;72(24):9264-77. doi: 10.1021/jo7017558. Epub 2007 Nov 01.

The pseudohelical hydrocarbons (R)-6, (S)-7, and (R)-8 and the helical hydrocarbon (P)-9, formally derived from the helical hydrocarbon (P)-4 by stepwise replacement of each of the four-membered rings by a five-membered ring, have been prepared. Their optical rotations vary...

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Widjaja T, Fitjer L, Pal A, et al. Pseudohelical and helical primary structures of 1,2-spiroannelated four- and five-membered rings: syntheses and chiroptical properties. J Org Chem. 2007;72(24):9264-77doi: 10.1021/jo7017558.
Widjaja, T., Fitjer, L., Pal, A., Schmidt, H. G., Noltemeyer, M., Diedrich, C., & Grimme, S. (2007). Pseudohelical and helical primary structures of 1,2-spiroannelated four- and five-membered rings: syntheses and chiroptical properties. The Journal of organic chemistry, 72(24), 9264-77. https://doi.org/10.1021/jo7017558
Widjaja, Tien, et al. "Pseudohelical and helical primary structures of 1,2-spiroannelated four- and five-membered rings: syntheses and chiroptical properties." The Journal of organic chemistry vol. 72,24 (2007): 9264-77. doi: https://doi.org/10.1021/jo7017558
Widjaja T, Fitjer L, Pal A, Schmidt HG, Noltemeyer M, Diedrich C, Grimme S. Pseudohelical and helical primary structures of 1,2-spiroannelated four- and five-membered rings: syntheses and chiroptical properties. J Org Chem. 2007 Nov 23;72(24):9264-77. doi: 10.1021/jo7017558. Epub 2007 Nov 01. PMID: 17973532.
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[Zn.

Angewandte Chemie (International ed. in English)

Yang Y, Pinkas J, Noltemeyer M, Schmidt HG, Roesky HW.
PMID: 29711560
Angew Chem Int Ed Engl. 1999 Mar 01;38(5):664-666. doi: 10.1002/(SICI)1521-3773(19990301)38:5<664::AID-ANIE664>3.0.CO;2-4.

The largest multinuclear zinc framework synthesized is in the title compound (see picture), which contains structural features closely related to the motifs found in layered and three-dimensional zincophosphates and zincophosphonates. The reactive centers make this zincophosphonate a viable precursor...

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Yang Y, Pinkas J, Noltemeyer M, et al. [Zn. Angew Chem Int Ed Engl. 1999;38(5):664-666doi: 10.1002/(SICI)1521-3773(19990301)38:5<664::AID-ANIE664>3.0.CO;2-4.
Yang, Y., Pinkas, J., Noltemeyer, M., Schmidt, H. G., & Roesky, H. W. (1999). [Zn. Angewandte Chemie (International ed. in English), 38(5), 664-666. https://doi.org/10.1002/(SICI)1521-3773(19990301)38:5<664::AID-ANIE664>3.0.CO;2-4
Yang, Yu, et al. "[Zn." Angewandte Chemie (International ed. in English) vol. 38,5 (1999): 664-666. doi: https://doi.org/10.1002/(SICI)1521-3773(19990301)38:5<664::AID-ANIE664>3.0.CO;2-4
Yang Y, Pinkas J, Noltemeyer M, Schmidt HG, Roesky HW. [Zn. Angew Chem Int Ed Engl. 1999 Mar 01;38(5):664-666. doi: 10.1002/(SICI)1521-3773(19990301)38:5<664::AID-ANIE664>3.0.CO;2-4. PMID: 29711560.
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