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Optimized methods for preparation of 6(I)-(ω-sulfanyl-alkylene-sulfanyl)-β-cyclodextrin derivatives.

Beilstein journal of organic chemistry

Bednářová E, Hybelbauerová S, Jindřich J.
PMID: 26977195
Beilstein J Org Chem. 2016 Feb 24;12:349-52. doi: 10.3762/bjoc.12.38. eCollection 2016.

A general high-yielding method for the preparation of monosubstituted β-cyclodextrin derivatives which have attached a thiol group in position 6 is described. The thiol group is attached through linkers of different lengths and repeating units (ethylene glycol or methylene)....

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Bednářová E, Hybelbauerová S, Jindřich J. Optimized methods for preparation of 6(I)-(ω-sulfanyl-alkylene-sulfanyl)-β-cyclodextrin derivatives. Beilstein J Org Chem. 2016;12:349-52doi: 10.3762/bjoc.12.38.
Bednářová, E., Hybelbauerová, S., & Jindřich, J. (2016). Optimized methods for preparation of 6(I)-(ω-sulfanyl-alkylene-sulfanyl)-β-cyclodextrin derivatives. Beilstein journal of organic chemistry, 12349-52. https://doi.org/10.3762/bjoc.12.38
Bednářová, Eva, et al. "Optimized methods for preparation of 6(I)-(ω-sulfanyl-alkylene-sulfanyl)-β-cyclodextrin derivatives." Beilstein journal of organic chemistry vol. 12 (2016): 349-52. doi: https://doi.org/10.3762/bjoc.12.38
Bednářová E, Hybelbauerová S, Jindřich J. Optimized methods for preparation of 6(I)-(ω-sulfanyl-alkylene-sulfanyl)-β-cyclodextrin derivatives. Beilstein J Org Chem. 2016 Feb 24;12:349-52. doi: 10.3762/bjoc.12.38. eCollection 2016. PMID: 26977195; PMCID: PMC4778511.
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Centimeter-Scale 2D van der Waals Vertical Heterostructures Integrated on Deformable Substrates Enabled by Gold Sacrificial Layer-Assisted Growth.

Nano letters

Islam MA, Kim JH, Schropp A, Kalita H, Choudhary N, Weitzman D, Khondaker SI, Oh KH, Roy T, Chung HS, Jung Y.
PMID: 28945439
Nano Lett. 2017 Oct 11;17(10):6157-6165. doi: 10.1021/acs.nanolett.7b02776. Epub 2017 Sep 27.

Two-dimensional (2D) transition metal dichalcogenides (TMDs) such as molybdenum or tungsten disulfides (MoS

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Islam MA, Kim JH, Schropp A, et al. Centimeter-Scale 2D van der Waals Vertical Heterostructures Integrated on Deformable Substrates Enabled by Gold Sacrificial Layer-Assisted Growth. Nano Lett. 2017;17(10):6157-6165doi: 10.1021/acs.nanolett.7b02776.
Islam, M. A., Kim, J. H., Schropp, A., Kalita, H., Choudhary, N., Weitzman, D., Khondaker, S. I., Oh, K. H., Roy, T., Chung, H. S., & Jung, Y. (2017). Centimeter-Scale 2D van der Waals Vertical Heterostructures Integrated on Deformable Substrates Enabled by Gold Sacrificial Layer-Assisted Growth. Nano letters, 17(10), 6157-6165. https://doi.org/10.1021/acs.nanolett.7b02776
Islam, Md Ashraful, et al. "Centimeter-Scale 2D van der Waals Vertical Heterostructures Integrated on Deformable Substrates Enabled by Gold Sacrificial Layer-Assisted Growth." Nano letters vol. 17,10 (2017): 6157-6165. doi: https://doi.org/10.1021/acs.nanolett.7b02776
Islam MA, Kim JH, Schropp A, Kalita H, Choudhary N, Weitzman D, Khondaker SI, Oh KH, Roy T, Chung HS, Jung Y. Centimeter-Scale 2D van der Waals Vertical Heterostructures Integrated on Deformable Substrates Enabled by Gold Sacrificial Layer-Assisted Growth. Nano Lett. 2017 Oct 11;17(10):6157-6165. doi: 10.1021/acs.nanolett.7b02776. Epub 2017 Sep 27. PMID: 28945439.
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Metal-free sp(3) C-H functionalization: a novel approach for the syntheses of selenide ethers and thioesters from methyl arenes.

Chemical communications (Cambridge, England)

Badsara SS, Liu YC, Hsieh PA, Zeng JW, Lu SY, Liu YW, Lee CF.
PMID: 25122526
Chem Commun (Camb). 2014 Oct 07;50(77):11374-7. doi: 10.1039/c4cc04503c.

A DTBP-promoted metal-free and solvent-free formation of C-Se and C-S bonds through sp(3) C-H functionalization of methyl arenes with diselenides and disulfides is described.

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Badsara SS, Liu YC, Hsieh PA, et al. Metal-free sp(3) C-H functionalization: a novel approach for the syntheses of selenide ethers and thioesters from methyl arenes. Chem Commun (Camb). 2014;50(77):11374-7doi: 10.1039/c4cc04503c.
Badsara, S. S., Liu, Y. C., Hsieh, P. A., Zeng, J. W., Lu, S. Y., Liu, Y. W., & Lee, C. F. (2014). Metal-free sp(3) C-H functionalization: a novel approach for the syntheses of selenide ethers and thioesters from methyl arenes. Chemical communications (Cambridge, England), 50(77), 11374-7. https://doi.org/10.1039/c4cc04503c
Badsara, Satpal Singh, et al. "Metal-free sp(3) C-H functionalization: a novel approach for the syntheses of selenide ethers and thioesters from methyl arenes." Chemical communications (Cambridge, England) vol. 50,77 (2014): 11374-7. doi: https://doi.org/10.1039/c4cc04503c
Badsara SS, Liu YC, Hsieh PA, Zeng JW, Lu SY, Liu YW, Lee CF. Metal-free sp(3) C-H functionalization: a novel approach for the syntheses of selenide ethers and thioesters from methyl arenes. Chem Commun (Camb). 2014 Oct 07;50(77):11374-7. doi: 10.1039/c4cc04503c. PMID: 25122526.
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Synthesis of 2-Sulfenylindenones via One-Pot Tandem Meyer-Schuster Rearrangement and Radical Cyclization of Arylpropynols with Disulfides.

The Journal of organic chemistry

Zhang XS, Jiao JY, Zhang XH, Hu BL, Zhang XG.
PMID: 27232156
J Org Chem. 2016 Jul 01;81(13):5710-6. doi: 10.1021/acs.joc.6b00762. Epub 2016 Jun 09.

A tandem annulation of arylpropynols with disulfides has been developed for the synthesis of 2-sulfenylindenone derivatives. The reaction pathway involves one-pot tandem Meyer-Schuster rearrangement of arylpropynols and successive radical cyclization with disulfides. Various arylpropynols and disulfides with a number...

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Zhang XS, Jiao JY, Zhang XH, et al. Synthesis of 2-Sulfenylindenones via One-Pot Tandem Meyer-Schuster Rearrangement and Radical Cyclization of Arylpropynols with Disulfides. J Org Chem. 2016;81(13):5710-6doi: 10.1021/acs.joc.6b00762.
Zhang, X. S., Jiao, J. Y., Zhang, X. H., Hu, B. L., & Zhang, X. G. (2016). Synthesis of 2-Sulfenylindenones via One-Pot Tandem Meyer-Schuster Rearrangement and Radical Cyclization of Arylpropynols with Disulfides. The Journal of organic chemistry, 81(13), 5710-6. https://doi.org/10.1021/acs.joc.6b00762
Zhang, Xing-Song, et al. "Synthesis of 2-Sulfenylindenones via One-Pot Tandem Meyer-Schuster Rearrangement and Radical Cyclization of Arylpropynols with Disulfides." The Journal of organic chemistry vol. 81,13 (2016): 5710-6. doi: https://doi.org/10.1021/acs.joc.6b00762
Zhang XS, Jiao JY, Zhang XH, Hu BL, Zhang XG. Synthesis of 2-Sulfenylindenones via One-Pot Tandem Meyer-Schuster Rearrangement and Radical Cyclization of Arylpropynols with Disulfides. J Org Chem. 2016 Jul 01;81(13):5710-6. doi: 10.1021/acs.joc.6b00762. Epub 2016 Jun 09. PMID: 27232156.
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Identification of volatile components of bobcat (Lynx rufus) urine.

Journal of chemical ecology

Mattina MJ, Pignatello JJ, Swihart RK.
PMID: 24258737
J Chem Ecol. 1991 Feb;17(2):451-62. doi: 10.1007/BF00994344.

Bobcat (Lynx rufus) urine reduces scent-marking activity of woodchucks (Marmota monax) and feeding activity of snowshoe hares (Lepus americanus) and deer (Odocoileus virginianus, O. hemionus). In order to identify the semiochemicals responsible for these behavior modifications, a dichloromethane extract...

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Mattina MJ, Pignatello JJ, Swihart RK. Identification of volatile components of bobcat (Lynx rufus) urine. J Chem Ecol. 1991;17(2):451-62doi: 10.1007/BF00994344.
Mattina, M. J., Pignatello, J. J., & Swihart, R. K. (1991). Identification of volatile components of bobcat (Lynx rufus) urine. Journal of chemical ecology, 17(2), 451-62. https://doi.org/10.1007/BF00994344
Mattina, M J, et al. "Identification of volatile components of bobcat (Lynx rufus) urine." Journal of chemical ecology vol. 17,2 (1991): 451-62. doi: https://doi.org/10.1007/BF00994344
Mattina MJ, Pignatello JJ, Swihart RK. Identification of volatile components of bobcat (Lynx rufus) urine. J Chem Ecol. 1991 Feb;17(2):451-62. doi: 10.1007/BF00994344. PMID: 24258737.
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Electron Attachment to Diselenides Revisited: Se-Se Bond Cleavage Is Neither Adiabatic nor the Most Favorable Process.

Journal of chemical theory and computation

Gámez JA, Yáñez M.
PMID: 26596436
J Chem Theory Comput. 2011 Jun 14;7(6):1726-35. doi: 10.1021/ct2002286. Epub 2011 May 24.

Up to now it has been generally assumed that the electron capture on diselenides XSeSeX' produces a fragmentation of the Se-Se bond. However, our high-level ab initio calculations indicate that this is the case only when the substituents X...

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Gámez JA, Yáñez M. Electron Attachment to Diselenides Revisited: Se-Se Bond Cleavage Is Neither Adiabatic nor the Most Favorable Process. J Chem Theory Comput. 2011;7(6):1726-35doi: 10.1021/ct2002286.
Gámez, J. A., & Yáñez, M. (2011). Electron Attachment to Diselenides Revisited: Se-Se Bond Cleavage Is Neither Adiabatic nor the Most Favorable Process. Journal of chemical theory and computation, 7(6), 1726-35. https://doi.org/10.1021/ct2002286
Gámez, José A, and Yáñez, Manuel. "Electron Attachment to Diselenides Revisited: Se-Se Bond Cleavage Is Neither Adiabatic nor the Most Favorable Process." Journal of chemical theory and computation vol. 7,6 (2011): 1726-35. doi: https://doi.org/10.1021/ct2002286
Gámez JA, Yáñez M. Electron Attachment to Diselenides Revisited: Se-Se Bond Cleavage Is Neither Adiabatic nor the Most Favorable Process. J Chem Theory Comput. 2011 Jun 14;7(6):1726-35. doi: 10.1021/ct2002286. Epub 2011 May 24. PMID: 26596436.
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Selective Thiolative Lactonization of Internal Alkynes Bearing a Hydroxyl Group with Carbon Monoxide and Organic Disulfides Catalyzed by Transition-Metal Complexes.

The Journal of organic chemistry

Higashimae S, Tamai T, Nomoto A, Ogawa A.
PMID: 26072971
J Org Chem. 2015 Jul 17;80(14):7126-33. doi: 10.1021/acs.joc.5b00977. Epub 2015 Jul 07.

Although many transition-metal catalysts are ineffective for the addition and carbonylative addition of organic disulfides to internal alkynes, dicobalt octacarbonyl and palladium complexes such as Pd(PPh3)4 and Pd(OAc)2 were found to exhibit excellent catalytic activity for the thiolative lactonization...

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Higashimae S, Tamai T, Nomoto A, et al. Selective Thiolative Lactonization of Internal Alkynes Bearing a Hydroxyl Group with Carbon Monoxide and Organic Disulfides Catalyzed by Transition-Metal Complexes. J Org Chem. 2015;80(14):7126-33doi: 10.1021/acs.joc.5b00977.
Higashimae, S., Tamai, T., Nomoto, A., & Ogawa, A. (2015). Selective Thiolative Lactonization of Internal Alkynes Bearing a Hydroxyl Group with Carbon Monoxide and Organic Disulfides Catalyzed by Transition-Metal Complexes. The Journal of organic chemistry, 80(14), 7126-33. https://doi.org/10.1021/acs.joc.5b00977
Higashimae, Shinya, et al. "Selective Thiolative Lactonization of Internal Alkynes Bearing a Hydroxyl Group with Carbon Monoxide and Organic Disulfides Catalyzed by Transition-Metal Complexes." The Journal of organic chemistry vol. 80,14 (2015): 7126-33. doi: https://doi.org/10.1021/acs.joc.5b00977
Higashimae S, Tamai T, Nomoto A, Ogawa A. Selective Thiolative Lactonization of Internal Alkynes Bearing a Hydroxyl Group with Carbon Monoxide and Organic Disulfides Catalyzed by Transition-Metal Complexes. J Org Chem. 2015 Jul 17;80(14):7126-33. doi: 10.1021/acs.joc.5b00977. Epub 2015 Jul 07. PMID: 26072971.
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HOF·CH3CN: probably the best oxygen transfer agent organic chemistry has to offer.

Accounts of chemical research

Rozen S.
PMID: 24871453
Acc Chem Res. 2014 Aug 19;47(8):2378-89. doi: 10.1021/ar500107b. Epub 2014 May 28.

The complex HOF·CH3CN is readily obtained by bubbling dilute fluorine into aqueous acetonitrile solution. It does not have to be purified or isolated, and its solution can react as is, after the concentration has been establish by any iodometric...

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Rozen S. HOF·CH3CN: probably the best oxygen transfer agent organic chemistry has to offer. Acc Chem Res. 2014;47(8):2378-89doi: 10.1021/ar500107b.
Rozen, S. (2014). HOF·CH3CN: probably the best oxygen transfer agent organic chemistry has to offer. Accounts of chemical research, 47(8), 2378-89. https://doi.org/10.1021/ar500107b
Rozen, Shlomo. "HOF·CH3CN: probably the best oxygen transfer agent organic chemistry has to offer." Accounts of chemical research vol. 47,8 (2014): 2378-89. doi: https://doi.org/10.1021/ar500107b
Rozen S. HOF·CH3CN: probably the best oxygen transfer agent organic chemistry has to offer. Acc Chem Res. 2014 Aug 19;47(8):2378-89. doi: 10.1021/ar500107b. Epub 2014 May 28. PMID: 24871453.
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Quantifying Changes in the Cellular Thiol-Disulfide Status during Differentiation of B Cells into Antibody-Secreting Plasma Cells.

International journal of cell biology

Hansen RE, Otsu M, Braakman I, Winther JR.
PMID: 24223594
Int J Cell Biol. 2013;2013:898563. doi: 10.1155/2013/898563. Epub 2013 Sep 24.

Plasma cells produce and secrete massive amounts of disulfide-containing antibodies. To accommodate this load on the secretory machinery, the differentiation of resting B cells into antibody-secreting plasma cells is accompanied by a preferential expansion of the secretory compartments of...

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Hansen RE, Otsu M, Braakman I, et al. Quantifying Changes in the Cellular Thiol-Disulfide Status during Differentiation of B Cells into Antibody-Secreting Plasma Cells. Int J Cell Biol. 2013;2013:898563doi: 10.1155/2013/898563.
Hansen, R. E., Otsu, M., Braakman, I., & Winther, J. R. (2013). Quantifying Changes in the Cellular Thiol-Disulfide Status during Differentiation of B Cells into Antibody-Secreting Plasma Cells. International journal of cell biology, 2013898563. https://doi.org/10.1155/2013/898563
Hansen, Rosa E, et al. "Quantifying Changes in the Cellular Thiol-Disulfide Status during Differentiation of B Cells into Antibody-Secreting Plasma Cells." International journal of cell biology vol. 2013 (2013): 898563. doi: https://doi.org/10.1155/2013/898563
Hansen RE, Otsu M, Braakman I, Winther JR. Quantifying Changes in the Cellular Thiol-Disulfide Status during Differentiation of B Cells into Antibody-Secreting Plasma Cells. Int J Cell Biol. 2013;2013:898563. doi: 10.1155/2013/898563. Epub 2013 Sep 24. PMID: 24223594; PMCID: PMC3800581.
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Nickel-catalyzed thiolation of unactivated aryl C-H bonds: efficient access to diverse aryl sulfides.

Chemical communications (Cambridge, England)

Yan SY, Liu YJ, Liu B, Liu YH, Shi BF.
PMID: 25661824
Chem Commun (Camb). 2015 Mar 07;51(19):4069-72. doi: 10.1039/c4cc10446c.

A nickel-catalyzed thiolation of unactivated C(sp(2))-H bonds with disulfides employing the PIP directing group was described. This process uses a catalytic nickel catalyst and no metallic oxidants or cocatalysts are required. The reaction tolerates various important functional groups and...

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Yan SY, Liu YJ, Liu B, et al. Nickel-catalyzed thiolation of unactivated aryl C-H bonds: efficient access to diverse aryl sulfides. Chem Commun (Camb). 2015;51(19):4069-72doi: 10.1039/c4cc10446c.
Yan, S. Y., Liu, Y. J., Liu, B., Liu, Y. H., & Shi, B. F. (2015). Nickel-catalyzed thiolation of unactivated aryl C-H bonds: efficient access to diverse aryl sulfides. Chemical communications (Cambridge, England), 51(19), 4069-72. https://doi.org/10.1039/c4cc10446c
Yan, Sheng-Yi, et al. "Nickel-catalyzed thiolation of unactivated aryl C-H bonds: efficient access to diverse aryl sulfides." Chemical communications (Cambridge, England) vol. 51,19 (2015): 4069-72. doi: https://doi.org/10.1039/c4cc10446c
Yan SY, Liu YJ, Liu B, Liu YH, Shi BF. Nickel-catalyzed thiolation of unactivated aryl C-H bonds: efficient access to diverse aryl sulfides. Chem Commun (Camb). 2015 Mar 07;51(19):4069-72. doi: 10.1039/c4cc10446c. PMID: 25661824.
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Modified denatured lysozyme effectively solubilizes fullerene c60 nanoparticles in water.

Nanotechnology

Siepi M, Politi J, Dardano P, Amoresano A, De Stefano L, Maria Monti D, Notomista E.
PMID: 28525394
Nanotechnology. 2017 Aug 18;28(33):335601. doi: 10.1088/1361-6528/aa744e. Epub 2017 May 19.

Fullerenes, allotropic forms of carbon, have very interesting pharmacological effects and engineering applications. However, a very low solubility both in organic solvents and water hinders their use. Fullerene C60, the most studied among fullerenes, can be dissolved in water...

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Siepi M, Politi J, Dardano P, et al. Modified denatured lysozyme effectively solubilizes fullerene c60 nanoparticles in water. Nanotechnology. 2017;28(33):335601doi: 10.1088/1361-6528/aa744e.
Siepi, M., Politi, J., Dardano, P., Amoresano, A., De Stefano, L., Maria Monti, D., & Notomista, E. (2017). Modified denatured lysozyme effectively solubilizes fullerene c60 nanoparticles in water. Nanotechnology, 28(33), 335601. https://doi.org/10.1088/1361-6528/aa744e
Siepi, Marialuisa, et al. "Modified denatured lysozyme effectively solubilizes fullerene c60 nanoparticles in water." Nanotechnology vol. 28,33 (2017): 335601. doi: https://doi.org/10.1088/1361-6528/aa744e
Siepi M, Politi J, Dardano P, Amoresano A, De Stefano L, Maria Monti D, Notomista E. Modified denatured lysozyme effectively solubilizes fullerene c60 nanoparticles in water. Nanotechnology. 2017 Aug 18;28(33):335601. doi: 10.1088/1361-6528/aa744e. Epub 2017 May 19. PMID: 28525394.
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Even-odd layer-dependent magnetotransport of high-mobility Q-valley electrons in transition metal disulfides.

Nature communications

Wu Z, Xu S, Lu H, Khamoshi A, Liu GB, Han T, Wu Y, Lin J, Long G, He Y, Cai Y, Yao Y, Zhang F, Wang N.
PMID: 27651106
Nat Commun. 2016 Sep 21;7:12955. doi: 10.1038/ncomms12955.

In few-layer transition metal dichalcogenides (TMDCs), the conduction bands along the ΓK directions shift downward energetically in the presence of interlayer interactions, forming six Q valleys related by threefold rotational symmetry and time reversal symmetry. In even layers, the...

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Wu Z, Xu S, Lu H, et al. Even-odd layer-dependent magnetotransport of high-mobility Q-valley electrons in transition metal disulfides. Nat Commun. 2016;7:12955doi: 10.1038/ncomms12955.
Wu, Z., Xu, S., Lu, H., Khamoshi, A., Liu, G. B., Han, T., Wu, Y., Lin, J., Long, G., He, Y., Cai, Y., Yao, Y., Zhang, F., & Wang, N. (2016). Even-odd layer-dependent magnetotransport of high-mobility Q-valley electrons in transition metal disulfides. Nature communications, 712955. https://doi.org/10.1038/ncomms12955
Wu, Zefei, et al. "Even-odd layer-dependent magnetotransport of high-mobility Q-valley electrons in transition metal disulfides." Nature communications vol. 7 (2016): 12955. doi: https://doi.org/10.1038/ncomms12955
Wu Z, Xu S, Lu H, Khamoshi A, Liu GB, Han T, Wu Y, Lin J, Long G, He Y, Cai Y, Yao Y, Zhang F, Wang N. Even-odd layer-dependent magnetotransport of high-mobility Q-valley electrons in transition metal disulfides. Nat Commun. 2016 Sep 21;7:12955. doi: 10.1038/ncomms12955. PMID: 27651106; PMCID: PMC5036047.
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Showing 1 to 12 of 588 entries