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Showing 1 to 12 of 14 entries
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Sensitive analysis of two barbiturates in human urine by capillary electrophoresis with sample stacking induced by moving reaction boundary.

Analytica chimica acta

Wang QL, Fan LY, Zhang W, Cao CX.
PMID: 17723774
Anal Chim Acta. 2006 Nov 24;580(2):200-5. doi: 10.1016/j.aca.2006.07.073. Epub 2006 Aug 04.

An on-line stacking method based on moving reaction boundary (MRB) was developed for the sensitive determination of barbital and phenobarbital in human urine via capillary electrophoresis (CE). The optimized conditions for the method are: 60 mmol L(-1) pH 11.0...

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Wang QL, Fan LY, Zhang W, et al. Sensitive analysis of two barbiturates in human urine by capillary electrophoresis with sample stacking induced by moving reaction boundary. Anal Chim Acta. 2006;580(2):200-5doi: 10.1016/j.aca.2006.07.073.
Wang, Q. L., Fan, L. Y., Zhang, W., & Cao, C. X. (2006). Sensitive analysis of two barbiturates in human urine by capillary electrophoresis with sample stacking induced by moving reaction boundary. Analytica chimica acta, 580(2), 200-5. https://doi.org/10.1016/j.aca.2006.07.073
Wang, Qiu-Ling, et al. "Sensitive analysis of two barbiturates in human urine by capillary electrophoresis with sample stacking induced by moving reaction boundary." Analytica chimica acta vol. 580,2 (2006): 200-5. doi: https://doi.org/10.1016/j.aca.2006.07.073
Wang QL, Fan LY, Zhang W, Cao CX. Sensitive analysis of two barbiturates in human urine by capillary electrophoresis with sample stacking induced by moving reaction boundary. Anal Chim Acta. 2006 Nov 24;580(2):200-5. doi: 10.1016/j.aca.2006.07.073. Epub 2006 Aug 04. PMID: 17723774.
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Chiral separations using polymeric surfactants and polyelectrolyte multilayers in open-tubular capillary electrochromatography.

Analytical chemistry

Kapnissi CP, Valle BC, Warner IM.
PMID: 14615987
Anal Chem. 2003 Nov 15;75(22):6097-104. doi: 10.1021/ac034452g.

In this study, fused-silica capillaries are modified using a polyelectrolyte multilayer (PEM) coating procedure in open-tubular capillary electrochromatography. The PEM coating was constructed in situ with alternating rinses of positively and negatively charged polymers. The quaternary ammonium salt poly...

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Kapnissi CP, Valle BC, Warner IM. Chiral separations using polymeric surfactants and polyelectrolyte multilayers in open-tubular capillary electrochromatography. Anal Chem. 2003;75(22):6097-104doi: 10.1021/ac034452g.
Kapnissi, C. P., Valle, B. C., & Warner, I. M. (2003). Chiral separations using polymeric surfactants and polyelectrolyte multilayers in open-tubular capillary electrochromatography. Analytical chemistry, 75(22), 6097-104. https://doi.org/10.1021/ac034452g
Kapnissi, Constantina P, et al. "Chiral separations using polymeric surfactants and polyelectrolyte multilayers in open-tubular capillary electrochromatography." Analytical chemistry vol. 75,22 (2003): 6097-104. doi: https://doi.org/10.1021/ac034452g
Kapnissi CP, Valle BC, Warner IM. Chiral separations using polymeric surfactants and polyelectrolyte multilayers in open-tubular capillary electrochromatography. Anal Chem. 2003 Nov 15;75(22):6097-104. doi: 10.1021/ac034452g. PMID: 14615987.
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Simultaneous Determination of Phenobarbital, Pentobarbital, Amobarbital and Secobarbital in Raw Milk via Liquid Chromatography with Electron Spray Ionization Tandem Mass Spectrometry.

Korean journal for food science of animal resources

Tian H, Zhou X, Chen C, He Y, Yu H, Zheng X.
PMID: 29725206
Korean J Food Sci Anim Resour. 2017;37(6):847-854. doi: 10.5851/kosfa.2017.37.6.847. Epub 2017 Dec 31.

A rapid, sensitive and specific liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed for the simultaneous determination of four barbiturates (phenobarbital, pentobarbital, amobarbital and secobarbital) in raw milk. The barbiturates were extracted using liquid-liquid extraction, ultrasonication and centrifugation, and...

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Tian H, Zhou X, Chen C, et al. Simultaneous Determination of Phenobarbital, Pentobarbital, Amobarbital and Secobarbital in Raw Milk via Liquid Chromatography with Electron Spray Ionization Tandem Mass Spectrometry. Korean J Food Sci Anim Resour. 2017;37(6):847-854doi: 10.5851/kosfa.2017.37.6.847.
Tian, H., Zhou, X., Chen, C., He, Y., Yu, H., & Zheng, X. (2017). Simultaneous Determination of Phenobarbital, Pentobarbital, Amobarbital and Secobarbital in Raw Milk via Liquid Chromatography with Electron Spray Ionization Tandem Mass Spectrometry. Korean journal for food science of animal resources, 37(6), 847-854. https://doi.org/10.5851/kosfa.2017.37.6.847
Tian, Huaixiang, et al. "Simultaneous Determination of Phenobarbital, Pentobarbital, Amobarbital and Secobarbital in Raw Milk via Liquid Chromatography with Electron Spray Ionization Tandem Mass Spectrometry." Korean journal for food science of animal resources vol. 37,6 (2017): 847-854. doi: https://doi.org/10.5851/kosfa.2017.37.6.847
Tian H, Zhou X, Chen C, He Y, Yu H, Zheng X. Simultaneous Determination of Phenobarbital, Pentobarbital, Amobarbital and Secobarbital in Raw Milk via Liquid Chromatography with Electron Spray Ionization Tandem Mass Spectrometry. Korean J Food Sci Anim Resour. 2017;37(6):847-854. doi: 10.5851/kosfa.2017.37.6.847. Epub 2017 Dec 31. PMID: 29725206; PMCID: PMC5932935.
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Erratum.

Science (New York, N.Y.)

[No authors listed]
PMID: 17837051
Science. 1958 Feb 28;127(3296):465. doi: 10.1126/science.127.3296.465.

the term Seconal, a trademark of Eli Lilly and Company for secobarbital sodium, was used as a generic term in the issue of 20 Dec. 1957 (vol. 126, p. 1120, column 2, line 48).

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Erratum. Science. 1958;127(3296):465doi: 10.1126/science.127.3296.465.
(1958). Erratum. Science (New York, N.Y.), 127(3296), 465. https://doi.org/10.1126/science.127.3296.465
"Erratum." Science (New York, N.Y.) vol. 127,3296 (1958): 465. doi: https://doi.org/10.1126/science.127.3296.465
Erratum. Science. 1958 Feb 28;127(3296):465. doi: 10.1126/science.127.3296.465. PMID: 17837051.
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Old and Cold: A Novel Case of Combined Secobarbital and Pentobarbital Poisoning in an Elderly Woman.

Cureus

Katz KD, Koons A, Makar G, Wier A.
PMID: 33552764
Cureus. 2021 Jan 03;13(1):e12446. doi: 10.7759/cureus.12446.

A 94-year-old woman was found unresponsive in her room at an independent living facility. Upon paramedic arrival, the patient had a Glasgow Coma Scale of 3, and she was transported to the emergency department (ED). In the ED, she...

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Katz KD, Koons A, Makar G, et al. Old and Cold: A Novel Case of Combined Secobarbital and Pentobarbital Poisoning in an Elderly Woman. Cureus. 2021;13(1):e12446doi: 10.7759/cureus.12446.
Katz, K. D., Koons, A., Makar, G., & Wier, A. (2021). Old and Cold: A Novel Case of Combined Secobarbital and Pentobarbital Poisoning in an Elderly Woman. Cureus, 13(1), e12446. https://doi.org/10.7759/cureus.12446
Katz, Kenneth D, et al. "Old and Cold: A Novel Case of Combined Secobarbital and Pentobarbital Poisoning in an Elderly Woman." Cureus vol. 13,1 (2021): e12446. doi: https://doi.org/10.7759/cureus.12446
Katz KD, Koons A, Makar G, Wier A. Old and Cold: A Novel Case of Combined Secobarbital and Pentobarbital Poisoning in an Elderly Woman. Cureus. 2021 Jan 03;13(1):e12446. doi: 10.7759/cureus.12446. PMID: 33552764; PMCID: PMC7854340.
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Quantitative analysis of thiamylal and its metabolite secobarbital using liquid chromatography-tandem mass spectrometry in adipose tissue, serum, and liver.

Journal of forensic sciences

Yoshioka N, Asano M, Kuse A, Kondo T, Takahashi M, Morichika M, Nakagawa K, Sakurada M, Ueno Y.
PMID: 34970733
J Forensic Sci. 2021 Dec 30; doi: 10.1111/1556-4029.14965. Epub 2021 Dec 30.

Thiamylal is an ultrashort-acting barbiturate used for intravenous administration or general anesthesia induction. However, some cases of poisoning and suicide with thiamylal administration have been reported. Additionally, there are few reports on its analysis in the organs and adipose...

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Yoshioka N, Asano M, Kuse A, et al. Quantitative analysis of thiamylal and its metabolite secobarbital using liquid chromatography-tandem mass spectrometry in adipose tissue, serum, and liver. J Forensic Sci. 2021;doi: 10.1111/1556-4029.14965.
Yoshioka, N., Asano, M., Kuse, A., Kondo, T., Takahashi, M., Morichika, M., Nakagawa, K., Sakurada, M., & Ueno, Y. (2021). Quantitative analysis of thiamylal and its metabolite secobarbital using liquid chromatography-tandem mass spectrometry in adipose tissue, serum, and liver. Journal of forensic sciences, . https://doi.org/10.1111/1556-4029.14965
Yoshioka, Naoki, et al. "Quantitative analysis of thiamylal and its metabolite secobarbital using liquid chromatography-tandem mass spectrometry in adipose tissue, serum, and liver." Journal of forensic sciences vol. (2021). doi: https://doi.org/10.1111/1556-4029.14965
Yoshioka N, Asano M, Kuse A, Kondo T, Takahashi M, Morichika M, Nakagawa K, Sakurada M, Ueno Y. Quantitative analysis of thiamylal and its metabolite secobarbital using liquid chromatography-tandem mass spectrometry in adipose tissue, serum, and liver. J Forensic Sci. 2021 Dec 30; doi: 10.1111/1556-4029.14965. Epub 2021 Dec 30. PMID: 34970733.
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1H NMR spectral simplification with achiral and chiral lanthanide shift reagents--IV. Thiopental and barbiturate analogues.

Journal of pharmaceutical and biomedical analysis

Eberhart ST, Hatzis A, Jimenez J, Rothchild R, Simons P.
PMID: 16867520
J Pharm Biomed Anal. 1987;5(3):233-45. doi: 10.1016/0731-7085(87)80027-4.

The 60 MHz (1)H NMR spectra of racemic thiopental, 1, have been studied with the achiral shift reagent, tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato) europium(III), 2, and the chiral tris[3-(trifluoromethylhydroxymethylene)-d-camphorato] europium(III), 3, and tris[3-(heptafluoropropylhydroxymethylene)-d-camphorato] europium(III), 4. Enantiomeric shift differences, DeltaDeltadelta, were clearly observed for...

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Eberhart ST, Hatzis A, Jimenez J, et al. 1H NMR spectral simplification with achiral and chiral lanthanide shift reagents--IV. Thiopental and barbiturate analogues. J Pharm Biomed Anal. 1987;5(3):233-45doi: 10.1016/0731-7085(87)80027-4.
Eberhart, S. T., Hatzis, A., Jimenez, J., Rothchild, R., & Simons, P. (1987). 1H NMR spectral simplification with achiral and chiral lanthanide shift reagents--IV. Thiopental and barbiturate analogues. Journal of pharmaceutical and biomedical analysis, 5(3), 233-45. https://doi.org/10.1016/0731-7085(87)80027-4
Eberhart, S T, et al. "1H NMR spectral simplification with achiral and chiral lanthanide shift reagents--IV. Thiopental and barbiturate analogues." Journal of pharmaceutical and biomedical analysis vol. 5,3 (1987): 233-45. doi: https://doi.org/10.1016/0731-7085(87)80027-4
Eberhart ST, Hatzis A, Jimenez J, Rothchild R, Simons P. 1H NMR spectral simplification with achiral and chiral lanthanide shift reagents--IV. Thiopental and barbiturate analogues. J Pharm Biomed Anal. 1987;5(3):233-45. doi: 10.1016/0731-7085(87)80027-4. PMID: 16867520.
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[Experimental meningoencephalitis by Naegleria fowleri in mice].

Kisaengch'unghak chapchi. The Korean journal of parasitology

Ahn MH, Im KI.
PMID: 12891021
Kisaengchunghak Chapchi. 1984 Dec;22(2):253-258. doi: 10.3347/kjp.1984.22.2.253.

Experimentally, primary amoebic meningoencephalitis (PAM) is induced by Naegleria fowleri in mouse and development of PAM may be influenced by the strain, weight and sex of mouse, and inoculum size of N. fowleri trophozoite. In this paper, the effect...

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Ahn MH, Im KI. [Experimental meningoencephalitis by Naegleria fowleri in mice]. Kisaengchunghak Chapchi. 1984;22(2):253-258doi: 10.3347/kjp.1984.22.2.253.
Ahn, M. H., & Im, K. I. (1984). [Experimental meningoencephalitis by Naegleria fowleri in mice]. Kisaengch'unghak chapchi. The Korean journal of parasitology, 22(2), 253-258. https://doi.org/10.3347/kjp.1984.22.2.253
Ahn, Myoung Hee, and Im, Kyung Il. "[Experimental meningoencephalitis by Naegleria fowleri in mice]." Kisaengch'unghak chapchi. The Korean journal of parasitology vol. 22,2 (1984): 253-258. doi: https://doi.org/10.3347/kjp.1984.22.2.253
Ahn MH, Im KI. [Experimental meningoencephalitis by Naegleria fowleri in mice]. Kisaengchunghak Chapchi. 1984 Dec;22(2):253-258. doi: 10.3347/kjp.1984.22.2.253. Korean. PMID: 12891021.
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13C4-secobarbital as the internal standard for the quantitative determination of secobarbital--a critical evaluation.

Journal of forensic sciences

Chang WT, Lin DL, Low IA, Liu RH.
PMID: 10855973
J Forensic Sci. 2000 May;45(3):659-64.

In this study, 13C4-secobarbital was used as an exemplar compound to illustrate the mechanism based on which the effectiveness of a proposed internal standard (IS) could be evaluated. A deuterated analog, 2H5-secobarbital, was also studied in parallel for comparison...

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Chang WT, Lin DL, Low IA, et al. 13C4-secobarbital as the internal standard for the quantitative determination of secobarbital--a critical evaluation. J Forensic Sci. 2000;45(3):659-64
Chang, W. T., Lin, D. L., Low, I. A., & Liu, R. H. (2000). 13C4-secobarbital as the internal standard for the quantitative determination of secobarbital--a critical evaluation. Journal of forensic sciences, 45(3), 659-64.
Chang, et al. "13C4-secobarbital as the internal standard for the quantitative determination of secobarbital--a critical evaluation." Journal of forensic sciences vol. 45,3 (2000): 659-64.
Chang WT, Lin DL, Low IA, Liu RH. 13C4-secobarbital as the internal standard for the quantitative determination of secobarbital--a critical evaluation. J Forensic Sci. 2000 May;45(3):659-64. PMID: 10855973.
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Sulpholane as a solvent for titration of barbiturates and sulpha drugs.

Talanta

Buxton TL, Caruso JA.
PMID: 18961269
Talanta. 1973 Feb;20(2):254-6. doi: 10.1016/0039-9140(73)80281-4.

Sulpholane (tetramethylenesulphone) has been used as the medium for non-aqueous potentiometric titration of barbiturates and sulpha drugs with tetrabutylammonium hydroxide. Recoveries for 0.1-0.3 mmole of barbituric acid, phenobarbital, amobarbital, barbital, secobarbital, sulphapyridine, sulphadiazine and sulphamerazine were generally in the...

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Buxton TL, Caruso JA. Sulpholane as a solvent for titration of barbiturates and sulpha drugs. Talanta. 1973;20(2):254-6doi: 10.1016/0039-9140(73)80281-4.
Buxton, T. L., & Caruso, J. A. (1973). Sulpholane as a solvent for titration of barbiturates and sulpha drugs. Talanta, 20(2), 254-6. https://doi.org/10.1016/0039-9140(73)80281-4
Buxton, T L, and Caruso, J A. "Sulpholane as a solvent for titration of barbiturates and sulpha drugs." Talanta vol. 20,2 (1973): 254-6. doi: https://doi.org/10.1016/0039-9140(73)80281-4
Buxton TL, Caruso JA. Sulpholane as a solvent for titration of barbiturates and sulpha drugs. Talanta. 1973 Feb;20(2):254-6. doi: 10.1016/0039-9140(73)80281-4. PMID: 18961269.
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The history of barbiturates a century after their clinical introduction.

Neuropsychiatric disease and treatment

López-Muñoz F, Ucha-Udabe R, Alamo C.
PMID: 18568113
Neuropsychiatr Dis Treat. 2005 Dec;1(4):329-43.

The present work offers an analysis of the historical development of the discovery and use of barbiturates in the field of psychiatry and neurology, a century after their clinical introduction. Beginning with the synthesis of malonylurea by von Baeyer...

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López-Muñoz F, Ucha-Udabe R, Alamo C. The history of barbiturates a century after their clinical introduction. Neuropsychiatr Dis Treat. 2005;1(4):329-43
López-Muñoz, F., Ucha-Udabe, R., & Alamo, C. (2005). The history of barbiturates a century after their clinical introduction. Neuropsychiatric disease and treatment, 1(4), 329-43.
López-Muñoz, Francisco, et al. "The history of barbiturates a century after their clinical introduction." Neuropsychiatric disease and treatment vol. 1,4 (2005): 329-43.
López-Muñoz F, Ucha-Udabe R, Alamo C. The history of barbiturates a century after their clinical introduction. Neuropsychiatr Dis Treat. 2005 Dec;1(4):329-43. PMID: 18568113; PMCID: PMC2424120.
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[Ultrastructural observation of Naegleria fowleri trophozoite in mouse brain and axenic culture].

Kisaengch'unghak chapchi. The Korean journal of parasitology

Ryu JS, Soh CT, Im KI.
PMID: 12891022
Kisaengchunghak Chapchi. 1984 Dec;22(2):259-266. doi: 10.3347/kjp.1984.22.2.259.

Present study was undertaken to elucidate the changes of the ultrastructure of Naegleria fowleri trophozoite in brain tissue of mice and culture medium. Naegleria fowleri, 0359 strain, which used in this study was cultured in axenic liquid medium, CGVS...

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Ryu JS, Soh CT, Im KI. [Ultrastructural observation of Naegleria fowleri trophozoite in mouse brain and axenic culture]. Kisaengchunghak Chapchi. 1984;22(2):259-266doi: 10.3347/kjp.1984.22.2.259.
Ryu, J. S., Soh, C. T., & Im, K. I. (1984). [Ultrastructural observation of Naegleria fowleri trophozoite in mouse brain and axenic culture]. Kisaengch'unghak chapchi. The Korean journal of parasitology, 22(2), 259-266. https://doi.org/10.3347/kjp.1984.22.2.259
Ryu, Jae Sook, et al. "[Ultrastructural observation of Naegleria fowleri trophozoite in mouse brain and axenic culture]." Kisaengch'unghak chapchi. The Korean journal of parasitology vol. 22,2 (1984): 259-266. doi: https://doi.org/10.3347/kjp.1984.22.2.259
Ryu JS, Soh CT, Im KI. [Ultrastructural observation of Naegleria fowleri trophozoite in mouse brain and axenic culture]. Kisaengchunghak Chapchi. 1984 Dec;22(2):259-266. doi: 10.3347/kjp.1984.22.2.259. Korean. PMID: 12891022.
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